KR950704451A - 미네랄 오일에 대한 표지 시약으로서의 아닐린(anilines as marking agents for mineral oils) - Google Patents

미네랄 오일에 대한 표지 시약으로서의 아닐린(anilines as marking agents for mineral oils) Download PDF

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KR950704451A
KR950704451A KR1019950702020A KR19950702020A KR950704451A KR 950704451 A KR950704451 A KR 950704451A KR 1019950702020 A KR1019950702020 A KR 1019950702020A KR 19950702020 A KR19950702020 A KR 19950702020A KR 950704451 A KR950704451 A KR 950704451A
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South Korea
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substituted
unsubstituted
alkyl
hydrogen
alkenyl
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KR1019950702020A
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KR100278235B1 (ko
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딜리크-브렌찡거 라이네르
라울프스 프리드리히-빌헬름
쉴로쎄르 울리케
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비베르바흐, 방에르트
바스프 악티엔게젤샤프트
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Abstract

하기 일반식(I)의 아닐린은 미네랄 오일의 마커로서 사용되며, 상기 아닐린은 미네랄 오닐 내에서 검출된다.
상기 식에서, R1및 R2는 서로 독립적으로 수소원자, 치환되거나 치환되지 않고 각 작용기에 1 내지 3개의 산소원자 또는 알킬아미노로 차단된 알킬 치환되거나 치환되지 않은 페닐이거나, 또는 R1및 R2가 질소원자와 함께 다른 헤테로 원자를 더 포함할 수 있는 5원 또는 6원 포화 헤테로시클릭 라디칼이거나, R1이 치환되지 않거나 치환된 수소이거나 치환되지 않거나 치환된 아미노이며, R3및 R7는 서로 독립적으로 수소, 치환되거나 치환되지 않은 알킬, 알케닐, 시아노, 니트로, 포르밀, 치환되거나 치환되지 않은 C2-C4-알칼오일, 포르밀 아미노, 치환되거나 치환되지 않은 C2-C4-알카노일아미노, 벤조일아미노이거나, R2와 함께 치환되지 않거나 메틸기로 일치환 내지 삼치환된 알킬렌이거나 또는 치환되지 않거나 페닐-치환된 알케닐렌이며, R4는 수소, 치환되거나 치환되지 않은 알킬, 알케닐, 시아노, 니트로이며, R5및 R6는 각각 수소, 치환되거나 치환된지 않은 알킬, 알케닐, 치환되거나 치환되지 않은 페닐, 니트로, 아실아미노, 치환되거나 치환되지 않은 히드록실, 치환되거나 치환되지 않은 술파모일, 알킬-, 알케닐- 또는 아릴술포닐, 아실 또는 치환되거나 치환되지 않은 카르복실이며, 라디칼 R3, R5또는 R7중 적어도 하나가 수소이다.

