KR880011223A - 폴리아릴렌설피드의 제조방법 - Google Patents

폴리아릴렌설피드의 제조방법 Download PDF

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Publication number
KR880011223A
KR880011223A KR1019880002309A KR880002309A KR880011223A KR 880011223 A KR880011223 A KR 880011223A KR 1019880002309 A KR1019880002309 A KR 1019880002309A KR 880002309 A KR880002309 A KR 880002309A KR 880011223 A KR880011223 A KR 880011223A
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KR
South Korea
Prior art keywords
polyarylene sulfide
calcium chloride
aromatic compound
prepared
dihalogenated aromatic
Prior art date
Application number
KR1019880002309A
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English (en)
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KR960015453B1 (ko
Inventor
히로시 이노우에
도시가즈 가또오
사또시 도마고우
노리아끼 에무라
Original Assignee
나까다니 요시오
도소 가부시기 가이샤
무도오 미노루
도소 서스틸 가부시기 가이샤
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Application filed by 나까다니 요시오, 도소 가부시기 가이샤, 무도오 미노루, 도소 서스틸 가부시기 가이샤 filed Critical 나까다니 요시오
Publication of KR880011223A publication Critical patent/KR880011223A/ko
Application granted granted Critical
Publication of KR960015453B1 publication Critical patent/KR960015453B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/0231—Polyarylenethioethers containing chain-terminating or chain-branching agents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0254—Preparatory processes using metal sulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/14—Polysulfides

Abstract

내용없음

Description

폴리아릴렌설피드의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 디할로겐화 방향족 화합물과 알카리금속 설피드를 비양자성 극성용매중 약 200 내지 약 270℃의 온도에서 약 0.5 내지 약 30시간동안 교반하면서 중합반응시켜 폴리아릴렌설피드를 제조하는 방법에 있어서, 디할로겐화 방향족 화합물의 전환율이 약 60 내지 약 98몰%에 도달된 후 디할로겐화 방향족 화합물 몰당 염화칼슘 약 0.05 내지 약 5몰을 첨가하고 반응을 계속시키는 것으로 이루어진 폴리아릴렌설피드의 제조방법.
  2. 제 1항에 있어서, 염화칼슘의 양이 디하로겐화 방향족 화합물 몰당 약0.1 내지 약 3몰인 폴리아리렌설피드의 제조방법.
  3. 제 1항에 있어서, 염화칼슘을 디할로겐화방향족 화합물의 전환율이 약 85 재지 약 97 몰%에 도달한 후 반응계에 첨가하고 반응을 게속시키는 폴리아릴렌설피드의 제조방법.
  4. 제 1항에 있어서, 중합반응을 약200 내지 약 270℃의 온도에서 약 1 내지 약15시간 동안 교반하면서 수행하는 폴리아릴렌설피드의 제조방법.
  5. 제1항에 있어서, 염화칼슘을 반응물에 첨가하기 전에 중합반응을 약 200 내지약 250℃의 온도에서 수행하는 폴리아릴렌설피드의 제조방법.
  6. 제 1항의 방법에 의해 제조된 폴리아릴렌 설피드.
  7. 제 2항의 방법에 의해 제조된 폴리아릴렌 설피드.
  8. 제3항의 방법에 의해 제조된 폴리아릴렌 설피도.
  9. 제 4항의 방법에 의해 제조된 폴리아릴렌 설피드.
  10. 제5항의 방법에 의해 제조된 폴리아릴렌 설피드.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880002309A 1987-03-06 1988-03-05 폴리아릴렌설피드의 제조방법 KR960015453B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP62049913A JPH0739489B2 (ja) 1987-03-06 1987-03-06 ポリアリ−レンスルフイドの製造方法
JP87-49913 1987-03-06
JP62-49913 1987-03-06

Publications (2)

Publication Number Publication Date
KR880011223A true KR880011223A (ko) 1988-10-27
KR960015453B1 KR960015453B1 (ko) 1996-11-14

