KR850001120A - 진한 황산 제조공정으로부터 열을 회수하는 방법 - Google Patents
진한 황산 제조공정으로부터 열을 회수하는 방법 Download PDFInfo
- Publication number
- KR850001120A KR850001120A KR1019840003828A KR840003828A KR850001120A KR 850001120 A KR850001120 A KR 850001120A KR 1019840003828 A KR1019840003828 A KR 1019840003828A KR 840003828 A KR840003828 A KR 840003828A KR 850001120 A KR850001120 A KR 850001120A
- Authority
- KR
- South Korea
- Prior art keywords
- sulfuric acid
- heat
- alloy
- recovery tower
- heat recovery
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/74—Preparation
- C01B17/76—Preparation by contact processes
- C01B17/80—Apparatus
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/74—Preparation
- C01B17/76—Preparation by contact processes
- C01B17/765—Multi-stage SO3-conversion
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F21/00—Constructions of heat-exchange apparatus characterised by the selection of particular materials
- F28F21/08—Constructions of heat-exchange apparatus characterised by the selection of particular materials of metal
- F28F21/081—Heat exchange elements made from metals or metal alloys
- F28F21/082—Heat exchange elements made from metals or metal alloys from steel or ferrous alloys
- F28F21/083—Heat exchange elements made from metals or metal alloys from steel or ferrous alloys from stainless steel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Treating Waste Gases (AREA)
- Gas Separation By Absorption (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명의 장치를 포함하는 황산플랜트의 공정도.
제3도는 본 발명의 장치와 공정에 관한 다이아그램.
제4도는 종래 중간흡수탑의 운전사이클에 대한 열회수탑의 운전사이클을 나타내는 그래프이다.
Claims (16)
- 삼산화황을 온도 120℃, 농도 98% 이상 101% 이하의 황산에 흡수시키고, 열교환기에서 황산의 흡수열을 다른 유체에 의하여 유용한 형태로 제거함을 특징으로 하는 황산 제조공정에서의 열을 회수하는 방법.
- 제1항에 있어서, 황산의 농도는 99% 이상인 것.
- 제1항에 있어서, 황산의 농도는 101% 이하인 것.
- 열회수탑에서 온도 120℃ 이상, 농도 98% 이상 101% 이하의 황산에 삼산화황을 흡수시키고, 흡수열에 의해 온도가 상승한 황산 스트리임을 고온의 진한황산과의 접촉에도 낮은 부식율을 가지는 합금으로 세워진 열교환기에 통과시켜 열교환기내에서 다른 유체에 의하여 유용한 형태로 황산에 흡수된 열을 제거하는 것을 특징으로 하는 황산 제조공정에서의 열에너지 회수방법.
- 제4항에 있어서, 황산은 열교환기에서 열회수탑으로 재순환된다는 것.
- 제5항에 있어서, 황산은 재순환되는 동안 98% 이상 99% 이하의 농도로 희석한다는 것.
- 제6항에 있어서, 재순환되는 황산은 묽은 황산이나 액체 또는 증기상태인 물을 첨가하여 희석한다는 것.
- 제6항에 있어서, 재순환되는 황산은 증기상태인 물을 첨가하여 희석한다는 것.
- 하부유입구로는 삼산화황을 포함하는 가스스트리임을, 상부유입구로는 98% 이상 101% 이하의 농도와 120℃의 온도를 가지는 황산스트리임을 열회수탑에서 삼산화황을 황산에 발열반응을 수반하면서 흡수시키고, 삼산화황이 흡수된 가스스트리임은 상부유출구로, 황산은 하부유출구로 빠져나갈 수 있도록 상부와 하부에 각각의 유입구와 유출구를 가지는 열회수탑과, 다른 유체와 열교환을 통하여 유용한 형태로 황산으로부터 흡수열을 회수하기 위하여 고온의 진한 황산과 접촉하여도 부식율이 낮은 합금으로 제조된 열교환기로 구성된 황산제조공정에서의 열에너지 회수장치.
- 제9항에 있어서, 열회수탑은 세라믹재로 피복된 탄소강으로 제조된 것이라는 것.
- 제9항에 있어서, 열회수탑은 고온의 진한황산과 접촉하여도 부식율이 낮은 합금들로 제조된 것이라는 것.
- 제11항에 있어서, 열회수탑은 주합금성분이 다음의 관계를 만족하는 합금들로 제조된다는 것 :0.35(Fe+Mn)+0.70(Cr)+0.30(Ni)-0.12(Mo)>39여기에서, Fe은 합금중 철의 wt%, Mn은 합금중 망간의 wt%, Cr은 합금중 크롬의 wt%, Ni은 합금중 닉켈의 wt%이고 Mo은 합금중 몰리브덴의 wt%이다.