Description

미네랄 오일에 대한 표지 시약으로서의 아닐린(ANILINES AS MARKING AGENTS FOR MINERAL OILS)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. 미네랄 오일을 마크하기 위하여, 마커로서, 하기 일반식(I)의 아닐린을 사용하는 방법.
    상기식에서, R1및 R2는 서로 독립적으로 수소원자, 치환되거나 치환되지 않고 각 작용기에 1 내지 3개의 산소원자 또는 C1-C4-알킬아미노로 차단된 C3-C18-알킬 또는 치환되거나 치환되지 않은 페닐이거나, 또는 R1및 R2가 질소원자와 함께 다른 헤테로 원자를 더 포함할 수 있는 5원 또는 6원 포화 헤테로시클릭 라디칼이거나, 또는 일반식 OL1또는 NL1L2의 라디칼로서, L1및 L2는 서로 독립적으로 수소, 치환되거나 치환되지 않은 C1-C18-알킬, C3-C18-알케닐 또는 치환되거나 치환되지 않은 페닐이며, R3및 R7는 서로 독립적으로 수소, 치환되거나 치환되지 않은 C1-C18-알킬, C2-C18-알케닐, 시아노, 니트로, 포르밀, 치환되거나 치환되지 않은 C2-C18-알케닐, 시아노, 니트로, 포르밀, 치환되거나 치환되지 않은 C2-C4-알칸오일아미노, 벤조일아미노이거나 또는 일반식 OL1, CH2COOL1, NL1L2, SL1또는 SO2NL1L2로서, L1및 L2가 각각 상기의 의미를 가지거나 R2와 함께 치환되지 않거나 메틸기로 일치환 내지 삼치환되는 C2- 또는 C3-알킬렌이거나 또는 치환되지 않거나 페닐-치환된 C2-또는 C3-알킬렌이며, R4는 수소, 치환되거나 치환되지 않은 C1-C18-알킬, C2-C18-알케닐, 시아노, 니트로, 또는 일반식 OL1, NL1L2, COOL1또는 SO2NL1L2의 라디칼이며, L1및 L2는 각각 상기한 바와 같으며, R5및 R6는 각 수소, 치환되거나 치환되지 않은 C1-C18알킬, C2-C18-알케닐, 치환되거나 치환되지 않은 페닐, 니트로, 포르밀아미노, 치환되거나 치환되지 않은 C2-C4-알카노일아미노, 벤조일아미노 또는 일반식 OL1, NL1L2, SO2NL1L2, SO2L3, COL1또는 COOL1의 라디칼로서, L1및 L2가 각각 상기와 같으며, L3는 치환되거나 치환되지 않은 C1-C18알킬, C2-C18-알케닐 또는 치환되지 않거나 치환된 페닐이며, 라디칼 R3, R5, 또는 R7중 적어도 하나가 수소이다.
  2. 제1항에 있어서, R1및 R2가 서로 독립적으로 수소원자, 치환되거나 치환되지 않고 각 작용기에 1 내지 3개의 산소원자 또는 C1-C4-알킬아미노로 차단된 C3-C18-알킬 또는 치환되거나 치환되지 않은 페닐이거나, 또는 R1및 R2가 질소원자와 함께 다른 헤테로 원자를 더 포함할 수 있는 5원 또는 6원 포화 헤테로시클릭 라디칼이며, R3및 R7는 서로 독립적으로 수소, C1-C4-알콕시이거나 또는 R2와 함께 메틸에 의해 일치환 내지 삼치환되는 1,3-프로필렌이며, R4및 R5는 1, 각각 수소이며, R6는 수소, C1-C4-알킬, C1-C4-알콕시, C1-C4-알카노일-아미노 또는 벤조일아미노인 것을 특징으로 하는 사용방법.
  3. 제1항에 있어서, R1및 R2각각 수소 또는 C1-C4알킬기이거나 또는 라디칼 R1및 R2중 최소한 하나가 수산기로 치환되고 C2-C15-알킬이며, 1 내지 3개의 C3-C4-알킬 아미노기 또는 에테르 작용기내에 1 내지 3개의 산소원자로 차단되는 C2-C15-알킬기인 것을 특징으로 하는 사용방법.
  4. 제1항에 따른 일반식(I)의 하나 이상 아닐린을 포함하는 미네랄 오일.
  5. 일반식(I)의 아닐린이 수성 매질에 의해 미네랄 오일을 처리하여 추출하고 버퍼 용액의 존재 또는 부재하에서 수성상에서 아미노아크라퀴논, 아미노파프탈렌, 아닐린, 아미노티오펜, 아미노티아졸 또는 아미노벤조이소티아졸류로 부터의 아민으로 부터 유도된 디아조늄염과 결합시켜, 아조염료를 형성하면서 추출하는 것을 특징으로 하는 미네날 오일에서 제1항에 따른 일반식(I)의 아닐린의 존재를 검출하는 방법.
  6. 제5항에 있어서, 일반식(I)의 아닐린이 디아조늄염의 산성 수용액으로 미네랄 오일을 처리하여 추출하며, 버퍼의 존재 또는 부재하에서 디아조늄염과 결합시켜, 아조 염료를 형성하면서 추출되는 것을 특징으로 하는 방법.
  7. 제5항에 있어서, 일반식(I)의 아닐린의 수용액으로 미네랄 오일을 처리하여 추출하며, 버퍼의 존재 또는 부재하에 수성상에서 기질에 고체 상태로 존재하는 디아조늄염과 결합하는 것을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019950702020A 1992-11-19 1993-11-09 광유용 표지물질로서의 아닐린 KR100278235B1 (ko)

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