KR970042364A - 정합가능하고 열처리 가능하고 내구적이고 아이알(ir) 반사률 스퍼터로 코팅된 유리 및 이의 제조방법 - Google Patents
정합가능하고 열처리 가능하고 내구적이고 아이알(ir) 반사률 스퍼터로 코팅된 유리 및 이의 제조방법 Download PDFInfo
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- KR970042364A KR970042364A KR1019960065628A KR19960065628A KR970042364A KR 970042364 A KR970042364 A KR 970042364A KR 1019960065628 A KR1019960065628 A KR 1019960065628A KR 19960065628 A KR19960065628 A KR 19960065628A KR 970042364 A KR970042364 A KR 970042364A
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- 239000011521 glass Substances 0.000 title claims abstract 56
- 238000000034 method Methods 0.000 title claims 7
- 238000004519 manufacturing process Methods 0.000 title claims 2
- 238000010438 heat treatment Methods 0.000 claims abstract 19
- 229910052581 Si3N4 Inorganic materials 0.000 claims abstract 5
- 239000011248 coating agent Substances 0.000 claims abstract 5
- 238000000576 coating method Methods 0.000 claims abstract 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract 4
- 229910000990 Ni alloy Inorganic materials 0.000 claims abstract 2
- 229910052759 nickel Inorganic materials 0.000 claims abstract 2
- 239000000463 material Substances 0.000 claims 36
- 239000000758 substrate Substances 0.000 claims 19
- 238000002834 transmittance Methods 0.000 claims 7
- 238000002310 reflectometry Methods 0.000 claims 5
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 claims 4
- 238000005452 bending Methods 0.000 claims 3
- 238000004544 sputter deposition Methods 0.000 claims 3
- 238000005496 tempering Methods 0.000 claims 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 2
- 229910052804 chromium Inorganic materials 0.000 claims 2
- 239000011651 chromium Substances 0.000 claims 2
- 229910001120 nichrome Inorganic materials 0.000 claims 2
- 238000007747 plating Methods 0.000 claims 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical group [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 230000005540 biological transmission Effects 0.000 claims 1
- 239000007799 cork Substances 0.000 claims 1
- 239000003063 flame retardant Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 239000012466 permeate Substances 0.000 claims 1
- 229910052709 silver Inorganic materials 0.000 claims 1
