KR890005170A - 폴리페놀의 폴리(비닐벤질에테르)의 제조방법 - Google Patents

폴리페놀의 폴리(비닐벤질에테르)의 제조방법 Download PDF

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Publication number
KR890005170A
KR890005170A KR1019880012076A KR880012076A KR890005170A KR 890005170 A KR890005170 A KR 890005170A KR 1019880012076 A KR1019880012076 A KR 1019880012076A KR 880012076 A KR880012076 A KR 880012076A KR 890005170 A KR890005170 A KR 890005170A
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South Korea
Prior art keywords
ether
halide
vinylbenzyl
carbon atoms
alkali metal
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KR1019880012076A
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English (en)
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KR910008336B1 (ko
Inventor
리우 밍-비안
갇샬크스 제임스
에커 어니스트
칼데코트 알프레드
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리챠드 지.워터맨
더 다우 케미칼 캄파니
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Publication of KR890005170A publication Critical patent/KR890005170A/ko
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Publication of KR910008336B1 publication Critical patent/KR910008336B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/16—Preparation of ethers by reaction of esters of mineral or organic acids with hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/38—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)

Abstract

내용 없음

Description

폴리페놀의 폴리(비닐벤질 에테르)의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 폴리페놀의 알칼리 금속, 알칼리 토금속 또는 암모늄염을 액체 반응 매질 중의 비닐벤질 할라이드와 반응시키는 단계를 포함하는, 폴리페놀의 폴리(비닐벤질 에테르)를 제조하는 방법에 있어서, 상기의 액체반응 매질이 필수적으로 탄소수 1 내지 11의 모노하이드릭 알콜 또는 글리콜, 중량 평균 분자량이 200 내지 4000 범위내인 폴리글리콜, 또는 글리세롤로 구성됨을 특징으로 하는 방법.
  2. 제1항에 있어서, 비닐벤질 할라이드가 비닐벤질 클로라이드인 방법.
  3. 제1항에 있어서, 일가 알콜이 메탄올, 에탄올, 1-프로판올, 2-프로판올, 1-부탄올 및 1-펜탄올로 구성된 그룹으로부터 선택되는 방법.
  4. 제1항에 있어서, 글리콜이 에틸렌 글리콜 및 프로필렌 글리콜로 구성된 그룹으로부터 선택되는 방법.
  5. 제1항에 있어서, 폴리글리콜이 폴리프로필렌 글리콜인 방법.
  6. 제1항에 있어서, 폴리페놀의 알칼리 금속염이, 폴리페놀을 수산화리튬, 수산화나트륨, 또는 수산화칼륨과 반등시킴으로써 제조되는 방법.
  7. 제1항에 있어서, 추가로 a) 제조된 에테르를 약1.0중량% 이하의 알칼리 금속, 알칼리 토금속, 또는 암모늄 할라이드를 용해시키는 용매중에 용해시키고, b) 할라이드 염으로부터 에테르 용액을 분리시킨후, c) 용액으로부터 에테르를 회수함으로써, 제조된 에테르의 할라이드 이온 함량을 감소시키는 단계를 특징으로 하는 방법.
  8. 제7항에 있어서, 용매가 탄소수 1 내지 4의 할로겐화된 알칼 또는 알켄, 포화된 지방족 케톤, 탄소수 1내지 6의 디알콕시-치환된 탄화수소, 사이클릭 에테르 및 클로로벤젠으로 구성된 그룹으로부터 선택되는 방법.
  9. a) 에테르를 1.0중량% 이하의 알칼리 금속, 알칼리 토금속, 또는 암모늄 할라이드를 용해시키는 용매중에 용해시키고, b) 할라이드 염으로부터 에테르 용액을 분리시킨 후, c) 용액으로부터 에테르를 회수하는 단계를 특징으로 하여, 폴리페놀의 알칼리 금속, 알칼리 토금속 또는 암모늄 염을 비닐벤질 할라이드와 반응시켜 제조한 폴리페놀의 폴리(비닐벤질 에테르)의 할라이드 이온 함량을 감소시키는 방법.
  10. 제9항에 있어서, 용매가 탄소수 1 내지 4의 할로겐화 알칸 또는 알켄, 포화 지방족 케톤, 탄소수 1 내지 6의 디알콕시-치환된 탄화수소, 사이클릭 에테르 및 클로로벤젠으로 구성된 그룹으로부터 선택되는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880012076A 1987-09-23 1988-09-19 폴리페놀의 폴리(비닐벤질 에테르)의 제조방법 KR910008336B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US100,067 1987-09-23
US07/100,067 US4956442A (en) 1987-09-23 1987-09-23 Process for preparing poly (vinylbenzyl ethers) of polyphenols

