KR850001142A - 낮은 에너지 소모로서 고순도 부텐-1의 제조방법 - Google Patents
낮은 에너지 소모로서 고순도 부텐-1의 제조방법 Download PDFInfo
- Publication number
- KR850001142A KR850001142A KR1019840004010A KR840004010A KR850001142A KR 850001142 A KR850001142 A KR 850001142A KR 1019840004010 A KR1019840004010 A KR 1019840004010A KR 840004010 A KR840004010 A KR 840004010A KR 850001142 A KR850001142 A KR 850001142A
- Authority
- KR
- South Korea
- Prior art keywords
- butene
- stage
- fractionation
- injected
- condenser
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C11/00—Aliphatic unsaturated hydrocarbons
- C07C11/02—Alkenes
- C07C11/08—Alkenes with four carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/005—Processes comprising at least two steps in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/04—Purification; Separation; Use of additives by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/08—Waste heat
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
첨부도면은 본 발명에 따른 공정도.
Claims (3)
- 포화지방족 알콜로 에테르화 시킴에 의하여 이소부텐을 제거하고, 이소부텐 부재류를 30-200ppm의 총량까지 부타디엔과 아세틸렌 유도체의 함량을 감소시키기 위하여 선택적으로 수소화시키는 단계를 거쳐, 선택적인 수소화단계로 부터의 반응류를 4-20절대기압의 압력하에서 첫번째 분별단계에 주입하고 이 단계에서 이소부탄과 소량의 부텐-1로 구성된 상부류와 원료류의 잔유성분들을 포함한 저부류를 얻으며, 첫번째 분별단계로부터의 저부류를 4-12절대기압의 압력범위하에서 둘째 분별단계에 주입하여 이곳으로부터 고순도 부텐-1로 구성된 상부 생성물을 수득하며, n-부탄, 트랜스-및 시스-부텐-2 및 소량의 부텐-1로 구성된 저부생성물을 수득하는 공정에 있어서, 둘째분별 단계로부터의 상부 생성물을 압축장치로 압축시킨 다음 일부는 첫번째 분별단계의 재보일러에 보내고 나머지는 둘째 분별단계의 재보일러에 보내어 두 재보일러에서 응축된 부텐-1의 일부는 최종제품으로 배출되고 일부는 다른 공정단계에서 사용함을 특징으로 하는 부타디엔 및 아세틸렌 유도체를 포함한 C4류로 구성된 원료물질로부터 낮은 에너지 소모로서 고순도 부텐-1의 제조방법.
- 청구범위 제1항에 있어서 최종제품으로서 배출되지 않은 부텐-1의 일부를 둘째 분별단계의 상단부에 주입하여 여기에서 환류에 사용하고, 일부는 첫째 분별단계의 상단 응축기에 주입하여 여기에서 증발되어 상부 생성물을 응축시키기 위한 냉각유체로서 사용함을 특징으로 하는 바의 방법.
