KR910000581A - 불투명한 디치환 퀴나크리돈 화합물의 제조방법 - Google Patents
불투명한 디치환 퀴나크리돈 화합물의 제조방법 Download PDFInfo
- Publication number
- KR910000581A KR910000581A KR1019890008428A KR890008428A KR910000581A KR 910000581 A KR910000581 A KR 910000581A KR 1019890008428 A KR1019890008428 A KR 1019890008428A KR 890008428 A KR890008428 A KR 890008428A KR 910000581 A KR910000581 A KR 910000581A
- Authority
- KR
- South Korea
- Prior art keywords
- compound
- alcohol
- quinacridone
- quinacridone compound
- base
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 13
- -1 disubstituted quinacridone compound Chemical class 0.000 title claims 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 9
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical group [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 6
- 239000002585 base Substances 0.000 claims 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- 150000001875 compounds Chemical class 0.000 claims 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 claims 2
- XPZQBGDNVOHQIS-UHFFFAOYSA-N 2,9-dichloro-5,12-dihydroquinolino[2,3-b]acridine-7,14-dione Chemical compound N1C2=CC=C(Cl)C=C2C(=O)C2=C1C=C(C(=O)C=1C(=CC=C(C=1)Cl)N1)C1=C2 XPZQBGDNVOHQIS-UHFFFAOYSA-N 0.000 claims 1
- TXWSZJSDZKWQAU-UHFFFAOYSA-N 2,9-dimethyl-5,12-dihydroquinolino[2,3-b]acridine-7,14-dione Chemical compound N1C2=CC=C(C)C=C2C(=O)C2=C1C=C(C(=O)C=1C(=CC=C(C=1)C)N1)C1=C2 TXWSZJSDZKWQAU-UHFFFAOYSA-N 0.000 claims 1
- BFEJTCHFLJECJN-UHFFFAOYSA-N 4,11-Dichloro-5,12-dihydroquino[2,3-b]acridine-7,14-dione Chemical compound N1C2=C(Cl)C=CC=C2C(=O)C2=C1C=C(C(C=1C=CC=C(C=1N1)Cl)=O)C1=C2 BFEJTCHFLJECJN-UHFFFAOYSA-N 0.000 claims 1
- NRCMAYZCPIVABH-UHFFFAOYSA-N Quinacridone Chemical class N1C2=CC=CC=C2C(=O)C2=C1C=C1C(=O)C3=CC=CC=C3NC1=C2 NRCMAYZCPIVABH-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 230000001476 alcoholic effect Effects 0.000 claims 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
- 239000000908 ammonium hydroxide Substances 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 150000002334 glycols Chemical class 0.000 claims 1
- 238000003801 milling Methods 0.000 claims 1
- 125000001453 quaternary ammonium group Chemical group 0.000 claims 1
- 125000001424 substituent group Chemical group 0.000 claims 1
- 238000006467 substitution reaction Methods 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B48/00—Quinacridones
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0022—Wet grinding of pigments
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0014—Influencing the physical properties by treatment with a liquid, e.g. solvents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (13)
- 불투명화 유효량의 알코올과 염기의 존재하에서 조 퀴나크리돈 화합물 또는 반안료성 퀴나크리돈 화합물을 분쇄하고 그 결과 생성되는 불투명한 화합물을 단리하는 것을 포함하는, 하기 일반식에 해당하는 불투명한 디치환 퀴나크리돈 화합물의 제조방법.상기식에서, R은 독립적으로 F, Cl, Br, C1-C3알킬 또는 C1-C3알콕시이다.
- 제1항에 있어서, 상기 퀴나크리돈 화합물이, 두 치환기가 동일하고 F, Cl, Br, CH3또는 OCH3인 2,9-디치환된 퀴나크리돈 또는 4,11-디치환된 퀴나크리돈인 방법.
- 제2항에 있어서, 상기 화합물이 2,9-디클로로퀴나크리돈인 방법.
- 제2항에 있어서, 상기 화합물이 2,9-디메틸퀴나크리돈인 방법.
- 제2항에 있어서, 상기 화합물이 4,11-디클로로퀴나크리돈인 방법.
- 제1항에 있어서, 상기 알코올이 저비점 알코올이고 알칸올과 글리콜로부터 선택되는 방법.
- 제6항에 있어서, 상기 알코올이 메탄올, 에탄올, 부탄올, 펜탄올 및 에틸렌 글리콜로부터 선택되는 방법.
- 제7항에 있어서, 상기 알코올이 메탄올인 방법.
- 제1항에 있어서, 상기 염기가 알칼리금속 수산화물 또는 4급 암모늄 수산화물인 방법.
- 제9항에 있어서, 상기 염기가 수산화칼륨 또는 수산화나트륨인 방법.
- 제1항에 있어서, 상기 알코올리 메탄올이고 상기 염기가 수산화칼륨 또는 수산화 나트륨인 방법.
- 제1항에 있어서, 상기 알코올이 상기 퀴나크리돈 화합물 중량의 5 내지 25배의 양으로 존재하고 상기 염기가 상기 알코올의 0.5 내지 10.0중량%인 양으로 존재하는 방법.
