MX168168B - Procedimiento para la obtencion de isocianatos - Google Patents

Procedimiento para la obtencion de isocianatos

Info

Publication number
MX168168B
MX168168B MX011415A MX1141588A MX168168B MX 168168 B MX168168 B MX 168168B MX 011415 A MX011415 A MX 011415A MX 1141588 A MX1141588 A MX 1141588A MX 168168 B MX168168 B MX 168168B
Authority
MX
Mexico
Prior art keywords
procedure
isocyanates
phosgene solution
suspension
rotor
Prior art date
Application number
MX011415A
Other languages
English (en)
Inventor
Berthold Keggenhoff
Bernd Weber
Heinz Sauer
Hermann Dallmeyer
Uwe-Jens Zarnack
Original Assignee
Bayer Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Ag filed Critical Bayer Ag
Publication of MX168168B publication Critical patent/MX168168B/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B01F25/451—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by means for moving the materials to be mixed or the mixture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
    • B01F27/2711—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator provided with intermeshing elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80—Mixing plants; Combinations of mixers
    • B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
    • B01F33/811—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1887—Stationary reactors having moving elements inside forming a thin film
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
    • B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
    • B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
    • B29B7/40—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft
    • B29B7/402—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft using a rotor-stator system with intermeshing elements, e.g. teeth
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91—Direction of flow or arrangement of feed and discharge openings
    • B01F2025/912—Radial flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191—Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Windings For Motors And Generators (AREA)

Abstract

La presente invención se refiere a procedimiento para la obtención de isocianatos mediante a) mezclando y reacción de soluciones o bien suspenciones de aminas primarias o bien de sus sales con solución de fosgeno, introduciéndose los productos para indicar la reacción, contínuamente en una zona de mezclado, que presenta al menos un disco de rotor, y el producto previo formado se extrae de nuevo; b) reacción adicional del producto primario formado bajo calentamiento, c) elaboración de la solución de isocianato obtenida para formar las correspondientes isocianatos en bruto y/o puros; el procedimiento está caracterizado porque en la realización de la etapa) la solución de fosgeno se alimenta axialamente con respecto al disco del rotor, y la amina que se encuentra en suspención en la solución de fosgeno pero a una cierta distancia de la misma contra el disco del rotor.
MX011415A 1987-05-21 1988-05-10 Procedimiento para la obtencion de isocianatos MX168168B (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19873717057 DE3717057A1 (de) 1987-05-21 1987-05-21 Verfahren zur herstellung von isocyanaten

Publications (1)

Publication Number Publication Date
MX168168B true MX168168B (es) 1993-05-07

Family

ID=6328049

Family Applications (1)

Application Number Title Priority Date Filing Date
MX011415A MX168168B (es) 1987-05-21 1988-05-10 Procedimiento para la obtencion de isocianatos

Country Status (8)

Country Link
US (1) US4851571A (es)
EP (1) EP0291819B1 (es)
JP (1) JPH0678295B2 (es)
BR (1) BR8802484A (es)
CA (1) CA1305162C (es)
DE (2) DE3717057A1 (es)
ES (1) ES2033364T3 (es)
MX (1) MX168168B (es)

