KR910004838B1 - 지르코늄계 과립 및 산화지르코늄 섬유의 제조방법 - Google Patents

지르코늄계 과립 및 산화지르코늄 섬유의 제조방법 Download PDF

Info

Publication number
KR910004838B1
KR910004838B1 KR1019880007359A KR880007359A KR910004838B1 KR 910004838 B1 KR910004838 B1 KR 910004838B1 KR 1019880007359 A KR1019880007359 A KR 1019880007359A KR 880007359 A KR880007359 A KR 880007359A KR 910004838 B1 KR910004838 B1 KR 910004838B1
Authority
KR
South Korea
Prior art keywords
zirconium
solution
phase stabilizer
aqueous solution
granules
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
KR1019880007359A
Other languages
English (en)
Korean (ko)
Other versions
KR890000350A (ko
Inventor
시바파 자다 시바난다
Original Assignee
맨빌 코오퍼레이션
로버트 에이. 보어드맨
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 맨빌 코오퍼레이션, 로버트 에이. 보어드맨 filed Critical 맨빌 코오퍼레이션
Publication of KR890000350A publication Critical patent/KR890000350A/ko
Application granted granted Critical
Publication of KR910004838B1 publication Critical patent/KR910004838B1/ko
Expired legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00Compounds of zirconium
    • C01G25/02Oxides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62227Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
    • C04B35/62231Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
    • C04B35/6225Fibres based on zirconium oxide, e.g. zirconates such as PZT
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/02Amorphous compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/60Compounds characterised by their crystallite size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/10Particle morphology extending in one dimension, e.g. needle-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/50Agglomerated particles
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/10Solid density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Manufacturing & Machinery (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Structural Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Inorganic Fibers (AREA)
  • Glass Compositions (AREA)
KR1019880007359A 1987-06-19 1988-06-18 지르코늄계 과립 및 산화지르코늄 섬유의 제조방법 Expired KR910004838B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US6580987A 1987-06-19 1987-06-19
US065,809 1987-06-19
US131,594 1987-12-11
US131594 1987-12-11
US07/131,594 US4927622A (en) 1987-06-19 1987-12-11 Process for producing zirconium based granules

Publications (2)

Publication Number Publication Date
KR890000350A KR890000350A (ko) 1989-03-14
KR910004838B1 true KR910004838B1 (ko) 1991-07-13

Family

ID=26746021

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019880007359A Expired KR910004838B1 (ko) 1987-06-19 1988-06-18 지르코늄계 과립 및 산화지르코늄 섬유의 제조방법

Country Status (3)

Country Link
US (1) US4927622A (enExample)
JP (1) JPS6461323A (enExample)
KR (1) KR910004838B1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5053214A (en) * 1987-06-19 1991-10-01 Manville Corporation Process for producing zirconium based granules
IT1230731B (it) * 1989-02-17 1991-10-29 Snia Fibre Fibre ceramiche a base di zro2 e sio2 e procedimento per la loro preparazione.
US5037579A (en) * 1990-02-12 1991-08-06 Nalco Chemical Company Hydrothermal process for producing zirconia sol
KR20030048401A (ko) * 2000-09-18 2003-06-19 로스맨즈 벤손 엔드 헤지스 인코퍼레이티드 비-가연성 처리 재료를 사용한 낮은 생담배 연기 궐련
WO2003023096A1 (en) * 2001-09-13 2003-03-20 Rothmans, Benson & Hedges Inc. Zirconium/metal oxide fibres
JP4520745B2 (ja) * 2002-03-15 2010-08-11 ロスマンズ、ベンソン アンド ヘッジズ インコーポレイテッド 改質された灰特性を有する可燃性紙を備えた低副流煙紙巻きタバコ
EP1549160A2 (en) * 2002-09-13 2005-07-06 Rothmans, Benson & Hedges Inc. Ceria/zirconia fibres for use in cigarettes
US20070276017A1 (en) * 2003-06-10 2007-11-29 Chikara Murakata Thiadiazoline Derivative
US7775204B2 (en) * 2007-01-05 2010-08-17 Long Ho Chen Warming shoe pad
JP6238286B2 (ja) * 2013-11-14 2017-11-29 国立研究開発法人物質・材料研究機構 ジルコニア連続繊維とその製造方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1249832B (enExample) * 1960-11-29
US3334962A (en) * 1962-10-08 1967-08-08 Nat Lead Co Process for the production of cubic crystalline zirconia
US4501818A (en) * 1983-07-05 1985-02-26 Norton Company Process for the preparation of ceramic powders
JPS60176920A (ja) * 1984-02-21 1985-09-11 Etsuro Kato ジルコニア系単結晶超微粒子の分散したゾルおよび製造方法
EP0171736B1 (en) * 1984-08-07 1992-05-27 Nippon Shokubai Kagaku Kogyo Co., Ltd Micronized zirconia and method for production thereof
US4619817A (en) * 1985-03-27 1986-10-28 Battelle Memorial Institute Hydrothermal method for producing stabilized zirconia
JPS62132708A (ja) * 1985-12-03 1987-06-16 Nok Corp セラミツクス超微粒子の製造法
US4719091A (en) * 1986-07-01 1988-01-12 Corning Glass Works Preparation of mono-sized zirconia powders by forced hydrolysis
US4769251A (en) * 1987-02-03 1988-09-06 Wenger Manufacturing, Inc. Low shear extrusion process for manufacture of quick cooking rice