- 청구범위 제1항과 2항에 있어서 환류제로서 둘째 분별단계의 상단부에 주입된 부텐-1과 첫째 분별단계의 응축기에 주입된 부텐-1은 환류제로서 둘째 단계에 그리고 첫째 단계의 응축기에 각각 들어가기전에 팽창되어 부텐-1의 증기를 발생하며 첫째단계의 응축기에서 발생한 부텐-1의 증기와 둘째 단계의 상단으로부터 발생한 부텐-1의 증기는 두 분별단계의 하나 또는 양쪽의 재보일러에 보냄을 특징으로 하는 바의 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT22293A/83 | 1983-07-28 | ||
IT22293/83A IT1194350B (it) | 1983-07-28 | 1983-07-28 | Procedimento per la produzione di butene-1 ad elevata purezza con basso consumo di energia |
IT2293A/83 | 1983-07-28 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR850001142A true KR850001142A (ko) | 1985-03-16 |
KR870000582B1 KR870000582B1 (ko) | 1987-03-23 |
Family
ID=11194279
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019840004010A KR870000582B1 (ko) | 1983-07-28 | 1984-07-10 | 부텐-1의 제조방법 |
Country Status (27)
Country | Link |
---|---|
US (1) | US4718986A (ko) |
JP (1) | JPS6051130A (ko) |
KR (1) | KR870000582B1 (ko) |
AU (1) | AU3003984A (ko) |
BE (1) | BE900249A (ko) |
BR (1) | BR8403666A (ko) |
CA (1) | CA1232617A (ko) |
DD (1) | DD222301A5 (ko) |
DE (1) | DE3426359A1 (ko) |
DK (1) | DK369684A (ko) |
ES (1) | ES534968A0 (ko) |
FR (1) | FR2549824B1 (ko) |
GB (1) | GB2144145B (ko) |
GR (1) | GR82651B (ko) |
HU (1) | HUT36763A (ko) |
IT (1) | IT1194350B (ko) |
LU (1) | LU85467A1 (ko) |
NL (1) | NL8402385A (ko) |
NO (1) | NO843021L (ko) |
PH (1) | PH20654A (ko) |
PL (1) | PL248947A1 (ko) |
PT (1) | PT78989B (ko) |
RO (1) | RO90564A (ko) |
SE (1) | SE8403427L (ko) |
TR (1) | TR22072A (ko) |
YU (1) | YU132084A (ko) |
ZA (1) | ZA845089B (ko) |
Families Citing this family (34)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5294304A (en) * | 1989-11-14 | 1994-03-15 | Ministry Of International Trade And Industry | Process for the recovery of absolute ethanol by vapor compression extractive distillation |
FR2673178B1 (fr) * | 1991-02-26 | 1994-02-11 | Institut Francais Petrole | Procede de separation de butanes et de butenes par distillation extractive. |
IT1270675B (it) | 1994-10-19 | 1997-05-07 | Enichem Spa | Procedimento per la separazione di paraffine in miscela con olefine |
IT1276802B1 (it) * | 1995-06-30 | 1997-11-03 | Enichem Spa | Procedimento integrato per la produzione di butene-1 |
DE10350045A1 (de) * | 2003-10-27 | 2005-05-25 | Basf Ag | Verfahren zur Herstellung von 1-Buten |
DE10350044A1 (de) * | 2003-10-27 | 2005-05-25 | Basf Ag | Verfahren zur Herstellung von 1-Buten |
DE10361823A1 (de) | 2003-12-30 | 2005-08-11 | Basf Ag | Verfahren zur Herstellung von Butadien und 1-Buten |
DE10361822A1 (de) * | 2003-12-30 | 2005-08-11 | Basf Ag | Verfahren zur Herstellung von Butadien |
DE10361824A1 (de) * | 2003-12-30 | 2005-07-28 | Basf Ag | Verfahren zur Herstellung von Butadien |
DE102004054766A1 (de) * | 2004-11-12 | 2006-05-18 | Basf Ag | Verfahren zur Herstellung von Butadien aus n-Butan |
DE102004055826A1 (de) * | 2004-11-19 | 2006-05-24 | Basf Ag | Verfahren und Vorrichtung zur Vollhydrierung eines Kohlenwasserstoffstromes |
DE102004059356A1 (de) * | 2004-12-09 | 2006-06-14 | Basf Ag | Verfahren zur Herstellung von Butadien aus n-Butan |
US20070137097A1 (en) * | 2005-12-16 | 2007-06-21 | Michio Ikura | Production of biodiesel from triglycerides via a thermal route |
