KR840006237A - 설포닐 우레아의 제조방법 - Google Patents

설포닐 우레아의 제조방법 Download PDF

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KR840006237A
KR840006237A KR1019830004227A KR830004227A KR840006237A KR 840006237 A KR840006237 A KR 840006237A KR 1019830004227 A KR1019830004227 A KR 1019830004227A KR 830004227 A KR830004227 A KR 830004227A KR 840006237 A KR840006237 A KR 840006237A
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푀리 베르너 (외 2)
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아놀드 자일러, 에른스트 알테르
시바-가이기 에이·지
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72—Nitrogen atoms
    • C07D213/73—Unsubstituted amino or imino radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/36—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/62—Oxygen or sulfur atoms
    • C07D213/70—Sulfur atoms
    • C07D213/71—Sulfur atoms to which a second hetero atom is attached
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72—Nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72—Nitrogen atoms
    • C07D213/74—Amino or imino radicals substituted by hydrocarbon or substituted hydrocarbon radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D521/00—Heterocyclic compounds containing unspecified hetero rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Pest Control & Pesticides (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

내용 없음

Description

설포닐 우레아의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (14)

  1. 다음 식(Ⅱ)의 화합물과 다음 식(Ⅲ)의 화합물을 염기의 존재하에 반응시켜서 다음 식(I)의 화합물을 제조하는 방법.
  3. A는 C3-6알키닐라디칼, 할로겐, C1-4알콕시, C1-4알킬티오, C1-4알킬설피닐, C1-4알킬설포닐, C1-4할로알콕시, C1-4할로알킬티오, C1-4할로알킬설피닐 혹은 C1-4할로알킬설포닐로 치환된 C1-6알킬라디칼, 혹은 C1-6알킬로 치환 혹은 비치환된 C2-4알케닐라디칼 혹은 할로겐, 시아노, 니트로, C1-4알킬, C1-4할로알킬, -X-C1-4알킬, C1-4알콕시카르보닐, 아미노, 모노 혹은 디(C1-4알킬)아미노, 카르바모일, 모노 혹은 디(C1-4알킬)카르바모일, 설파모일, 모노-혹은 디(C1-4알킬) 설파모일라디칼이고, A-X는 아미노라디칼 -NR6R7을 형성하고, E는 메틴 혹은 질소이고,
  4. R1은 수소, 할로겐, C1-4알킬, C1-4알콕시, C1-4할로알킬, C1-4할로알콕시, C2-5알콕시알콕시, C1-5알킬티오, C1-5알킬설피닐 혹은 C1-5알킬설포닐이고, R2는 1-3 할로겐원자로 치환 혹은 비치환된 C1-3알킬 혹은 C1-3알콕시이고, R3는 수소, 할로겐, 아미노기 -NR4R5혹은 1-3 할로겐원자로 혹은 비치환된 C1-3알킬 혹은 메톡시, 에톡시 혹은 1-3 할로겐원자로 치환 혹은 비치환된 C1-4알콕시이고, R4는 수소 혹은 메틸이고, R5는 수소, C1-2알킬 혹은 메톡시이고, R6와R7은 각기 독립하여 수소, C1-4알킬, C3-6알케닐, C3-4알키닐, C3-6알콕시알킬, C1-4시아노알킬 혹은 두기가 질소와 함께 산소, 황을 지니는 5- 혹은 6원소의 포화이고 리환을 형성하고 혹은 -NR8라디칼이 되고, R8은 수소, C1-4알킬 혹은 벤질이고,
  5. X는 산소, 황, 혹은 설피닐 혹은 설포닐로서, 만일 X-A가 C3-4알케닐설피드, -설피닐 혹은 설포닐라디칼이고, R1이 수소, 할로겐, 메틸, 메톡시, 트리플루오로메틸, 니트로, 시아노 혹은 메톡시메틸이면 R2는 C1-2알킬, 알콕시 혹은 메톡시메틸, R3는 메틸 혹은 메톡시가 되어야 한다.
  6. 다음 식(Ⅳ)의 화합물과 다음 식(Ⅴ)의 화합물을 염기의 존재하에 반응시켜서 상기한 식(I)의 화합물을 제조하는 방법.
  8. 상기 식에서 각 치환기는 1항에서 정의한 대로임.
  9. 다음 식(Ⅵ)의 화합물과 다음 식(Ⅴ)의 화합물을 반응시켜서 상기한 식(I)의 화합물을 제조하는 방법.
  11. 상기 식에서,
  12. Rq는 페닐, 할로겐 혹은 C1-4알칼로 치환된 페닐, C1-4알킬, C2-8알콕시알킬이고,
  13. Y는 황 혹은 산소이고, 그 외는 상기한 1항에 정의한 대로임.
  14. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019830004227A 1982-09-08 1983-09-08 설포닐 우레아의 제조방법 KR900005370B1 (ko)

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CH5337/82 1982-09-08
CH533782 1982-09-08
CH5337/82-2 1982-09-08
CH228383 1983-04-28
CH2283/83-8 1983-04-28

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KR840006237A true KR840006237A (ko) 1984-11-22
KR900005370B1 KR900005370B1 (ko) 1990-07-28

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US (2) US4579583A (ko)
EP (1) EP0103543B1 (ko)
KR (1) KR900005370B1 (ko)
AR (1) AR240929A1 (ko)
AU (1) AU576474B2 (ko)
BR (1) BR8304862A (ko)
CA (1) CA1221965A (ko)
DE (1) DE3373901D1 (ko)
ES (1) ES525435A0 (ko)
IL (1) IL69670A (ko)
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IL69670A0 (en) 1983-12-30
US4579583A (en) 1986-04-01
AU576474B2 (en) 1988-09-01
EP0103543A3 (en) 1985-05-15
AU1879883A (en) 1984-03-15
US4579583B1 (ko) 1989-02-14
CA1221965A (en) 1987-05-19
ES8506694A1 (es) 1985-08-01
IL69670A (en) 1987-01-30
BR8304862A (pt) 1984-04-24
PH20984A (en) 1987-06-18
EP0103543A2 (de) 1984-03-21
AR240929A1 (es) 1991-03-27
DE3373901D1 (en) 1987-11-05
US4690707A (en) 1987-09-01
EP0103543B1 (de) 1987-09-30
KR900005370B1 (ko) 1990-07-28
ES525435A0 (es) 1985-08-01
AR240929A2 (es) 1991-03-27

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