MX170640B - Preparacion de alcanosulfonamidas - Google Patents
Preparacion de alcanosulfonamidasInfo
- Publication number
- MX170640B MX170640B MX018528A MX1852889A MX170640B MX 170640 B MX170640 B MX 170640B MX 018528 A MX018528 A MX 018528A MX 1852889 A MX1852889 A MX 1852889A MX 170640 B MX170640 B MX 170640B
- Authority
- MX
- Mexico
- Prior art keywords
- carbon atoms
- alkyl
- formula
- preparation
- chlorine
- Prior art date
Links
- 125000004432 carbon atom Chemical group C* 0.000 abstract 4
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 2
- 229910052801 chlorine Inorganic materials 0.000 abstract 2
- 239000000460 chlorine Substances 0.000 abstract 2
- 229910052731 fluorine Inorganic materials 0.000 abstract 2
- 239000011737 fluorine Substances 0.000 abstract 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- -1 alkanesulfonyl halide Chemical class 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 150000004292 cyclic ethers Chemical class 0.000 abstract 1
- 125000001153 fluoro group Chemical group F* 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical group II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/38—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reaction of ammonia or amines with sulfonic acids, or with esters, anhydrides, or halides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Enzymes And Modification Thereof (AREA)
Abstract
La presente invención se refiere a un procedimiento para la preparación de alcanosulfonamidas que tienen la fórmula: R-SO2 NR1 R2 en donde R se selecciona de alquilo de 1 a 20 átomos de carbono o alquilo de 1 a 20 átomos de carbono sustituido con uno o más de cloro, flúor o mezclas de ellos; y R1 y R2 pueden ser iguales o diferentes y se seleccionan de hidrógeno o alquilo de 1 a 20 átomos de carbono, caracterizado porque comprende tratar un halogenuro de alcansulfonilo que tiene la fórmula: RSO2X en donde R es como se definió anteriormente y X es flúor, cloro, bromo o yodo, con una cantidad efectiva de un compuesto de la fórmula: HNR1 R2 en donde R1 y R2 son como se definió anterior mente, en presencia de un solvente seleccionado de eteres ciclicos de 4 a 8 átomos de carbono o sus mezclas.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/277,824 US4970339A (en) | 1988-11-30 | 1988-11-30 | Preparation of alkanesulfonamides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX170640B true MX170640B (es) | 1993-09-02 |
Family
ID=23062504
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX018528A MX170640B (es) | 1988-11-30 | 1989-11-29 | Preparacion de alcanosulfonamidas |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4970339A (es) |
| EP (1) | EP0371271B1 (es) |
| JP (1) | JPH02200661A (es) |
| BR (1) | BR8906056A (es) |
| CA (1) | CA2001876A1 (es) |
| DE (1) | DE68905908T2 (es) |
| DK (1) | DK601489A (es) |
| MX (1) | MX170640B (es) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5166431A (en) * | 1988-11-30 | 1992-11-24 | Elf Atochem North America, Inc. | Preparation of alkanesulfonamides |
| JPH0687820A (ja) * | 1991-03-21 | 1994-03-29 | Hoechst Ag | N−アルキルスルホンアミドの製法 |
| IT1264813B1 (it) * | 1993-07-28 | 1996-10-10 | Oxon Italia Spa | Procedimento per la preparazione di alcansolfonammidi |
| US5599983A (en) * | 1995-08-21 | 1997-02-04 | Smith; Gary S. | Preparation of alkanesulfonamides with low residual ammonium impurities |
| US5618976A (en) * | 1996-03-06 | 1997-04-08 | Elf Atochem North America, Inc. | Alkanesulfonamides from ammonium alkanesulfonates |
| CN105949092A (zh) * | 2016-06-21 | 2016-09-21 | 太仓市东明化工有限公司 | 一种甲基磺酰胺的制备方法 |
| CN115448857A (zh) * | 2021-06-08 | 2022-12-09 | 联化科技(台州)有限公司 | 一种连续化制备磺酰胺类化合物的方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA466527A (en) * | 1950-07-11 | Chemical Developments Of Canada Limited | Organic sulphur compounds | |
| US3300529A (en) * | 1964-01-13 | 1967-01-24 | American Cyanamid Co | Alkylenesulfonamides and method of preparing same |
| US3336383A (en) * | 1964-07-08 | 1967-08-15 | Aerojet General Co | Nitro-containing sulfonamide compounds |
| US3574740A (en) * | 1968-06-11 | 1971-04-13 | Pennwalt Corp | Method of preparing methane sulfonamide and its derivatives |
| FR2029262A5 (es) * | 1969-01-22 | 1970-10-16 | Ugine Kuhlmann | |
| DE2107914A1 (de) * | 1971-02-19 | 1972-08-31 | Farbenfabriken Bayer Ag, 5090 Leverkusen | N-(Mono- oder Di-amino-phenylalkyl)perfluoralkan-sulfonamide |
| DE2201578A1 (de) * | 1971-03-23 | 1972-10-05 | Eprova Ag | Leicht wasserloesliche,nicht ionische Roentgenkontrastmittel und Verfahren zu ihrer Herstellung |
| US3781441A (en) * | 1972-01-17 | 1973-12-25 | Exxon Research Engineering Co | Use of 4-chloro-3,5-dinitrobenzene-sulfonamide as a fungicide |
| US4260497A (en) * | 1979-11-26 | 1981-04-07 | Colgate-Palmolive Company | Methanesulfonamides as antistatic agents for laundered fabrics |
| GR80986B (en) * | 1983-11-28 | 1985-03-19 | Lilly Co Eli | Improved process for preparing sulfonamides |
| FR2609986B1 (fr) * | 1987-01-23 | 1989-05-05 | Elf Aquitaine | Procede ameliore d'obtention d'alcanes sulfonamides |
-
1988
- 1988-11-30 US US07/277,824 patent/US4970339A/en not_active Expired - Lifetime
-
1989
- 1989-10-31 CA CA002001876A patent/CA2001876A1/en not_active Abandoned
- 1989-11-02 EP EP89120282A patent/EP0371271B1/en not_active Expired - Lifetime
- 1989-11-02 DE DE8989120282T patent/DE68905908T2/de not_active Expired - Fee Related
- 1989-11-29 MX MX018528A patent/MX170640B/es unknown
- 1989-11-29 DK DK601489A patent/DK601489A/da not_active Application Discontinuation
- 1989-11-29 JP JP1310497A patent/JPH02200661A/ja active Pending
- 1989-11-30 BR BR898906056A patent/BR8906056A/pt not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| DK601489D0 (da) | 1989-11-29 |
| EP0371271A1 (en) | 1990-06-06 |
| US4970339A (en) | 1990-11-13 |
| CA2001876A1 (en) | 1990-05-31 |
| DE68905908D1 (de) | 1993-05-13 |
| BR8906056A (pt) | 1990-06-26 |
| DE68905908T2 (de) | 1993-08-19 |
| EP0371271B1 (en) | 1993-04-07 |
| DK601489A (da) | 1990-05-31 |
| JPH02200661A (ja) | 1990-08-08 |
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