US7638573B2 (en) * | 2006-04-07 | 2009-12-29 | Exxonmobil Chemical Patents Inc. | Butyl nanocomposite via low Mw elastomer pre-blend |
KR100822847B1 (ko) * | 2007-03-29 | 2008-04-16 | 한국에너지기술연구원 | 올레핀/파라핀 혼합가스에서 올레핀 분리 기술 |
KR100836707B1 (ko) | 2007-04-25 | 2008-06-10 | 한국에너지기술연구원 | 올레핀/파라핀 혼합가스에서 고순도 부텐-1 분리 기술 |
US20080302650A1 (en) * | 2007-06-08 | 2008-12-11 | Brandon Bello | Process to recover low grade heat from a fractionation system |
EP2259855B1 (en) * | 2008-04-04 | 2012-06-20 | Lummus Technology Inc. | Batch process and system for the production of olefins |
US7982086B2 (en) * | 2009-02-03 | 2011-07-19 | Catalytic Distillation Technologies | Deisobutenizer |
US9044711B2 (en) * | 2009-10-28 | 2015-06-02 | Oasys Water, Inc. | Osmotically driven membrane processes and systems and methods for draw solute recovery |
CN105771654A (zh) | 2009-10-28 | 2016-07-20 | Oasys水有限公司 | 正向渗透分离工艺 |
JP5863734B2 (ja) * | 2013-09-18 | 2016-02-17 | ラムス テクノロジー インク | 直鎖アルファオレフィンを製造するためのシステムおよびプロセス |
JP6140591B2 (ja) | 2013-11-21 | 2017-05-31 | 東洋エンジニアリング株式会社 | 蒸留装置 |
JP6289112B2 (ja) | 2014-01-17 | 2018-03-07 | 東洋エンジニアリング株式会社 | 蒸留塔 |
CN104926587B (zh) * | 2014-03-21 | 2017-06-16 | 青岛科技大学 | 一种1‑丁烯分离纯化的节能工艺流程 |
JP2014159464A (ja) * | 2014-05-07 | 2014-09-04 | Lummus Technology Inc | 直鎖アルファオレフィンを製造するためのシステムおよびプロセス |
CN104926588B (zh) * | 2015-06-24 | 2016-08-24 | 长岭炼化岳阳工程设计有限公司 | 分离碳四烯烃中2-丁烯的方法及分离碳四烯烃中2-丁烯的系统 |
GB201604608D0 (en) * | 2016-03-18 | 2016-05-04 | Johnson Matthey Davy Technologies Ltd | Process |
CN110088067A (zh) | 2016-12-21 | 2019-08-02 | 沙特基础全球技术有限公司 | 由催化裂化的烃料流生产烯烃的方法 |
CN110741067B (zh) * | 2017-06-08 | 2022-04-12 | 株式会社Lg化学 | 蒸馏装置及蒸馏方法 |
BR112021002933A2 (pt) * | 2018-08-23 | 2021-05-11 | Lummus Technology Llc | processo para a produção de isobutileno de alta pureza |
KR102536741B1 (ko) | 2018-12-20 | 2023-05-24 | 주식회사 엘지화학 | 라피네이트-2의 정제방법 및 정제장치 |
KR102605241B1 (ko) | 2018-12-20 | 2023-11-22 | 주식회사 엘지화학 | 라피네이트-2의 정제방법 및 정제장치 |
AR120161A1 (es) * | 2019-10-07 | 2022-02-02 | Lummus Technology Inc | Coproducción de isobutano y buteno-1 de alta pureza a partir de c₄ mixto |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2509136A (en) * | 1949-06-17 | 1950-05-23 | Gulf Oil Corp | Process and apparatus for concentrating dilute solutions |
US2619814A (en) * | 1950-04-22 | 1952-12-02 | Lummus Co | Fractional distillation |
DE1110668B (de) * | 1960-07-30 | 1961-07-13 | Linde Eismasch Ag | Verfahren und Einrichtung zum Trennen von Dreistoffgemischen, bei denen zwei Komponenten eine azeotrop siedende Mischung bilden, durch Tieftemperaturrektifikation |
US3568457A (en) * | 1969-03-05 | 1971-03-09 | Universal Oil Prod Co | Separation of propane and propylene by distillation |
FR2310327A1 (fr) * | 1975-05-09 | 1976-12-03 | Raffinage Cie Francaise | Procede d'obtention d'isobutylene de grande purete |
DE2724365C3 (de) * | 1977-05-28 | 1979-09-06 | Basf Ag, 6700 Ludwigshafen | Verfahren zum Trennen eines C4 -Kohlenwasserstoffgemisches durch extraktive Destillation |
GB1573553A (en) * | 1977-05-30 | 1980-08-28 | Stevens C | Apparatus for purifying a liquid |