- 제9항에 있어서, 열교환기는 주합금성분이 다음의 관계를 만족하는 합금들로 제조된다는 것.0.35(Fe+Mn)+0.70(Cr)+0.30(Ni)-0.12(Mo)>39여기에서, Fe은 합금중 철의 wt%, Mn은 합금중 망간의 wt%, Cr은 합금중 크롬의 wt%, Ni은 합금중 닉켈의 wt%이고, Mo은 합금중 몰리브덴의 wt%이다.
- 제9항에 있어서, 열교환기는 열회수탑의 외부에 설치한다는 것.
- 제9항에 있어서, 열교환기는 열회수탑의 내부에 설회한는 것.
- 약 1000kpa의 압력하에서는 삼산화황을 98% 이상 105% 이하의 농도와 120℃ 이상의 온도를 갖는 황산에 흡수시켜, 삼산화황의 흡수에 의해 흡수된 열을 다른 유체와의 열교환에 의해서 황산으로부터 유용한 형태로 회수함을 특징으로 하는 황산 제조공정에서의 열을 회수하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US510527 | 1983-07-05 | ||
US06/510,527 US4576813A (en) | 1983-07-05 | 1983-07-05 | Heat recovery from concentrated sulfuric acid |
Publications (2)
Publication Number | Publication Date |
---|---|
KR850001120A true KR850001120A (ko) | 1985-03-16 |
KR870000916B1 KR870000916B1 (ko) | 1987-05-07 |
Family
ID=24031126
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019840003828A KR870000916B1 (ko) | 1983-07-05 | 1984-07-03 | 진한 황산 제조공정으로 부터 열을 회수하는 방법 |
Country Status (18)
Country | Link |
---|---|
US (1) | US4576813A (ko) |
EP (1) | EP0130967B2 (ko) |
JP (1) | JPS6036310A (ko) |
KR (1) | KR870000916B1 (ko) |
AU (1) | AU564505B2 (ko) |
BR (1) | BR8403294A (ko) |
CA (1) | CA1256671A (ko) |
DE (1) | DE3468857D1 (ko) |
DZ (1) | DZ713A1 (ko) |
ES (2) | ES8601066A1 (ko) |
FI (1) | FI77634C (ko) |
IN (1) | IN161448B (ko) |
MA (1) | MA20164A1 (ko) |
MX (1) | MX164158B (ko) |
NZ (1) | NZ208754A (ko) |
TR (1) | TR21894A (ko) |
YU (1) | YU45188B (ko) |
ZA (1) | ZA845086B (ko) |
Families Citing this family (31)
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US4670242A (en) * | 1984-11-09 | 1987-06-02 | Monsanto Company | Heat recovery from concentrated sulfuric acid |
US4996038A (en) * | 1983-07-05 | 1991-02-26 | Monsanto Company | Heat recovery from concentrated sulfuric acid |
DE3508532A1 (de) * | 1985-03-09 | 1986-09-18 | Bayer Ag, 5090 Leverkusen | Verwendung einer chromhaltigen legierung |
US5130112A (en) * | 1990-03-23 | 1992-07-14 | Monsanto Company | Method for recovering high grade process energy from a contact sulfuric acid process |
US5118490A (en) * | 1989-06-21 | 1992-06-02 | Monsanto Company | Absorption of wet conversion gas |
BR9106271A (pt) * | 1990-03-23 | 1993-04-13 | Monsanto Co | Metodo para recuperacao de energia de processo de alto grau a partir de um processo de acido sulfurico por contato |
DE4308151C2 (de) * | 1993-03-15 | 1995-01-19 | Bayer Ag | Verwendung von Knet- und Gußwerkstoffen sowie Schweißzusatzwerkstoffen aus austenitischem Stahl für mit heißer konzentrierter Schwefelsäure oder Oleum beaufschlagte Bauteile |
DE4342188C2 (de) * | 1993-12-10 | 1998-06-04 | Bayer Ag | Austenitische Legierungen und deren Verwendung |
US5538707A (en) * | 1994-03-01 | 1996-07-23 | Monsanto Company | Acid concentration control in SO3 absorption |
CA2405709A1 (en) | 2000-04-12 | 2001-10-25 | Human Genome Sciences, Inc. | Albumin fusion proteins |
DE10128032A1 (de) * | 2001-06-08 | 2002-12-12 | Outokumpu Oy | Verfahren zum Schutz gegen Korrossion eines Stahlteils aus austenitischem oder halbaustenitischem Stahl bei der Herstellung von Schwefelsäure |
DE10153692A1 (de) * | 2001-10-31 | 2003-05-15 | Outokumpu Oy | Verfahren und Vorrichtung zur Herstellung von Schwefelsäure |
GB0129607D0 (en) * | 2001-12-11 | 2002-01-30 | Sui See C | Exhaust eater energy generator |
DE102005008109A1 (de) * | 2005-02-21 | 2006-08-24 | Outokumpu Technology Oy | Verfahren und Anlage zur Herstellung von Schwefelsäure |
