KR920011934A - 중공 유리 소구체의 제조방법 - Google Patents

중공 유리 소구체의 제조방법 Download PDF

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Publication number
KR920011934A
KR920011934A KR1019910017998A KR910017998A KR920011934A KR 920011934 A KR920011934 A KR 920011934A KR 1019910017998 A KR1019910017998 A KR 1019910017998A KR 910017998 A KR910017998 A KR 910017998A KR 920011934 A KR920011934 A KR 920011934A
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KR
South Korea
Prior art keywords
dispersion
solution
surfactant
heating
concentration
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KR1019910017998A
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English (en)
Inventor
블록 제이콥
조세프 테시어 노엘
조세프 콜라게오 안토니
Original Assignee
스티븐 티. 트링거
더블유, 알. 그레이스 앤드 컴패니-콘
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by 스티븐 티. 트링거, 더블유, 알. 그레이스 앤드 컴패니-콘 filed Critical 스티븐 티. 트링거
Publication of KR920011934A publication Critical patent/KR920011934A/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
    • C03C11/002—Hollow glass particles
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/10—Forming beads
    • C03B19/1005—Forming solid beads
    • C03B19/106—Forming solid beads by chemical vapour deposition; by liquid phase reaction
    • C03B19/1065—Forming solid beads by chemical vapour deposition; by liquid phase reaction by liquid phase reactions, e.g. by means of a gel phase

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Glass Compositions (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Silicon Compounds (AREA)

Abstract

내용 없음

Description

중공 유리 소구체의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (20)

  1. a)ⅰ)계면활성제, ⅱ)유리를 제조하는데 필요한 성분 한 개 이상, 및 ⅲ)가열시 가스를 생성시킬 수 있는 화합물을 혼합하여 용액 또는 분산액을 형성시키고; b)계면활성제 함유 용액 또는 분산액으로부터 미적을 형성시키며; c)미적을 가열하여 중공 유리구를 제조하고; 또 d)중공 유리구를 냉각 및 회수하는 단계를 포함하는, 중공 유리구를 제조하는 방법.
  2. 제1항에 있어서, 용액 또는 분산액을 분무함으로써 미적을 형성시키는 방법.
  3. 제2항에 있어서, 가열하기 전에 계면활성제 함유 용액 또는 분산액을 분무 건조시키는 방법.
  4. 제1항에 있어서, 계면활성제가 비이온성 계면활성제인 방법.
  5. 제4항에 있어서, 계면활성제가 플루오르화탄소 계면활성제인 방법.
  6. 제1항에 있어서, 계면활성제 농도가 전체 용액 또는 분산액에 대해 약 0.05내지 5중량%인 방법.
  7. 제6항에 있어서, 계면활성제 농도가 전체 용액 또는 분산액에 대해 약 0.1 내지 3중량%인 방법.
  8. 제1항에 있어서, 상기 유리를 제조하는데 필요한 상기 성분이 실리카 원, 한 개 이상의 금속 양이온, 및 붕소함유 화합물을 포함하는 방법.
  9. 제8항에 있어서, 실리카 원이 규산나트륨, 콜로이드형 실리카 분말, 실리카 졸, 및 이들의 혼합물로부터 선정되는 방법.
  10. 제8항에 있어서, 금속 양이온이 알칼리금속 또는 알칼리토금속 및 알루미늄으로부터 선정되는 방법.
  11. 제8항에 있어서, 붕소 화합물이 붕산, 붕산염 및 이들의 혼합물로부터 선정되는 방법.
  12. 제9항에 있어서, 실리카 농도가 용액 또는 분산액의 총 고형분에 대해 약 40 내지 90중량%인 방법.
  13. 제1항에 있어서, 가스 발생 화합물이 우레아인 방법.
  14. 제13항에 있어서, 우레아 농도가 용액 또는 분산액의 총 고형분에 대해 약 0.2 내지 20중량%인 방법.
  15. 제14항에 있어서, 우레아 농도가 용액 또는 분산액의 총 고형분에 대해 약 0.4 내지 12중량%인 방법.
  16. 제1항에 있어서, 약 800 내지 1700℃에서 가열하는 방법.
  17. 제16항에 있어서, 상기 온도가 약 1000내지 1500℃인 방법.
  18. 제17항에 있어서, 약 0.1내지 5초간 가열하는 방법.
  19. 제18항에 있어서, 약 0.5 내지 2초간 가열하는 방법.
  20. 제2항에 있어서, 노즐을 통해 용액 또는 분산액을 분하여 상기 미적을 형성시키는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019910017998A 1990-12-20 1991-10-10 중공 유리 소구체의 제조방법 KR920011934A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US632,199 1990-12-20
US07/632,199 US5069702A (en) 1990-12-20 1990-12-20 Method of making small hollow glass spheres

Publications (1)