Family

ID=12844251

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019880002309A KR960015453B1 (ko) 1987-03-06 1988-03-05 폴리아릴렌설피드의 제조방법

Country Status (6)

Country Link
US (1) US4840986A (ko)
EP (1) EP0281406B1 (ko)
JP (1) JPH0739489B2 (ko)
KR (1) KR960015453B1 (ko)
CA (1) CA1309549C (ko)
DE (1) DE3882746T2 (ko)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01246127A (ja) * 1987-12-19 1989-10-02 Idemitsu Petrochem Co Ltd 塩化リチウムの回収方法
JP2684637B2 (ja) * 1988-06-03 1997-12-03 東ソー株式会社 ポリフェニレンスルフィドの製造方法
US5026824A (en) * 1988-08-17 1991-06-25 Eastman Kodak Company Copoly(phenylene sulfide)
US5021546A (en) * 1989-03-16 1991-06-04 Eastman Kodak Company Copoly(phenylene sulfide)
US5064937A (en) * 1989-03-27 1991-11-12 Eastman Kodak Company Copoly(phenylene sulfide)
DE3911766A1 (de) * 1989-04-11 1990-10-18 Bayer Ag Polyarylensulfide mit sulfonsaeure- und/oder sulfonsaeurederivat-endgruppen, deren herstellung und verwendung
US5250603A (en) * 1992-01-24 1993-10-05 Phillips Petroleum Company Polymer/bi-lobal fiber composites having improved strength
US5789533A (en) * 1995-06-29 1998-08-04 Tonen Chemical Corporation Polyarylene sulfide, a process for the preparation thereof and a composition comprising the same
ATE246987T1 (de) * 1995-12-12 2003-08-15 Uponor Innovation Ab Verfahren zum herstellen von homogenen materialien mit einem extruder, und extruder
JP2002293937A (ja) * 2001-03-30 2002-10-09 Petroleum Energy Center ポリアリーレンスルフィド副生塩の処理方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS453368Y1 (ko) * 1967-07-28 1970-02-16
US3919177A (en) * 1973-11-19 1975-11-11 Phillips Petroleum Co P-phenylene sulfide polymers
US4038263A (en) * 1975-05-27 1977-07-26 Phillips Petroleum Company Production of p-phenylene sulfide polymers
US4495332A (en) * 1982-07-29 1985-01-22 Kureha Kagaku Kogyo Kabushiki Kaisha Process for producing aromatic sulfide polymers
US4588789A (en) * 1983-12-07 1986-05-13 Phillips Petroleum Company Method for the crystallization of poly(arylene sulfide)
CA1230197A (en) * 1983-12-07 1987-12-08 Lacey E. Scoggins Method for the crystallization of poly(arylene sulfide)
US4645828A (en) * 1984-03-23 1987-02-24 Oncogen Platelet related growth regulator
JPS617332A (ja) * 1984-06-20 1986-01-14 Kureha Chem Ind Co Ltd 高分子量ポリアリ−レンスルフイドの製造法
US4645826A (en) * 1984-06-20 1987-02-24 Kureha Kagaku Kogyo Kabushiki Kaisha Process for production of high to ultra-high molecular weight linear polyarylenesulfides
JPS62150751A (ja) * 1985-12-25 1987-07-04 Toray Ind Inc ポリフエニレンスルフイド樹脂封止電子部品
JPS62156162A (ja) * 1985-12-28 1987-07-11 Toray Ind Inc ポリフエニレンスルフイド樹脂組成物

Also Published As

Publication number Publication date
JPH0739489B2 (ja) 1995-05-01
DE3882746D1 (de) 1993-09-09
CA1309549C (en) 1992-10-27
JPS63218735A (ja) 1988-09-12
KR960015453B1 (ko) 1996-11-14
DE3882746T2 (de) 1994-02-24
EP0281406A2 (en) 1988-09-07
US4840986A (en) 1989-06-20
EP0281406B1 (en) 1993-08-04
EP0281406A3 (en) 1989-04-05

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