AU2007258609B2 (en) | 2006-06-07 | 2013-01-24 | Human Genome Sciences, Inc. | Albumin fusion proteins |
US8070850B2 (en) * | 2008-01-11 | 2011-12-06 | E H P Technology, LLC | Process for liberating metals using direct production of leach grade acid solutions |
JOP20200123A1 (ar) | 2010-01-20 | 2017-06-16 | Mecs Inc | استرجاع الطاقة في تصنيع حمض السلفريك |
DE102010006541B4 (de) * | 2010-02-01 | 2016-03-17 | Outotec Oyj | Verfahren und Anlage zum Abkühlen von Säure |
EP2632567B1 (en) | 2010-10-29 | 2019-08-07 | MECS, Inc. | Regenerative recovery of sulfur dioxide from effluent gases |
CN102353283A (zh) * | 2011-10-08 | 2012-02-15 | 上海奥格利环保工程有限公司 | 硫酸生产中对低温位的吸收反应热回收装置 |
MA37598B1 (fr) | 2012-05-02 | 2016-05-31 | Mecs Inc | Récupération régénérative de contaminants à partir de gaz d'effluent |
CA2902562C (en) | 2013-03-15 | 2022-01-04 | Ernesto Vera-Castaneda | Recovery of sulfur trioxide heat of absorption |
MY183705A (en) | 2013-03-15 | 2021-03-09 | Mecs Inc | Regenerative recovery of contaminants from effluent gases |
CN103836602B (zh) * | 2014-04-01 | 2016-03-02 | 丁华 | 双对称管壳式硫酸冷却器 |
CN103979501B (zh) * | 2014-06-11 | 2016-08-24 | 南京凯盛国际工程有限公司 | 一种石膏制酸换热装置 |
DE102016103976A1 (de) * | 2016-03-04 | 2017-09-07 | Thyssenkrupp Ag | Verfahren und Vorrichtung zur Herstellung von Schwefelsäure |
WO2017192264A1 (en) | 2016-05-03 | 2017-11-09 | Chemetics Inc. | Energy efficient sulfuric acid system for humid environments |
DE102017200439A1 (de) | 2017-01-12 | 2018-07-12 | Thyssenkrupp Ag | Verfahren zur Herstellung von Salpetersäure |
CN109319743A (zh) * | 2017-08-01 | 2019-02-12 | 上海乐谦工程科技有限公司 | 一种简法节能增效制取硫酸工艺 |
US20210214825A1 (en) | 2018-08-29 | 2021-07-15 | Chemetics Inc. | Austenitic stainless alloy with superior corrosion resistance |
EP4301695A1 (en) * | 2022-05-27 | 2024-01-10 | Chemetics Inc. | Tail gas treatment system and method for a sulfuric acid production plant |
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US2017676A (en) * | 1933-03-11 | 1935-10-15 | American Lurgi Corp | Method of and apparatus for condensing sulphuric acid |
US2071598A (en) * | 1935-01-11 | 1937-02-23 | American Lurgi Corp | Method of producing fuming sulphuric acid having a high concentration |
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US2655431A (en) * | 1949-01-21 | 1953-10-13 | Chemical Construction Corp | Sulfuric acid production by absorption |
GB687160A (en) * | 1949-05-31 | 1953-02-11 | Bayer Ag | Manufacture of sulphuric acid |
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DE1667642C3 (de) * | 1966-02-09 | 1980-01-17 | Nautschno-Issleodovatelskij Institut Po Udobrenijam I Insektofungizidam Im. Prof. J.V. Samojlova, Moskau | Kontaktverfahren zur Herstellung von Schwefelsäure |
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DE1567716B2 (de) * | 1966-12-03 | 1977-02-17 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur katalytischen umsetzung von so tief 2 und so tief 3 und schwefelsaeureherstellung |
US3649187A (en) * | 1970-02-09 | 1972-03-14 | Monsanto Co | Corrosion resistant apparatus |
GB1280624A (en) * | 1970-02-16 | 1972-07-05 | Imp Smelting Corp Ltd | Improvements in or relating to the purification of sulphuric acid |
CH547231A (de) * | 1970-10-15 | 1974-03-29 | Metallgesellschaft Ag | Zwischenabsorber fuer die absorption von so3 und verfahren zum betreiben des zwischenabsorbers. |