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CA2010224A1 (en) * 1989-02-23 1990-08-23 Teruyuki Nagata Preparation process of xylylene diisocyanate
JPH03133949A (ja) * 1989-10-18 1991-06-07 Mitsui Toatsu Chem Inc イソシアネートの製造方法
DE19638567A1 (de) * 1996-09-20 1998-03-26 Bayer Ag Mischer-Reaktor und Verfahren zur Durchführung von Reaktionen, insbesondere die Phosgenierung von primären Aminen
DE19817691A1 (de) 1998-04-21 1999-10-28 Basf Ag Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl
DE10026142A1 (de) * 2000-05-26 2001-12-13 Basf Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von organischen Mono- oder Polyisocyanaten
DE10032269A1 (de) 2000-07-03 2002-01-31 Basf Ag Verfahren und Vorrichtung zur Verringerung von Nebenprodukten bei der Vermischung von Eduktströmen
WO2003053066A1 (en) 2001-12-17 2003-06-26 Microsoft Corporation Skip macroblock coding
US20040001546A1 (en) 2002-06-03 2004-01-01 Alexandros Tourapis Spatiotemporal prediction for bidirectionally predictive (B) pictures and motion vector prediction for multi-picture reference motion compensation
CA2486551C (en) * 2002-07-01 2012-01-03 University Of Manitoba A sensor system and method for measuring strain in structure
DE10260082A1 (de) 2002-12-19 2004-07-01 Basf Ag Verfahren zur kontinuierlichen Herstellung von Isocyanaten
DE10307141A1 (de) * 2003-02-20 2004-09-02 Bayer Ag Verfahren zur Herstellung von (Poly)isocyanaten in der Gasphase
US9077960B2 (en) 2005-08-12 2015-07-07 Microsoft Corporation Non-zero coefficient block pattern coding
US7547801B2 (en) * 2006-06-26 2009-06-16 Bayer Materialscience Llc Process for the continuous preparation of isocyanates
EP2044009B1 (de) * 2006-07-13 2015-02-25 Basf Se Verfahren zur herstellung von isocyanaten
BRPI0719471B1 (pt) * 2006-12-19 2018-07-03 Dow Global Technologies Inc. Dispositivo para produzir dispersões e método para produzir uma dispersão polimérica, emulsão ou látex
US9205388B2 (en) * 2007-06-27 2015-12-08 H R D Corporation High shear system and method for the production of acids
US8080685B2 (en) * 2007-06-27 2011-12-20 H R D Corporation System and process for production of benzoic acids and phthalic acids
US8034972B2 (en) * 2007-06-27 2011-10-11 H R D Corporation System and process for production of toluene diisocyanate
DE102007054233B4 (de) * 2007-11-12 2010-06-10 Ika-Werke Gmbh & Co. Kg Vorrichtung zum Dispergieren oder Homogenisieren
DE102007061688A1 (de) 2007-12-19 2009-06-25 Bayer Materialscience Ag Verfahren und Mischaggregat zur Herstellung von Isocyanaten durch Phosgenierung primärer Amine
ATE516316T1 (de) 2008-02-13 2011-07-15 Bayer Materialscience Ag Verfahren zur herstellung von polycarbonaten
DE102008012037A1 (de) 2008-03-01 2009-09-03 Bayer Materialscience Ag Verfahren zur Herstellung von Methylen-diphenyl-diisocyanaten
DE102008063728A1 (de) * 2008-12-18 2010-06-24 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
US20110228630A1 (en) * 2010-03-16 2011-09-22 Dow Global Technologies, Inc. Reduced Transit Static Mixer Configuration
US20110230679A1 (en) * 2010-03-16 2011-09-22 Dow Global Technologies, Inc. Reactive Static Mixer
CN101947427A (zh) * 2010-08-24 2011-01-19 天津大学 一种带有进料分布装置的高剪切反应器
US9138717B2 (en) * 2010-12-29 2015-09-22 Wanhua Chemical Group Co., Ltd High-speed mixing reactor and application thereof
SE536456C2 (sv) * 2011-12-15 2013-11-12 Metso Paper Sweden Ab Blandningsenhet innefattande åtminstone två rotorkroppar föranvändning i en blandningsanordning och en blandningsanordning
JP6113824B2 (ja) 2012-03-19 2017-04-12 バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングＢａｙｅｒ Ｉｎｔｅｌｌｅｃｔｕａｌ Ｐｒｏｐｅｒｔｙ ＧｍｂＨ イソシアネートの製造方法
CN108147980B (zh) * 2012-09-24 2020-10-23 科思创德国股份有限公司 通过二胺悬浮体的光气化制备二异氰酸酯的方法
CN103752386A (zh) * 2013-07-05 2014-04-30 嘉兴市禾新科技创业投资有限公司 液体磨
DE202013009790U1 (de) * 2013-12-04 2015-03-05 Mühlbauer Technology Gmbh Dynamischer Mischer
CN105854776B (zh) * 2016-06-07 2018-06-05 上海弗鲁克科技发展有限公司 一种用于快速竞争反应的高剪切反应器
CN105879817A (zh) * 2016-06-16 2016-08-24 无锡市翱宇特新科技发展有限公司 一种多轴搅拌反应釜
KR102596786B1 (ko) 2016-12-21 2023-11-02 코베스트로 도이칠란트 아게 이소시아네이트를 제조하는 방법
CN109718725B (zh) * 2017-10-31 2022-02-08 中国石油化工股份有限公司 连续制胶机、连续制胶方法及连续制备催化剂胶体的方法和系统
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JPS61268344A (ja) * 1985-01-22 1986-11-27 Funken:Kk 微粉炭、オイルコ−クス等の粉体をスラリ−化するための連続混練方法及びその装置

Also Published As

Publication number Publication date
EP0291819B1 (de) 1992-07-08
DE3717057A1 (de) 1988-12-01
EP0291819A2 (de) 1988-11-23
EP0291819A3 (de) 1991-01-16
JPS63303961A (ja) 1988-12-12
ES2033364T3 (es) 1993-03-16
CA1305162C (en) 1992-07-14
DE3872594D1 (de) 1992-08-13
JPH0678295B2 (ja) 1994-10-05
DE3717057C2 (es) 1989-11-02
US4851571A (en) 1989-07-25
BR8802484A (pt) 1988-12-20

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