KR940009169A - 수성 혼합물로부터 트리옥산을 분리하는 방법 - Google Patents

수성 혼합물로부터 트리옥산을 분리하는 방법 Download PDF

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Publication number
KR940009169A
KR940009169A KR1019930022685A KR930022685A KR940009169A KR 940009169 A KR940009169 A KR 940009169A KR 1019930022685 A KR1019930022685 A KR 1019930022685A KR 930022685 A KR930022685 A KR 930022685A KR 940009169 A KR940009169 A KR 940009169A
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KR
South Korea
Prior art keywords
trioxane
water
mixture
aqueous mixture
separate
Prior art date
Application number
KR1019930022685A
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English (en)
Inventor
아르놀트 디터
Original Assignee
엥엘하르트, 루츠
훽스트 아크티엔게젤샤프트
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 엥엘하르트, 루츠, 훽스트 아크티엔게젤샤프트 filed Critical 엥엘하르트, 루츠
Publication of KR940009169A publication Critical patent/KR940009169A/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D323/00—Heterocyclic compounds containing more than two oxygen atoms as the only ring hetero atoms
    • C07D323/04—Six-membered rings
    • C07D323/06—Trioxane

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)

Abstract

본 발명은 과증발시켜 트리옥산, 물 및 포름알데히드의 혼합물로부터 물을 추출하고, 정류시켜 물이 감손된 혼합물(보유액)을 트리옥산과 트리옥산, 물 및 포름알데히드의 공비 혼합물로 분리시킴을 특징으로 하는 트리옥산의 분리 방법에 관한 것이다.

Description

수성 혼합물로부터 트리옥산을 분리하는 방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명의 실시양태의 실례를 도시한 것이다.

Claims (2)

  1. 과증발시켜 혼합물로부터 물을 추출하고, 정류시켜 물이 감손된 혼합물(보유액)을 트리옥산과 트리옥산, 물 및 포름알데히드의 공비 혼합물로 분리시킴을 특징으로 하여, 본질적으로 트리옥산, 물 및 포름알데히드로 이루어진 수성 혼합물로부터 트리옥산을 분리하는 방법.
  2. 제1항에 있어서, 과증발이 폴리비닐 알콜의 막을 사용하여 70내지 120℃의 온도 및 보유액 측에서 1 내지 3bar이고 투과액 측에서 30내지 150mbar인 압력에서 수행되는 방법.
    ※참고사항:최초출원 내용에 의하여 공개하는 것임.
KR1019930022685A 1992-10-31 1993-10-29 수성 혼합물로부터 트리옥산을 분리하는 방법 KR940009169A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE4236853 1992-10-31
DEP4236853.7 1992-10-31

Publications (1)

Publication Number Publication Date
KR940009169A true KR940009169A (ko) 1994-05-20

Family

ID=6471835

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019930022685A KR940009169A (ko) 1992-10-31 1993-10-29 수성 혼합물로부터 트리옥산을 분리하는 방법

Country Status (7)

Country Link
US (1) US5523419A (ko)
EP (1) EP0596381B1 (ko)
JP (1) JPH06199830A (ko)
KR (1) KR940009169A (ko)
DE (1) DE59309737D1 (ko)
SG (1) SG49998A1 (ko)
TW (1) TW294604B (ko)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19526307A1 (de) * 1995-07-19 1997-01-23 Hoechst Ag Verfahren zur Abtrennung von Trioxan aus einem wäßrigen Gemisch
DE19732291A1 (de) * 1997-07-26 1999-01-28 Basf Ag Verfahren zur Abtrennung von Trioxan
JP3978301B2 (ja) * 1999-09-30 2007-09-19 矢崎総業株式会社 高強度軽量導体、撚線圧縮導体
DE10309832B4 (de) * 2002-03-07 2007-02-15 Gkss-Forschungszentrum Geesthacht Gmbh Verfahren und Vorrichtung zur Gewinnung eines Mediums aus einem Rohmedium
DE10361516A1 (de) * 2003-12-23 2005-07-28 Basf Ag Verfahren zur Abtrennung von Trioxan aus einem Trioxan/Formaldehyd/Wasser-Gemisch mittels Druckwechsel-Rektifikation
DE102004049055A1 (de) * 2004-10-08 2006-04-13 Ticona Gmbh Verfahren zur Herstellung und Reinigung von zyklischen Formalen
DE102004049056A1 (de) * 2004-10-08 2006-04-13 Ticona Gmbh Verfahren zur Herstellung und Reinigung von zyklischen Formalen
JP5349330B2 (ja) * 2007-01-25 2013-11-20 ビーエーエスエフ ソシエタス・ヨーロピア 圧力スイング精留を用いるトリオキサン／ホルムアルデヒド／水−混合物からのトリオキサンの分離方法
JP6440156B2 (ja) 2014-07-29 2018-12-19 オルガノ株式会社 有機溶剤精製システム及び方法
CN108329294A (zh) * 2018-04-10 2018-07-27 中国科学院成都有机化学有限公司 甲醛制备三聚甲醛的耦合方法
CN111978288B (zh) * 2020-10-14 2021-02-23 中化学科学技术研究有限公司 一种三聚甲醛的制备工艺及装置

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4043873A (en) * 1973-06-15 1977-08-23 Societa' Italiana Resine S.I.R. S.P.A. Plural stage recovery of trioxane in a process having a molecular distillation step
JPS57179182A (en) * 1981-04-27 1982-11-04 Asahi Chem Ind Co Ltd Recovering method of trioxane
DE3328126A1 (de) * 1983-08-04 1985-02-21 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von trioxan aus waessrigen, handelsueblichen formaldehydloesungen
US5061349A (en) * 1988-12-20 1991-10-29 Kueppenbender Herbert Method of isolating trioxane from aqueous trioxane solutions by distillative separation

Also Published As

Publication number Publication date
JPH06199830A (ja) 1994-07-19
EP0596381B1 (de) 1999-08-18
EP0596381A1 (de) 1994-05-11
DE59309737D1 (de) 1999-09-23
SG49998A1 (en) 1998-06-15
US5523419A (en) 1996-06-04
TW294604B (ko) 1997-01-01

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