- 제1항에 있어서, 상기 반안료성 퀴나크리돈 화합물이 조 퀴나크리돈 화합물의 건조 예비 분쇄 또는 산 페이스트화에 의해 생성되는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/209,255 US4895948A (en) | 1988-06-20 | 1988-06-20 | Process for preparation of opaque quinacridones |
CH209,255 | 1988-06-20 | ||
US209255 | 1998-12-10 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR910000581A true KR910000581A (ko) | 1991-01-29 |
KR970000737B1 KR970000737B1 (ko) | 1997-01-18 |
Family
ID=22778024
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019890008428A KR970000737B1 (ko) | 1988-06-20 | 1989-06-19 | 불투명한 이치환 퀴나크리돈 화합물의 제조방법 |
Country Status (5)
Country | Link |
---|---|
US (1) | US4895948A (ko) |
EP (1) | EP0348346B1 (ko) |
JP (1) | JP2791109B2 (ko) |
KR (1) | KR970000737B1 (ko) |
DE (1) | DE58908205D1 (ko) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5194088A (en) * | 1991-07-08 | 1993-03-16 | Ciba-Geigy Corporation | Process for conditioning organic pigments |
US5383966A (en) * | 1992-12-23 | 1995-01-24 | Miles Inc. | Process for the preparation of dispersible quinacridones |
DE4403231A1 (de) * | 1994-02-03 | 1995-08-10 | Hoechst Ag | Verfahren zur Herstellung von Chinacridonpigmenten |
US5491235A (en) * | 1994-05-06 | 1996-02-13 | Bayer Corporation | Process for the preparation of organic pigments |
US5496405A (en) | 1994-12-06 | 1996-03-05 | Bayer Corporation | Process for the preparation of organic pigments |
US5711800A (en) * | 1996-12-31 | 1998-01-27 | Bayer Corporation | Organic pigment compositions |
US5698024A (en) * | 1996-12-31 | 1997-12-16 | Bayer Corporation | Organic pigment compositions |
US6402829B1 (en) | 2000-12-20 | 2002-06-11 | Sun Chemical Corporation | Process for preparing a substantially pure gamma phase quinacridone pigment of large particle size |
US6494948B2 (en) * | 2000-12-22 | 2002-12-17 | Bayer Corporation | Preparation of quinacridone pigment compositions |
DE60218632T2 (de) * | 2001-02-08 | 2007-11-15 | Ciba Speciality Chemicals Holding Inc. | Konditionierung von organischen pigmenten |
JP4214493B2 (ja) | 2006-07-20 | 2009-01-28 | Dic株式会社 | 高彩度c.i.ピグメントレッド254及びその製造方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1051762A (ko) * | 1963-04-30 | 1900-01-01 | ||
US3298847A (en) * | 1963-08-12 | 1967-01-17 | Du Pont | Method of making quinacridone solid solutions |
US3524856A (en) * | 1967-08-07 | 1970-08-18 | Sherwin Williams Co | 4,11-dichloroquinacridone pigments |
US4298398A (en) * | 1980-08-28 | 1981-11-03 | E. I. Du Pont De Nemours And Company | Process for converting premilled crude quinacridone to pigmentary form |
US4541872A (en) * | 1982-06-21 | 1985-09-17 | Ciba-Ceigy Corporation | Preparation of pigmentary grade pigment from crude pigment |
CA1199026A (en) * | 1982-06-21 | 1986-01-07 | Edward E. Jaffe | Preparation of pigmentary grade pigment from crude pigment |
US4469523A (en) * | 1983-07-11 | 1984-09-04 | E. I. Du Pont De Nemours And Company | Borax dispersion milling of quinacridones |
DE3338806A1 (de) * | 1983-10-26 | 1985-05-09 | Hoechst Ag, 6230 Frankfurt | Deckende x-modifikation des unsubstituierten linearen trans-chinacridons |
US4801702A (en) * | 1985-11-06 | 1989-01-31 | Ciba-Geigy Corporation | Process for the preparation and conditioning or organic pigments |
US4760144A (en) * | 1986-11-13 | 1988-07-26 | Ciba-Geigy Corporation | Process for preparation of yellow shade modification of gamma quinacridone |
US4810304A (en) * | 1987-02-02 | 1989-03-07 | Ciba-Geigy Corporation | Solid solutions of pyrrolo-(3,4-C)-pyrroles with quinacridones |
US4857646A (en) * | 1987-08-24 | 1989-08-15 | Ciba-Geigy Corporation | Modified beta-quinacridone pigment |
-
1988
- 1988-06-20 US US07/209,255 patent/US4895948A/en not_active Expired - Lifetime
-
1989
- 1989-06-13 EP EP89810445A patent/EP0348346B1/de not_active Expired - Lifetime
- 1989-06-13 DE DE58908205T patent/DE58908205D1/de not_active Expired - Fee Related
- 1989-06-19 KR KR1019890008428A patent/KR970000737B1/ko not_active IP Right Cessation
- 1989-06-20 JP JP1155940A patent/JP2791109B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
DE58908205D1 (de) | 1994-09-22 |
KR970000737B1 (ko) | 1997-01-18 |
JPH0240386A (ja) | 1990-02-09 |
US4895948A (en) | 1990-01-23 |
EP0348346A2 (de) | 1989-12-27 |
JP2791109B2 (ja) | 1998-08-27 |
EP0348346B1 (de) | 1994-08-17 |
EP0348346A3 (de) | 1991-10-09 |
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