Publications (2)

Publication Number Publication Date
KR890005170A true KR890005170A (ko) 1989-05-13
KR910008336B1 KR910008336B1 (ko) 1991-10-12

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KR1019880012076A KR910008336B1 (ko) 1987-09-23 1988-09-19 폴리페놀의 폴리(비닐벤질 에테르)의 제조방법

Country Status (11)

Country Link
US (1) US4956442A (ko)
EP (1) EP0310835B1 (ko)
JP (1) JP2656956B2 (ko)
KR (1) KR910008336B1 (ko)
AT (1) ATE93507T1 (ko)
AU (2) AU626069B2 (ko)
BR (1) BR8804909A (ko)
DE (1) DE3883472T2 (ko)
IL (1) IL87751A (ko)
MX (1) MX166033B (ko)
ZA (1) ZA887100B (ko)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7193019B2 (en) * 2003-10-22 2007-03-20 Mitsubishi Gas Chemical Company, Inc. Process for the production of vinyl compound
EP2006318B1 (en) * 2007-06-18 2014-04-30 Mitsubishi Gas Chemical Company, Inc. Process for the production of vinyl compound
JP5233710B2 (ja) * 2008-02-12 2013-07-10 三菱瓦斯化学株式会社 樹脂組成物、プリプレグおよび金属箔張り積層板
US20180362435A1 (en) * 2017-06-14 2018-12-20 Chevron Phillips Chemical Company Lp High porosity aromatic resins as promoters in acrylate production from coupling reactions of olefins and carbon dioxide
JPWO2022054614A1 (ko) 2020-09-10 2022-03-17

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3058953A (en) * 1959-05-27 1962-10-16 Dow Chemical Co Vinylbenzylhalophenylether and polymers and method of making the same
US4116936A (en) * 1975-07-23 1978-09-26 The Dow Chemical Company Polyvinylbenzyl ethers of polyphenols, their polymers and copolymers
US4180680A (en) * 1978-07-28 1979-12-25 The Dow Chemical Company Preparation of halophenylvinylbenzyl ethers
JPS6067521A (ja) * 1983-09-22 1985-04-17 Agency Of Ind Science & Technol 高分子架橋剤とその製法
US4774316A (en) * 1986-08-15 1988-09-27 The Dow Chemical Company Copolymer of vinylbenzyl ether of polyhydric halogenated phenolic compound and aromatic polycyanate ester compound
US4707558A (en) * 1986-09-03 1987-11-17 The Dow Chemical Company Monomers and oligomers containing a plurality of vinylbenzyl ether groups, method for their preparation and cured products therefrom

Also Published As

Publication number Publication date
ZA887100B (en) 1990-05-30
MX166033B (es) 1992-12-16
AU626069B2 (en) 1992-07-23
AU7112291A (en) 1991-06-13
AU636710B2 (en) 1993-05-06
EP0310835A2 (en) 1989-04-12
US4956442A (en) 1990-09-11
EP0310835B1 (en) 1993-08-25
JPH01158034A (ja) 1989-06-21
BR8804909A (pt) 1989-05-02
ATE93507T1 (de) 1993-09-15
IL87751A (en) 1992-02-16
KR910008336B1 (ko) 1991-10-12
DE3883472D1 (de) 1993-09-30
IL87751A0 (en) 1989-02-28
AU2234488A (en) 1989-03-23
JP2656956B2 (ja) 1997-09-24
DE3883472T2 (de) 1994-01-13
EP0310835A3 (en) 1989-08-02

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