US4137129A (en) * | 1977-10-07 | 1979-01-30 | Uop Inc. | Fractionation process |
JPS5575780A (en) * | 1978-12-01 | 1980-06-07 | Hisaka Works Ltd | Heat pump type water making equipment |
EP0016284B1 (en) * | 1979-03-21 | 1983-06-22 | DAVY McKEE (LONDON) LIMITED | Process for the production of a sulphur-free butene-1 rich stream |
US4230535A (en) * | 1979-06-15 | 1980-10-28 | Uop Inc. | Heat-pumped fractionation process |
US4277268A (en) * | 1979-10-17 | 1981-07-07 | Conoco, Inc. | Heat pump fractionation process |
US4336407A (en) * | 1980-02-25 | 1982-06-22 | Chemical Research & Licensing Company | Catalytic distillation process |
US4360405A (en) * | 1980-05-12 | 1982-11-23 | The Lummus Company | Process for fractionating close boiling components of a multi-component system |
FR2495605A1 (fr) * | 1980-12-05 | 1982-06-11 | Inst Francais Du Petrole | Procede d'obtention du butene-1 de haute purete a partir d'une coupe c4 olefinique |
US4395310A (en) * | 1981-07-14 | 1983-07-26 | Exxon Research And Engineering Co. | Fractionation system |
JPS5892625A (ja) * | 1981-11-27 | 1983-06-02 | Nippon Zeon Co Ltd | C↓4炭化水素留分より高純度ブテン−1又はブテン−1/イソブテン混合物の分離方法 |
DE3318858A1 (de) * | 1983-05-25 | 1984-11-29 | Basf Ag, 6700 Ludwigshafen | Verfahren zur trennung eines im wesentlichen n-butene und butane enthaltenden c(pfeil abwaerts)4(pfeil abwaerts)-kohlenwasserstoffgemisches |
-
1983
- 1983-07-28 IT IT22293/83A patent/IT1194350B/it active
-
1984
- 1984-06-27 SE SE8403427A patent/SE8403427L/xx not_active Application Discontinuation
- 1984-06-29 AU AU30039/84A patent/AU3003984A/en not_active Abandoned
- 1984-07-03 ZA ZA845089A patent/ZA845089B/xx unknown
- 1984-07-04 GR GR75185A patent/GR82651B/el unknown
- 1984-07-06 GB GB08417308A patent/GB2144145B/en not_active Expired
- 1984-07-10 KR KR1019840004010A patent/KR870000582B1/ko active IP Right Grant
- 1984-07-16 LU LU85467A patent/LU85467A1/fr unknown
- 1984-07-17 DE DE19843426359 patent/DE3426359A1/de not_active Ceased
- 1984-07-19 BR BR8403666A patent/BR8403666A/pt unknown
- 1984-07-24 CA CA000459575A patent/CA1232617A/en not_active Expired
- 1984-07-25 PH PH31031A patent/PH20654A/en unknown
- 1984-07-25 NO NO843021A patent/NO843021L/no unknown
- 1984-07-26 PL PL24894784A patent/PL248947A1/xx unknown
- 1984-07-26 FR FR8411912A patent/FR2549824B1/fr not_active Expired
- 1984-07-26 YU YU01320/84A patent/YU132084A/xx unknown
- 1984-07-27 HU HU842899A patent/HUT36763A/hu unknown
- 1984-07-27 PT PT78989A patent/PT78989B/pt unknown
- 1984-07-27 BE BE0/213406A patent/BE900249A/fr not_active IP Right Cessation
- 1984-07-27 RO RO84115360A patent/RO90564A/ro unknown
- 1984-07-27 JP JP59155718A patent/JPS6051130A/ja active Pending
- 1984-07-27 DK DK369684A patent/DK369684A/da not_active Application Discontinuation
- 1984-07-27 DD DD84265726A patent/DD222301A5/de unknown
- 1984-07-27 ES ES534968A patent/ES534968A0/es active Granted
- 1984-07-30 NL NL8402385A patent/NL8402385A/nl not_active Application Discontinuation
-
1985
- 1985-01-01 TR TR22072A patent/TR22072A/xx unknown
-
1986
- 1986-09-04 US US06/904,046 patent/US4718986A/en not_active Expired - Fee Related
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