- 239000004332 silver Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 238000010276 construction Methods 0.000 abstract 1
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Abstract
스퍼터로 코팅된 층구조는 필요한 두께의 Si3N4의 두개의 층 사이에 위치한 비질화 및 비산화된 니켈 또는 니켈합금을 포함하고, 열처리를 위해 건축 및 자동차유리에 이용되고 △E 특성이 열처리되지 않은 제품과 같은 코팅을 열처리된 제품 사이로 일치하도록 매우 낮다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (21)
- 유리기판에 스퍼터로 코팅된 층구로를 포함하는 유리재료는 바깥으로 부터, (3) 실리콘질화물로 된 하부 도금층과; (b) 니켈 또는 니켈합금을 포함하는 금속층과; (c) 실리콘질화물로 구성된 상부도금 층을 구비하고, 상기 층들은 유리기판이 두께가 약 1.5mm-l3mm 이고 상기 층구조를 가질때 열처리시 층이 생긴 유리재료가 유리측 반사률 (△EH) 이약 2.0 보다 크기 않도록 두께가 충분한 유리재료
- 제1항에 있어서, 상기 층구조는 실버가 없는 유리재료
- 제1항에 있어서, 층 (a)는 두께가 5-7OÅ 이고, 층 (b)는 두께가 30-15OÅ 이고, 층 (c)는 두께가 200-500Å인 유리 재료
- 제3항에 있어서, 열처리시 층이 생긴 유리재료는 피막측 반사률 (△EH) 가 5.0 보다 크지 않고 가시투과률 (△EH) 가 약 5.0 보다 크지 않고 열처리 전후해서TY 약 1% - 80%, RGY 약 4% - 55% RfY 약 4% - 65%, Eh 약 0.1-0.75, Eh 약 0.1-0.75, Rs 약 20 -500 ohms/sq 의 특성을 지닌 유리재료
- 제3항에 있어서, 층 (a)는 두께가 30-5OÅ 이고, 층 (b)는 두께가 50-lOOÅ 이고, 층 (c)는 두께가 300-400Å인 유리재료는 열처리전후, TY가 70% 이하이고, RGY가 약 5% - 45%이고, RfY 약 5% - 45%이고, 가시색채 ah가 약 0±2 이고, bh가 약 -4±4 이고, En이 약 0.2-0.75 이고, Eh가 약 0.2-0.75이고, Rs가 약 20 -300 ohms/sq 의 특성을 지닌 유리재료
- 제5항에 있어서, 상기 재료는 내구적 및 화학적 방염제이고, 층 (b)는 어떠한 산화물도 없는 유리재료
- 제5항에 있어서 상기 열처리는 탬퍼링이고 층(b)는 어떠한 산화물도 없는 유리재료
- 제1항에 있어서, 층 (a)는 두께가 약 40Å 이고, 층 (b)는 두께가 75Å 이고, 크롬에 대한 비질산 및 비산화된 니크롬의 질량비가 약 80 : 20 이고, 층 (c)는 두께가 350Å이고, 탬퍼링 전후 상기 유리재료는 TY가 약 50%, RGY가 약 13%, RfY가 약 10% - 11%이고, 유리측 반사를 △Eh 가 약 1.5 이하이고, 피막측 반사률 △Eh가 약 4.0 이하이고, 가사투과를 △Eh가 약 4.0 이하인 유리재료
- 제8항에 있어서, 상기 유리측 반사를 (△EH) 는 약 0.5 이하이고, 상기 피막측 반사률 (△EH) 는 약 2.0이하이고, 상기 가시투과를 (△EH) 는 약 1.0 이하이고, 상기 유리재료는 내구적 이고 화학적으로 내성이 있는 유리 재료
- 제1항에 있어서, 층 (a)는 두께가 40Å 이고, 층 (b)는 두께가 140Å 이고, 크롬에 대한 비질화 및 비산화된 니크롬의 질량비가 약 80 : 20 이고, 층 (c)는 두께가 350Å이고, 탬퍼링 전후 상기 유리재료는 TY가 약 30%, RGY가 약 20% - 21%, RfY가 약 16%의 특성을 나타내고, 유리측 반사를 △En 가 약 2.0 이하이고, 피막측 반사를 △EH가 약 4.0 이하이고, 가시투과률이 약 3.0 이하이고, 상기 유리재료는 내구적 및 화학적으로 내성인 유리재료
- 제5항, 제8항 또는 제10항중 어느 한항에 있어서, 실리콘 질화물은 질량이 최대 6%인 알루미늄을 함유하고, 상기 층구조는 상기 층 (a), (b), 및 (c)로 구성되는 상기 층구조는 내구적 및 화학적으로 내성인 유리재료
- (a) 유리기판에 제1항에 따른 층구조를 스퍼터-코팅하는 단계와; (b) 벤딩, 탬퍼링, 열강화 및 이의 결합을 구성하는 그룹으로 부터 선택된 열처리를 상기 코팅된 유리기판에 하는 단계를 포함하고, 상기 열처리후, 이 유리재료가 유리측 반사를 (△EH) 이 약 2.0 이하인 코팅된 유리재료를 열처리하는 방법
