KR870007091A - 5-비닐-2-노르보르넨의 연속적 제조방법 - Google Patents

5-비닐-2-노르보르넨의 연속적 제조방법 Download PDF

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Publication number
KR870007091A
KR870007091A KR870000342A KR870000342A KR870007091A KR 870007091 A KR870007091 A KR 870007091A KR 870000342 A KR870000342 A KR 870000342A KR 870000342 A KR870000342 A KR 870000342A KR 870007091 A KR870007091 A KR 870007091A
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South Korea
Prior art keywords
butadiene
cyclopentadiene
total weight
dicyclopentadiene
norbornene
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KR870000342A
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English (en)
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KR950000632B1 (ko
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가즈오 기무라
마사히로 우스이
후지오 마스꼬
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모리 히데오
스미또모 가가꾸 고오교 가부시끼가이샤
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C13/00—Cyclic hydrocarbons containing rings other than, or in addition to, six-membered aromatic rings
    • C07C13/02—Monocyclic hydrocarbons or acyclic hydrocarbon derivatives thereof
    • C07C13/08—Monocyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with a five-membered ring
    • C07C13/15—Monocyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with a five-membered ring with a cyclopentadiene ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/20—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
    • C07C2/50—Diels-Alder conversion
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/36—Systems containing two condensed rings the rings having more than two atoms in common
    • C07C2602/42—Systems containing two condensed rings the rings having more than two atoms in common the bicyclo ring system containing seven carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음

Description

5-비닐-2-노르보르넨의 연속적 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

  1. 시클로펜타디엔 및 부타디엔의 총중량 또는 시클로펜타디엔 및 디시클로펜타디엔 및 부타디엔의 혼합물의 총중량에 대하여 10~10,000ppm의 N,N-디에틸히드록실아민을 가하고, 생성된 혼합물을 내압 반응기에 연속적으로 도입시키고, 내압 반응기내에서 기상 부분의 부재하에 반응 시키고 반응 생성물을 연속적으로 취출함을 특징으로 하는 딜스-알더 반응에 의해 시클로펜타디엔 및 부타디엔으로부터 또는 시클로펜타디엔 및 디시클로펜타디엔 및 부타디엔의 혼합물로부터 5-비닐-2-노르보르넨을 연속적으로 제조하는 방법.
  2. 제1항에 있어서시, 클로펜타디엔 및 부타디엔의 총중량 또는 시클로펜타디엔 및 디시클로펜타디엔 및 부타디엔의 혼합물이 총중량에 대하여 100-5,000ppm의 N,N-디에틸히드록실아민을 가함을 특징으로 하는 5-비닐-2-노르보르넨의 연속적 제조방법.
  3. 시클로펜타디엔의 및 부타디엔의 총중량 또는 시클로펜타디엔 및 디시클로펜타디엔 및 부타디엔의 혼합물의 총중량에 대하여 10-10,000ppm의 4-옥소-2,2,6,6-테트라메틸피페리딘-1-옥실을 가하고, 생성된 혼합물을 내압반응기에 연속적으로 도입시키고, 내압 반응기내에서 기상 부분의 부재하에 반응시키고 반응 생성물을 연속적으로 취출함을 특징으로 하는, 딜스-알더 반응에 의해 시클로펜타디엔및 부타디엔으로부터 또는 시클로펜타디엔 및 디시클로펜타디엔 및 부타디엔의 혼합물로부터 5-비닐-2-노르보르넨을 연속적으로 제조하는 방법.
  4. 제3항에 있어서, 시클로펜타디엔 및 부타디엔의 총중량 또는 시클로펜타디엔 및 디시클로펜타디엔 및 부타디엔의 혼합물의 총중량에 대하여 100~5,000ppm의 4-옥소-2,2,6,6-테트라메틸피페리딘-1-옥실을 가함을 특징으로 하는 5-비닐-2-2-노르보르넨의 연속적 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870000342A 1986-01-18 1987-01-17 5-비닐-2-노르보르넨의 연속적 제조방법 KR950000632B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP61008603A JPS62167735A (ja) 1986-01-18 1986-01-18 ５−ビニル−２−ノルボルネンの連続的製造方法
JP8603 1986-01-18
JP86-8603 1986-01-18