Publication Number Publication Date
KR920011934A true KR920011934A (ko) 1992-07-25

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Family Applications (1)

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KR1019910017998A KR920011934A (ko) 1990-12-20 1991-10-10 중공 유리 소구체의 제조방법

Country Status (12)

Country Link
US (2) US5069702A (ko)
EP (1) EP0493734B1 (ko)
JP (1) JPH04275927A (ko)
KR (1) KR920011934A (ko)
AT (1) ATE120725T1 (ko)
AU (1) AU635187B2 (ko)
CA (1) CA2051837A1 (ko)
DE (1) DE69108703T2 (ko)
DK (1) DK0493734T3 (ko)
ES (1) ES2070408T3 (ko)
HK (1) HK43796A (ko)
MY (1) MY131212A (ko)

Families Citing this family (71)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3021586B2 (ja) * 1990-09-17 2000-03-15 富士通株式会社 低誘電率セラミック基板とグリーンシートの製造方法
JPH0742177B2 (ja) * 1992-11-19 1995-05-10 工業技術院長 中空炭素質球状体の製造方法
ATE186037T1 (de) * 1993-09-08 1999-11-15 Pq Holding Inc Hohle borosilikatmikrokugeln und herstellungsverfahren
KR970702827A (ko) * 1994-04-25 1997-06-10 워렌 리차드 보비 용융 미립자를 포함하는 조성물 및 그 제조방법(compositions comprising fused particulates and methods of making them)
US6045913A (en) * 1995-11-01 2000-04-04 Minnesota Mining And Manufacturing Company At least partly fused particulates and methods of making them by flame fusion
US6254981B1 (en) 1995-11-02 2001-07-03 Minnesota Mining & Manufacturing Company Fused glassy particulates obtained by flame fusion
JP3633091B2 (ja) * 1996-04-09 2005-03-30 旭硝子株式会社 微小無機質球状中実体の製造方法
US6360562B1 (en) 1998-02-24 2002-03-26 Superior Micropowders Llc Methods for producing glass powders
US6000241A (en) * 1998-08-26 1999-12-14 Particle Technology, Inc. Process for making barium containing silicate glass powders
US7456571B1 (en) 2002-05-21 2008-11-25 Imaging Systems Technology Microsphere plasma display
KR19990073271A (ko) * 1999-06-29 1999-10-05 정상옥 실리카구및그제조방법
ATE427751T1 (de) 1999-07-08 2009-04-15 Cap Biotechnology Inc Calcium-enthaltende strukture und verfahren zur herstellung und verwendung davon
US7923930B1 (en) 2000-01-12 2011-04-12 Imaging Systems Technology Plasma-shell device
KR100853920B1 (ko) 2000-03-14 2008-08-25 제임스 하디 인터내셔널 파이낸스 비.브이. 저밀도 첨가제를 포함한 섬유시멘트 건축재료
US8138673B1 (en) 2002-05-21 2012-03-20 Imaging Systems Technology Radiation shielding
US8198812B1 (en) 2002-05-21 2012-06-12 Imaging Systems Technology Gas filled detector shell with dipole antenna
US7405516B1 (en) 2004-04-26 2008-07-29 Imaging Systems Technology Plasma-shell PDP with organic luminescent substance
US8198811B1 (en) 2002-05-21 2012-06-12 Imaging Systems Technology Plasma-Disc PDP
US7932674B1 (en) 2002-05-21 2011-04-26 Imaging Systems Technology Plasma-dome article of manufacture
US7727040B1 (en) 2002-05-21 2010-06-01 Imaging Systems Technology Process for manufacturing plasma-disc PDP
US8513887B1 (en) 2002-05-21 2013-08-20 Imaging Systems Technology, Inc. Plasma-dome article of manufacture
US7455798B2 (en) * 2002-08-23 2008-11-25 James Hardie International Finance B.V. Methods for producing low density products
AU2003250614B2 (en) * 2002-08-23 2010-07-15 James Hardie Technology Limited Synthetic hollow microspheres
MXPA05003691A (es) 2002-10-07 2005-11-17 James Hardie Int Finance Bv Material mixto de fibrocemento de densidad media durable.
CN1805783A (zh) * 2003-05-16 2006-07-19 詹姆士·哈代国际金融公司 生产低密度产品的方法
US20090146108A1 (en) * 2003-08-25 2009-06-11 Amlan Datta Methods and Formulations for Producing Low Density Products
US20050065240A1 (en) * 2003-09-24 2005-03-24 Kyte William J, Grout composition, dispenser therefor, and method of use
US20090156385A1 (en) 2003-10-29 2009-06-18 Giang Biscan Manufacture and use of engineered carbide and nitride composites
US7772773B1 (en) 2003-11-13 2010-08-10 Imaging Systems Technology Electrode configurations for plasma-dome PDP
US8129906B1 (en) 2004-04-26 2012-03-06 Imaging Systems Technology, Inc. Lumino-shells
US8106586B1 (en) 2004-04-26 2012-01-31 Imaging Systems Technology, Inc. Plasma discharge display with fluorescent conversion material
US8339041B1 (en) 2004-04-26 2012-12-25 Imaging Systems Technology, Inc. Plasma-shell gas discharge device with combined organic and inorganic luminescent substances
US8368303B1 (en) 2004-06-21 2013-02-05 Imaging Systems Technology, Inc. Gas discharge device with electrical conductive bonding material
US7604523B1 (en) 2004-06-21 2009-10-20 Imaging Systems Technology Plasma-shell PDP