- 제12항에 있어서, 상기 열처리는 유리재료에 약 1200°F 이상의 주변온도를 가하고, 상기 유리재료를 탬퍼하기 위한 소정의 시간주기동안 상기 유리재료를 감금질하므로써 상기 유리를 탬퍼링하는 단계를 포함하는 코팅된 유리재료를 열처리하는 방법
- (a) 유리기판에 제3항을 따른 층구조를 스퍼터로 코팅하는 단계와; (b) 벤딩, 탬퍼링, 열강화 및 이의 결합으로 구성된 그룹으로 부터 선택된 열처리를 상기 코팅된 유리기판에 가하는 단계를 포함하고, 상기 열처리 후 상기 유리재료는 유리측 반사를 (△EH) 이 약 2.0 이하고, 퍼막측 반사를 (△EH) 이 약 5.0 이하이고, 열처리전후 TY는 약 1% -80%, RGY는 약 4% -55%, RfY는 약 4% -65%, En는 약 0.1-0.75,5는 약 0.1-0.75, Rs 약 20 - 500 ohms/sq 인 코팅된 유리재료를 열처리하는 방법
- 제14항에 있어서, 상기 스퍼터 코팅단계는 두께가 약 30-5OÅ 으로 층 (a)을 불이는 단계와, 두께가 약 50-110Å으로 층 (b)를 붙이는 단계와, 두께가 300-400Å 으로 층 (c)을 붙이는 단계를 포함하고, 열처리전후, TY가 70% 이하이고, RGY는 약 5% - 45%이고, RfY는 약 5% - 45%이고, 가시색채 ah가 약 0±2 이고, bh가 약 -4±4 이고, En는 약 0.2-0.75 이고, Eh는 약 0.2-0.75이고, Rs는 약 20 - 300 ohns/sq 열처리 전후, 상기유리재료는 내구 및 화학적으로 내성인 코팅된 유리재료를 열처리하는 방법
- 제15항에 있어서, 상기 층(b)은 약 75Å 두께로 붙여지고, 열처리 전후 유리재료는 TY가 약 50%, 가시투과률 △EH 가 약 50% 이하, 및 유리측 반사률 (△EH) 이 약 0.5이하인 방법
- 제15항에 있어서, 상기 층(b)은 약 140Å 으로 붙여지고, 열처리 전후 유리재료는 TY가 약 30%, 가시투과률 (△EH) 이 약 3.0 이하인 방법
- 동일한 유리측 모양을 하도록 열처리가 되지 않은 스퍼터로 코팅된 유리재료와 미학적으로 일치하는 열처리된 스퍼터로 코팅된 유리재료를 만드는 방법은, (a) 두개 이상의 유리기판의 각각에 청구항 1을 따른 층구조를 스퍼터 코틱하는 단계와; (b) 벤딩, 탬퍼링, 열강하 및 이의 결합을 구성하는 군으로 부터 선택된 열처리를 하나 이상의 상기 스퍼터로 코팅기판에 가하는 단계를 포함하므로써, 열처리후, 하나 이상의 상기 기판이 상기 반사률 (△EH) 이 상기 열처리되지 않은 기판에 비해 약 2.0 보다 크지 않고, 이렇게 형성된 상기 열처리된 스퍼터로 코팅된 기판은 상기 열처리되지 않은 스퍼터로 코팅된 기판과 같은 유리측 모양을 하는 열처리 된 스퍼터로 코팅된 유리재료를 만드는 방법
- 제18항에 있어서, 상기 열처리전후 상기 유리기판은, TY가 70% 이하이고, RGY가 약 5% - 45%이고, RfY가 약 5% - 45%이고, 가시색채 ah가 약 0±2 이고, bh가 약 -4±4 이고, En이 약 0.2-0.75 이고, Eh가 약 0.2-0.75이고, Rs가 약 20 - 300 ohma/sq 의 특성을 하고, 열처리후, 상기 열처리된 기판은 상기 열처리되지 않은 기판에 비해, 피막측 반사률 (△EH) 가 약 5.0 보다 크기 않고, 가시투과률 (△EH) 이 약 5.0 보다 크지 않은 방법
- 제18항에 있어서, 상기 열처리전후 상기 유리기판은, TY가 50%, RGY가 약13%, RfY가 약 10% - 11%, 유리특 반사률 (△EH) 가 약 1.5 이하이고, 피막측반사률 (△EH) 가 약 4.0 이하이고, 가시투과률 (△EH) 가 약 4.0 이하이고, 상기 코팅된 유리가판이 내구적이고 화학적으로 내성인 방법
- 제18항에 있어서, 상기 열처리전후 상기 유리기팝은, TY가 30% 이고, RGY가 약20-21% 이고, RfY가 약 16% 이고, 유리특 반사률 (△EH) 가 약 2.0 이하이고, 피막측반사률 (△EH) 가 약 4.0 이하이고, 가시투과률 (△EH) 가 약 3.0 이하이고, 상기 코팅된 유리가판이 내구적 및 화학적으로 내성인 방법
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US08/572,061 | 1995-12-14 | ||
US08/572,061 US5688585A (en) | 1993-08-05 | 1995-12-14 | Matchable, heat treatable, durable, IR-reflecting sputter-coated glasses and method of making same |
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