DE2348108A1 (de) * | 1973-09-25 | 1975-04-03 | Metallgesellschaft Ag | Verfahren und vorrichtung zur absorption von so tief 3 |
DE2529709C3 (de) * | 1975-07-03 | 1981-02-26 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Schwefelsäure |
DE2700009C3 (de) * | 1977-01-03 | 1979-11-15 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur Aufkonzentrierung von verdünnter Phosphorsäure |
US4123107A (en) * | 1977-02-03 | 1978-10-31 | Freeport Minerals Company | Integrated sulfur mining - sulfuric acid production system |
DE2824010A1 (de) * | 1978-06-01 | 1979-12-13 | Metallgesellschaft Ag | Verfahren zur aufkonzentrierung von verduennter phosphorsaeure |
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DE2945021A1 (de) * | 1979-11-08 | 1981-05-21 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur herstellung von konzentrierter schwefelsaeure |
JPS5734003A (en) * | 1980-06-21 | 1982-02-24 | Hidenori Arai | Obtaining method of steam for concentrating phosphoric acid from heat removed from absorption system in sulfuric acid preparing apparatus |
CA1181569A (en) * | 1982-06-11 | 1985-01-29 | Frank Smith | Apparatus and process |
-
1983
- 1983-07-05 US US06/510,527 patent/US4576813A/en not_active Expired - Lifetime
-
1984
- 1984-07-02 ES ES533910A patent/ES8601066A1/es not_active Expired
- 1984-07-03 YU YU1162/84A patent/YU45188B/xx unknown
- 1984-07-03 TR TR21894A patent/TR21894A/xx unknown
- 1984-07-03 KR KR1019840003828A patent/KR870000916B1/ko not_active IP Right Cessation
- 1984-07-03 IN IN481/MAS/84A patent/IN161448B/en unknown
- 1984-07-03 BR BR8403294A patent/BR8403294A/pt not_active IP Right Cessation
- 1984-07-03 MA MA20388A patent/MA20164A1/fr unknown
- 1984-07-03 JP JP59137863A patent/JPS6036310A/ja active Granted
- 1984-07-03 NZ NZ208754A patent/NZ208754A/en unknown
- 1984-07-03 FI FI842672A patent/FI77634C/fi not_active IP Right Cessation
- 1984-07-03 ZA ZA845086A patent/ZA845086B/xx unknown
- 1984-07-03 AU AU30233/84A patent/AU564505B2/en not_active Expired
- 1984-07-03 CA CA000458014A patent/CA1256671A/en not_active Expired
- 1984-07-04 DE DE8484870093T patent/DE3468857D1/de not_active Expired
- 1984-07-04 EP EP84870093A patent/EP0130967B2/en not_active Expired - Lifetime
- 1984-07-04 MX MX201907A patent/MX164158B/es unknown
- 1984-12-10 DZ DZ847352A patent/DZ713A1/fr active
-
1985
- 1985-05-29 ES ES543604A patent/ES8604032A1/es not_active Expired
Also Published As
Publication number | Publication date |
---|---|
IN161448B (ko) | 1987-12-05 |
ES533910A0 (es) | 1985-10-16 |
NZ208754A (en) | 1987-10-30 |
CA1256671A (en) | 1989-07-04 |
YU45188B (en) | 1992-05-28 |
FI842672A (fi) | 1985-01-06 |
JPH0459243B2 (ko) | 1992-09-21 |
ES543604A0 (es) | 1986-01-16 |
MX164158B (es) | 1992-07-20 |
MA20164A1 (fr) | 1985-04-01 |
BR8403294A (pt) | 1985-06-18 |
ZA845086B (en) | 1985-03-27 |
DE3468857D1 (en) | 1988-02-25 |
FI77634C (fi) | 1989-04-10 |
KR870000916B1 (ko) | 1987-05-07 |
US4576813A (en) | 1986-03-18 |
TR21894A (tr) | 1985-10-07 |
ES8601066A1 (es) | 1985-10-16 |
YU116284A (en) | 1987-10-31 |
ES8604032A1 (es) | 1986-01-16 |
AU3023384A (en) | 1985-01-10 |
DZ713A1 (fr) | 2004-09-13 |
EP0130967B2 (en) | 1995-05-03 |
FI842672A0 (fi) | 1984-07-03 |
AU564505B2 (en) | 1987-08-13 |
EP0130967B1 (en) | 1988-01-20 |
EP0130967A1 (en) | 1985-01-09 |
JPS6036310A (ja) | 1985-02-25 |
FI77634B (fi) | 1988-12-30 |
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