US8113898B1 (en) 2004-06-21 2012-02-14 Imaging Systems Technology, Inc. Gas discharge device with electrical conductive bonding material
US7998571B2 (en) 2004-07-09 2011-08-16 James Hardie Technology Limited Composite cement article incorporating a powder coating and methods of making same
FR2875494B1 (fr) * 2004-09-17 2007-01-19 Sylvain Rakotoarison Microspheres de silice, procede de fabrication, assemblages et utilisations possibles de ces microspheres de silice
US20060060820A1 (en) * 2004-09-21 2006-03-23 Schumacher Ray F Hollow porous-wall glass microspheres for hydrogen storage
US7666807B2 (en) * 2004-09-21 2010-02-23 Savannah River Nuclear Solutions, Llc Hollow porous-wall glass microspheres for hydrogen storage
US8951608B1 (en) 2004-10-22 2015-02-10 Imaging Systems Technology, Inc. Aqueous manufacturing process and article
US20090151283A1 (en) * 2005-02-15 2009-06-18 James Hardie International Finance B.V. Flooring sheet and modular flooring system
US8299696B1 (en) 2005-02-22 2012-10-30 Imaging Systems Technology Plasma-shell gas discharge device
AU2006216407A1 (en) 2005-02-24 2006-08-31 James Hardie Technology Limited Alkali resistant glass compositions
US7730746B1 (en) 2005-07-14 2010-06-08 Imaging Systems Technology Apparatus to prepare discrete hollow microsphere droplets
WO2007067774A2 (en) 2005-12-08 2007-06-14 James Hardie International Finance B.V. Engineered low-density heterogeneous microparticles and methods and formulations for producing the microparticles
KR20070074344A (ko) * 2006-01-09 2007-07-12 삼성전자주식회사 박막 트랜지스터 기판과 그 제조 방법 및 이를 포함한 액정표시 장치
US7863815B1 (en) 2006-01-26 2011-01-04 Imaging Systems Technology Electrode configurations for plasma-disc PDP
US8618733B1 (en) 2006-01-26 2013-12-31 Imaging Systems Technology, Inc. Electrode configurations for plasma-shell gas discharge device
US7535175B1 (en) 2006-02-16 2009-05-19 Imaging Systems Technology Electrode configurations for plasma-dome PDP
US8278824B1 (en) 2006-02-16 2012-10-02 Imaging Systems Technology, Inc. Gas discharge electrode configurations
US8410695B1 (en) 2006-02-16 2013-04-02 Imaging Systems Technology Gas discharge device incorporating gas-filled plasma-shell and method of manufacturing thereof
US8035303B1 (en) 2006-02-16 2011-10-11 Imaging Systems Technology Electrode configurations for gas discharge device
EP1832560A3 (de) * 2006-03-07 2010-03-24 Omega Minerals Germany GmbH Verfahren zur Herstellung keramischer oder glasartiger Mikrohohlkugeln
US7791037B1 (en) 2006-03-16 2010-09-07 Imaging Systems Technology Plasma-tube radiation detector
KR100869946B1 (ko) 2006-04-06 2008-11-24 삼성전자주식회사 컨텐츠 관리 서버 및 그의 컨텐츠 관리방법
CA2648966C (en) 2006-04-12 2015-01-06 James Hardie International Finance B.V. A surface sealed reinforced building element
US8209927B2 (en) 2007-12-20 2012-07-03 James Hardie Technology Limited Structural fiber cement building materials
US20100139320A1 (en) * 2008-12-04 2010-06-10 Savannah River Nulcear Solutions, Llc Hollow porous-wall glass microspheres and composition and process for controlling pore size and pore volume
US8940364B2 (en) * 2008-12-19 2015-01-27 Xurex, Inc. System, formulation and method for producing ceramic vacuum microspheres
US9013102B1 (en) 2009-05-23 2015-04-21 Imaging Systems Technology, Inc. Radiation detector with tiled substrates
US8302596B1 (en) * 2009-10-22 2012-11-06 Lockheed Martin Corporation Robust glass to metal sealing joint
JP2011116607A (ja) * 2009-12-07 2011-06-16 Kochi Univ ガラス中空体の製造方法およびガラス中空体
US8815408B1 (en) 2009-12-08 2014-08-26 Imaging Systems Technology, Inc. Metal syntactic foam
US20110152057A1 (en) * 2009-12-21 2011-06-23 Gang Qi Hollow microspheres
US20130344337A1 (en) * 2011-03-07 2013-12-26 3M Innovative Properties Company Hollow microspheres
KR101156207B1 (ko) * 2011-08-30 2012-06-18 한스바이오메드 주식회사 인산칼슘 마이크로스피어 약물전달체의 제조방법
KR20160034326A (ko) * 2013-07-18 2016-03-29 쓰리엠 이노베이티브 프로퍼티즈 컴파니 유리 마이크로버블, 원산물, 및 그의 제조 방법
DE102015225766A1 (de) * 2015-12-17 2017-06-22 Dennert Poraver Gmbh Verfahren und Anlage zur Herstellung von Blähglaspartikeln
PT3184494T (pt) * 2015-12-21 2018-05-08 Adf Mat Gmbh Composição química para produção de partículas de vidro esféricas e ocas com alta resistência à compressão
WO2018233449A1 (zh) * 2017-06-21 2018-12-27 中国石油大学(华东) 高强度地聚合物空心微球、其制备方法和相变储能微球
BR112022014385A2 (pt) 2020-01-24 2022-09-20 Basf Se Processo para preparar partículas de vidro esféricas ocas, e, dispositivo de aquecimento

