CN101498063B - 全稳定立方相氧化锆晶体纤维的制备方法 - Google Patents
全稳定立方相氧化锆晶体纤维的制备方法 Download PDFInfo
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- CN101498063B CN101498063B CN2009100137817A CN200910013781A CN101498063B CN 101498063 B CN101498063 B CN 101498063B CN 2009100137817 A CN2009100137817 A CN 2009100137817A CN 200910013781 A CN200910013781 A CN 200910013781A CN 101498063 B CN101498063 B CN 101498063B
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- zirconium
- ethanol
- organic polymer
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- acetylacetone
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- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 claims abstract description 29
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- NGDQQLAVJWUYSF-UHFFFAOYSA-N 4-methyl-2-phenyl-1,3-thiazole-5-sulfonyl chloride Chemical compound S1C(S(Cl)(=O)=O)=C(C)N=C1C1=CC=CC=C1 NGDQQLAVJWUYSF-UHFFFAOYSA-N 0.000 claims description 6
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- NREVZTYRXVBFAQ-UHFFFAOYSA-N propan-2-ol;yttrium Chemical compound [Y].CC(C)O.CC(C)O.CC(C)O NREVZTYRXVBFAQ-UHFFFAOYSA-N 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
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- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 14
- 229910001928 zirconium oxide Inorganic materials 0.000 description 14
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Abstract
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CN2009100137817A CN101498063B (zh) | 2009-01-14 | 2009-01-14 | 全稳定立方相氧化锆晶体纤维的制备方法 |
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CN101498063B true CN101498063B (zh) | 2011-11-23 |
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Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101736439B (zh) * | 2009-12-04 | 2011-12-14 | 济南大学 | 含有磁性或金属纳米晶的形貌可调的纤维 |
CN102465357B (zh) * | 2010-11-19 | 2013-10-02 | 山东鲁阳股份有限公司 | 多晶氧化锆纤维及氧化锆/氧化铝复合纤维的制备方法 |
CN102766154B (zh) * | 2012-07-28 | 2015-04-22 | 山东大学 | 一步溶剂法制备氧化锆纤维生产用有机聚锆前驱体或其甩丝液的方法 |
CN102787393B (zh) * | 2012-08-07 | 2014-05-21 | 山东大学 | 氧化锆晶体纤维制备中聚乙酰丙酮合锆前驱体纤维的压力解析方法、装置及配体回收技术 |
CN102775143A (zh) * | 2012-08-22 | 2012-11-14 | 安徽同和晶体新材料股份有限公司 | 一种全稳定四方相氧化锆晶体纤维的制备方法 |
CN103130271B (zh) * | 2013-01-10 | 2015-03-25 | 浙江大学 | 超低密度块状全稳定氧化锆气凝胶及其制备方法 |
CN103993387B (zh) * | 2014-05-30 | 2016-08-17 | 山东大学 | 一种耐超高温千米级连续氧化锆晶体纤维的制备方法 |
CN103993388B (zh) * | 2014-05-30 | 2016-05-04 | 山东大学 | 一种用于制备高性能氧化锆晶体纤维的高温压力解析技术 |
CN103993389B (zh) * | 2014-05-30 | 2015-11-04 | 山东大学 | 一种醋酸氧锆-甲醇体系制备连续氧化锆晶体纤维的方法 |
CN105369393A (zh) * | 2014-08-12 | 2016-03-02 | 山东宏瑞超高温纤维科技有限公司 | 一种氧化锆陶瓷纤维的制备方法 |
CN105839227B (zh) * | 2016-06-06 | 2018-05-04 | 山东大学 | 一种静电纺丝制备介孔氧化锆纤维的方法 |
CN108301071A (zh) * | 2018-01-17 | 2018-07-20 | 太原理工大学 | 一种碳化锆晶体纤维的制备方法及其制备的碳化锆晶体纤维 |
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