Publications (2)

Publication Number Publication Date
KR870007091A true KR870007091A (ko) 1987-08-14
KR950000632B1 KR950000632B1 (ko) 1995-01-26

Family

ID=11697537

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Application Number Title Priority Date Filing Date
KR1019870000342A KR950000632B1 (ko) 1986-01-18 1987-01-17 5-비닐-2-노르보르넨의 연속적 제조방법

Country Status (7)

Country Link
US (1) US4777309A (ko)
EP (1) EP0229987B1 (ko)
JP (1) JPS62167735A (ko)
KR (1) KR950000632B1 (ko)
CA (1) CA1270860A (ko)
DE (1) DE3665571D1 (ko)
MX (1) MX172655B (ko)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW229214B (ko) * 1992-01-10 1994-09-01 Shell Oil Co
US5565069A (en) * 1994-05-30 1996-10-15 Sumitomo Chemical Company Limited Process for producing 5-vinyl-2-norbornene
JP4712440B2 (ja) * 2005-05-18 2011-06-29 シロキ工業株式会社 タンブルシート
IT1391108B1 (it) * 2008-08-19 2011-11-18 Fastech S R L Processo per la preparazione di etilidennorbornene.
JP6247882B2 (ja) * 2013-10-03 2017-12-13 株式会社サン・ペトロケミカル ５−ビニル−２−ノルボルネンの製造方法及びこれに用いる重合禁止剤の回収方法
CN105585414B (zh) * 2014-10-22 2019-11-12 中国石油化工股份有限公司 一种合成乙烯基降冰片烯的方法
CN104744201B (zh) * 2015-02-13 2017-04-05 浙江大学 通过多侧线变压型管式反应器合成乙叉降冰片烯的方法
CN104744202B (zh) * 2015-02-13 2017-04-05 浙江大学 一进多出变压型管式反应器合成乙烯基降冰片烯的方法
CN105541529B (zh) * 2015-12-07 2017-10-31 上海派尔科化工材料股份有限公司 一种乙烯基降冰片烯的生产方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD94175A (ko) *
DE94175C (ko) *
NL296169A (ko) * 1962-08-14
JPS4525941Y1 (ko) * 1966-12-21 1970-10-09
JPS5138380B2 (ko) * 1972-07-05 1976-10-21
NL7302865A (ko) * 1973-03-01 1974-09-03
SU462810A1 (ru) * 1973-03-07 1975-03-05 Предприятие П/Я В-8952 Способ получени винилнорборнена
DE2326070C3 (de) * 1973-05-22 1979-10-25 Siemens Ag, 1000 Berlin Und 8000 Muenchen Vorrichtung zur Entfernung von Kohlendioxid aus zum Betrieb von elektrochemischen Zellen dienender Luft
JPS5115001A (en) * 1974-07-30 1976-02-06 Jujo Paper Co Ltd Arukariparupuno seizoho
DE3307486A1 (de) * 1983-03-03 1984-09-06 Bunawerke Hüls GmbH, 4370 Marl Verfahren zum verhindern der bildung von polymeren nebenprodukten bei der herstellung von diels-alder-addukten
JPS59164731A (ja) * 1983-03-11 1984-09-17 Japan Synthetic Rubber Co Ltd エチリデンノルボルネンの製造方法
DE3311405C2 (de) * 1983-03-29 1986-10-09 Bunawerke Hüls GmbH, 4370 Marl Verfahren zur kontinuierlichen Herstellung von 5-Ethyliden-bicyclo-[2.2.1]-hepten-(2) und 5-Methylen-6-methyl-bicyclo-[2.2.1]-hepten-(2)

Also Published As

Publication number Publication date
DE3665571D1 (en) 1989-10-19
EP0229987B1 (en) 1989-09-13
EP0229987A1 (en) 1987-07-29
US4777309A (en) 1988-10-11
KR950000632B1 (ko) 1995-01-26
JPS62167735A (ja) 1987-07-24
CA1270860A (en) 1990-06-26
MX172655B (es) 1994-01-06
JPH0329772B2 (ko) 1991-04-25

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