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL232500A (ko) * 1957-10-22
US3061495A (en) * 1959-06-29 1962-10-30 Standard Oil Co Method of acid treating hollow glass spheres
US3365315A (en) * 1963-08-23 1968-01-23 Minnesota Mining & Mfg Glass bubbles prepared by reheating solid glass partiles
US3699050A (en) * 1967-08-02 1972-10-17 Emerson & Cuming Inc Spray dried product for feed in the manufacture of hollow glass spheres and process for forming said spray dried product
GB1568817A (en) * 1975-11-13 1980-06-04 Sovitec Sa Glass-former comp
US4133854A (en) * 1977-06-16 1979-01-09 The United States Of America As Represented By The United States Department Of Energy Method for producing small hollow spheres
US4119422A (en) * 1977-08-18 1978-10-10 Pittsburgh Corning Corporation Pulverulent borosilicate composition and a method of making a cellular borosilicate body therefrom
US4671909A (en) * 1978-09-21 1987-06-09 Torobin Leonard B Method for making hollow porous microspheres
US4257799A (en) * 1979-07-26 1981-03-24 The United States Of America As Represented By The United States Department Of Energy Method for producing small hollow spheres
US4336338A (en) * 1980-08-15 1982-06-22 The United States Of America As Represented By The United States Department Of Energy Hollow microspheres of silica glass and method of manufacture
US4442175A (en) * 1983-01-27 1984-04-10 Corning Glass Works Cellular ceramic bodies and method making same
US4778502A (en) * 1984-06-21 1988-10-18 Saint-Gobain Vitrage Production of glass microspheres
FR2566384B1 (fr) * 1984-06-21 1986-09-05 Saint Gobain Vitrage Perfectionnements aux techniques de production de microspheres en verre
GB8515744D0 (en) * 1985-06-21 1985-07-24 Glaverbel Vitreous beads
US4767726A (en) * 1987-01-12 1988-08-30 Minnesota Mining And Manufacturing Company Glass microbubbles
CA1321048C (en) * 1987-03-05 1993-08-10 Robert W. J. Lencki Microspheres and method of producing same
FR2619101A1 (fr) * 1987-08-05 1989-02-10 Saint Gobain Vitrage Technique de production de microspheres en silice
US4983550A (en) * 1988-08-24 1991-01-08 Potters Industries, Inc. Hollow glass spheres
US5064784A (en) * 1989-04-18 1991-11-12 Tokai Kogyo Co., Ltd. Glass frit useful for the preparation of glass bubbles, and glass bubbles prepared by using it

Also Published As

Publication number Publication date
MY131212A (en) 2007-07-31
ES2070408T3 (es) 1995-06-01
EP0493734A1 (en) 1992-07-08
EP0493734B1 (en) 1995-04-05
ATE120725T1 (de) 1995-04-15
HK43796A (en) 1996-03-22
CA2051837A1 (en) 1992-06-21
US5069702A (en) 1991-12-03
DE69108703T2 (de) 1995-08-17
US5176732A (en) 1993-01-05
DK0493734T3 (da) 1995-06-19
AU8966691A (en) 1992-06-25
JPH04275927A (ja) 1992-10-01
AU635187B2 (en) 1993-03-11
DE69108703D1 (de) 1995-05-11

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