Also Published As

Publication number Publication date
US4927622A (en) 1990-05-22
KR890000350A (ko) 1989-03-14
JPH0474289B2 (enExample) 1992-11-25
JPS6461323A (en) 1989-03-08

Similar Documents

Publication Publication Date Title
KR910004838B1 (ko) 지르코늄계 과립 및 산화지르코늄 섬유의 제조방법
US4883779A (en) Ceramic articles containing silicon carbide
Mori et al. Preparation of high‐purity ZrSiO4 powder using sol–gel processing and mechanical properties of the sintered body
US4800180A (en) Ceramic articles containing silicon carbide
CN101498063B (zh) 全稳定立方相氧化锆晶体纤维的制备方法
AU613249B2 (en) Improved zirconium oxide fibers and process for their preparation
CN110592723B (zh) 微纳米氧化锆纤维及其制备方法
Mamana et al. Influence of the synthesis process on the features of Y2O3-stabilized ZrO2 powders obtained by the sol–gel method
KR101074152B1 (ko) 저온에서 pva를 이용한 나노 크기의 이트리아 분말의 합성방법
US4798814A (en) Oxidation resistant alumina-silica articles containing silicon carbide and carbon
US5112781A (en) Process for producing zirconium based granules and zirconium oxide fibers
US4732878A (en) Oxidation resistant carbon containing alumina-silica articles
Kundu et al. Preparation and thermal evolution of sol-gel derived transparent ZrO2 and MgO-ZrO2 gel monolith
KR20040035770A (ko) 지르코늄/금속 산화물 섬유
US5053214A (en) Process for producing zirconium based granules
Sun et al. Fabrication of zirconia fibers by a sol-gel combined rotational centrifugal spinning technique
JP2010505047A (ja) 多結晶コランダム繊維及びその製造方法
Pullar et al. Blow spun strontium zirconate fibres produced from a sol-gel precursor
JPH042608A (ja) ジルコン粉末の合成法
US4931316A (en) Preparation of interstitial titanium ceramic fibers
Lu et al. Synthesis of long ZrTiO 4 fibers by a sol–gel process free of organic components
KR100210959B1 (ko) 소결성이 우수한 y203 분말의 제조방법
CN103757751A (zh) 一种超高温氧化锆陶瓷纤维的制备方法
Song et al. Optimized preparation of MgO-ZrO2 nanocomposite powders by assisted sol-gel method
Park et al. Influence of calcination temperature on phase transformation and grain size of electrospun zirconium oxide fibers

Legal Events

Date Code Title Description
PA0109 Patent application

St.27 status event code: A-0-1-A10-A12-nap-PA0109

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

G160 Decision to publish patent application
PG1605 Publication of application before grant of patent

St.27 status event code: A-2-2-Q10-Q13-nap-PG1605

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U11-oth-PR1002

Fee payment year number: 1

FPAY Annual fee payment

Payment date: 19940701

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 19950714

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 19950714

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000