KR900016075A - m-페녹시벤질 알코올의 제조방법 - Google Patents

m-페녹시벤질 알코올의 제조방법 Download PDF

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Publication number
KR900016075A
KR900016075A KR1019900005503A KR900005503A KR900016075A KR 900016075 A KR900016075 A KR 900016075A KR 1019900005503 A KR1019900005503 A KR 1019900005503A KR 900005503 A KR900005503 A KR 900005503A KR 900016075 A KR900016075 A KR 900016075A
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KR
South Korea
Prior art keywords
alkylene glycol
alcohol
group
hydroxybenzyl alcohol
preparing
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KR1019900005503A
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English (en)
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KR920003776B1 (ko
Inventor
류 오오이
신지 다께나까
지도시 시마까와
Original Assignee
니시무라 하루오
미쓰이도오아쓰 가가꾸 가부시끼가이샤
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Publication of KR900016075A publication Critical patent/KR900016075A/ko
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Publication of KR920003776B1 publication Critical patent/KR920003776B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/18—Preparation of ethers by reactions not forming ether-oxygen bonds
    • C07C41/24—Preparation of ethers by reactions not forming ether-oxygen bonds by elimination of halogens, e.g. elimination of HCl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/16—Preparation of ethers by reaction of esters of mineral or organic acids with hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C4/00—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms
    • C07C4/08—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms by splitting-off an aliphatic or cycloaliphatic part from the molecule
    • C07C4/12—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms by splitting-off an aliphatic or cycloaliphatic part from the molecule from hydrocarbons containing a six-membered aromatic ring, e.g. propyltoluene to vinyltoluene
    • C07C4/14—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms by splitting-off an aliphatic or cycloaliphatic part from the molecule from hydrocarbons containing a six-membered aromatic ring, e.g. propyltoluene to vinyltoluene splitting taking place at an aromatic-aliphatic bond
    • C07C4/16—Thermal processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/257—Ethers having an ether-oxygen atom bound to carbon atoms both belonging to six-membered aromatic rings
    • C07C43/295—Ethers having an ether-oxygen atom bound to carbon atoms both belonging to six-membered aromatic rings containing hydroxy or O-metal groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

내용 없음.

Description

m-페녹시벤질 알코올의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (5)

  1. 반응 용매로서 안킬렌 글리콜을 사용함을 특징으로 하는, 구리 촉매 및 염기 존재하에서 m-히드록시벤질 알코올과 클로로 벤젠을 반응 시킴에 의한 m-페녹시벤질 알코올의 제조방법.
  2. 제1항에 있어서, 알킬렌 글리콜은 하기식 (Ⅰ)로 표시된 에틴렌글리콜 또는 프로필렌글리콜임을 특징으로 하는 방법.
    (식중에서, R 및 R1는 서로 독립으로 수소원자, 메틸기, 에틸기, 프로필기 또는 부틸기이며, X1및 X2는 서로 독립직으로 수소원자 또는 메틸기이며: n은 1-10의 정수임)
  3. 제1항에 있어서, 알킬렌 글리콜은 m-히드록시벤질 알코올의 몰당 0.1∼10몰의 양으로 사용함을 특징으로하는 방법.
  4. 제1항에 있어서, 클로로벤젠은 m-히드록시벤질 알코올의 몰당 0.1-20몰의 양으로 사용함을 특징으로 하는 방법.
  5. 제1항 있어서, 반응은 120-200℃에서 수행함을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019900005503A 1989-04-19 1990-04-19 m-페녹시벤질 알코올의 제조방법 KR920003776B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP1-97630 1989-04-19
JP9763089 1989-04-19

Publications (2)

Publication Number Publication Date
KR900016075A true KR900016075A (ko) 1990-11-12
KR920003776B1 KR920003776B1 (ko) 1992-05-14

Family

ID=14197488

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019900005503A KR920003776B1 (ko) 1989-04-19 1990-04-19 m-페녹시벤질 알코올의 제조방법

Country Status (5)

Country Link
US (1) US5068459A (ko)
EP (1) EP0394042B1 (ko)
KR (1) KR920003776B1 (ko)
CA (1) CA2014818C (ko)
DE (1) DE69001191T2 (ko)

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3371120A (en) * 1964-09-21 1968-02-27 Monsanto Co 3, 4'-halogen-containing diphenyl ethers and thio ethers
DE2213785A1 (de) * 1972-03-22 1973-09-27 Union Rheinische Braunkohlen Verfahren zur herstellung von phenoxyphenolen bzw. chlorphenoxyphenolen
DE3200431A1 (de) * 1982-01-09 1983-07-21 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von 4-fluor-3-phenoxytoluol
JPS61257938A (ja) * 1985-05-13 1986-11-15 Mitsui Toatsu Chem Inc ｍ−フエノキシベンジルアルコ−ルの製造方法

Also Published As

Publication number Publication date
CA2014818A1 (en) 1990-10-19
EP0394042A1 (en) 1990-10-24
DE69001191D1 (de) 1993-05-06
KR920003776B1 (ko) 1992-05-14
US5068459A (en) 1991-11-26
CA2014818C (en) 1995-02-28
EP0394042B1 (en) 1993-03-31
DE69001191T2 (de) 1993-10-14

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