KR830007584A - 트리아졸일 펜테놀류의 과학 이성체의 제조방법 - Google Patents

트리아졸일 펜테놀류의 과학 이성체의 제조방법 Download PDF

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Publication number
KR830007584A
KR830007584A KR1019810004924A KR810004924A KR830007584A KR 830007584 A KR830007584 A KR 830007584A KR 1019810004924 A KR1019810004924 A KR 1019810004924A KR 810004924 A KR810004924 A KR 810004924A KR 830007584 A KR830007584 A KR 830007584A
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KR
South Korea
Prior art keywords
general formula
alcohol derivative
aluminum hydride
lithium aluminum
atom
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KR1019810004924A
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English (en)
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KR870001792B1 (ko
Inventor
유지 후나끼
유끼오 요네요시
유끼오 이시구리
가즈오 이즈미
Original Assignee
니시기다 도모스미
스미또모 가가꾸고오교 가부시끼 가이샤
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Priority claimed from JP17770480A external-priority patent/JPH0232249B2/ja
Priority claimed from JP18240780A external-priority patent/JPS57106669A/ja
Application filed by 니시기다 도모스미, 스미또모 가가꾸고오교 가부시끼 가이샤 filed Critical 니시기다 도모스미
Publication of KR830007584A publication Critical patent/KR830007584A/ko
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Publication of KR870001792B1 publication Critical patent/KR870001792B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/12—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647—Triazoles; Hydrogenated triazoles
    • A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
    • C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles

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  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Environmental Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)

Abstract

내용 없음

Description

트리아졸일 펜테놀류의 과학 이성체의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (9)

  1. 일반식(Ⅱ)로 표시되는 트리아졸일 알코올 유도체를 수식수소화 리튬 알루미늄형의 키랄 환워제로 부제 환원시킴을 특징으로 하는 , (-) 또는 (+)의 광학 활성을 가지며 일반식(I)로 표시되는 트리아졸일 알코올 유도체의 제조방법.
    (상기 식에서,
    X는 수소원자 또는 염소 원자를 나타내고, 별표는 부제 탄소 원자를 나타냄).
  2. 제1항에 있어서, 1당량의 수소화 리튬 알루미늄, N-치환 에페드린의 광학 대칭제 중의 하나, 1당량 및 2당량의 N-알킬아닐린으로 부터 제조된, 수식수소화 리튬 알루미늄의 키랄 환원제를 사용함을 특징으로 하는 방법.
  3. 제1항에 있어서, 1당량의 수소화 리튬 알루미늄, 2-N,N-이치환 아미노 -1-페닐에탄올의 광학대칭체중의 하나, 1당량 및 2당량의 N-알킬아닐린으로부터 제조된, 수식수소화리튬 알루미늄의 키랄 환원제를 사용함을 특징으로 하는 방법.
  4. 제1항에 있어서, 1당량의 수소화 리튬 알루미늄, 2내지 3당량의 (-)-또는 (+)-멘톨로부터 제조된, 수식수소화 리튬 알루미늄의 키랄 환원제를 사용함을 특징으로 하는방법.
  5. 일반식(I′)로 표시되는 트리아졸일 알코올 유도체의 라세미체를 광학활성 카르복실산의 반응성 유도체와 반응시켜 두부분 입체 이성체 에스테르를 얻고, 상기 부분 입체 이성체 에스테르 중의 하나를 분리하고, 분리된 에스테르를 가수분해 시킴을 특징으로 하는,(-) 또는 (+)의 광학 활성을 가지며 일반식(I)로 표시는 트리아졸일 알코올 유도체의 제조방법.
    (상기 식에서,
    X는 수소원자 또는 염소원자를 나타내고, 별표는 부제 탄소원자를 나타냄).
  6. 제5항에 있어서, (-)- 또는 (+)-멘톡실아세틸 클로라이드가 광학활성 카르복실산의 반응성 유도체로서 사용됨을 특징으로 하는방법.
  7. (-)의 광학 활성을 가지며 하기 일반식으로 표시되는 트리아졸일 알코올 유도체를 유효 성분으로 함유하는 살균제 조성물을 균에대해 사용함을 특징으로 하는 균의 방제방법.
    (상기 식에서, X는 수소원자 또는 염소원자이고, 별표는 부제 탄소원자를 나타냄).
  8. (+)의 광학 활성을 가지며 하기 일반식으로 표시되는 트리아졸 알코올 유도체를 유효성분으로 함유하는 식물 생장조절제를 식물에 사용함을 특징으로 하는 식물 생장 조절방법.
    (상기 식에서, X는 수소원자 또는 염소원자를 나타내고, 별표는 부제 탄소원자를 나타냄).
  9. (+)의 광학 활성을 가지며 하기 일반식으로 표시되는 트리아졸일 알코올 유도체를 유효성분으로 함유하는 제초제 조성물을 잡초에 대해 사용함을 특징으로 하는 제초방법.
    (상기 식에서, X는 수소원자 또는 염소원자를 나타내고, 별표는 부제 탄소원자를 나타냄)
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019810004924A 1980-12-15 1981-12-15 트리아졸일펜테놀류의 광학 이성체의 제조 방법 KR870001792B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP177704/80 1980-12-15
JP17770480A JPH0232249B2 (ja) 1980-12-15 1980-12-15 Kogakukatsuseitoriazoriruarukoorujudotaiojukoseibuntoshiteganjusurusatsukinzai
JP18240780A JPS57106669A (en) 1980-12-22 1980-12-22 Optically active triazolyl alcohol derivative, its preparation, and plant growth regulator and herbicide containing said derivative as active component
JP182407/80 1980-12-22

Publications (2)

Publication Number Publication Date
KR830007584A true KR830007584A (ko) 1983-11-04
KR870001792B1 KR870001792B1 (ko) 1987-10-12

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Country Link
US (1) US4435203A (ko)
EP (1) EP0054431B1 (ko)
KR (1) KR870001792B1 (ko)
AU (1) AU544099B2 (ko)
BR (1) BR8108116A (ko)
CA (1) CA1172641A (ko)
DE (3) DE3175949D1 (ko)
DK (2) DK160301C (ko)
ES (1) ES8207159A1 (ko)
HU (1) HU187385B (ko)
IL (1) IL64481A0 (ko)
MY (2) MY102225A (ko)
NZ (1) NZ199185A (ko)
RO (3) RO86318B (ko)
SU (1) SU1582987A3 (ko)
YU (1) YU43055B (ko)

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DK102190A (da) 1990-04-25
RO86318A (ro) 1985-03-15
EP0054431B1 (en) 1987-03-04
DK162223C (da) 1992-02-17
SU1582987A3 (ru) 1990-07-30
AU544099B2 (en) 1985-05-16
DK162223B (da) 1991-09-30
MY102222A (en) 1992-05-15
BR8108116A (pt) 1982-09-21
DE3175949D1 (en) 1987-04-09
DE3177314D1 (de) 1996-04-18
AU7792581A (en) 1982-06-24
RO86318B (ro) 1985-03-31
DK160301B (da) 1991-02-25
KR870001792B1 (ko) 1987-10-12
DE3177314T2 (de) 1996-09-19
DK553881A (da) 1982-06-16
CA1172641A (en) 1984-08-14
YU292281A (en) 1983-10-31
NZ199185A (en) 1984-05-31
DK160301C (da) 1991-08-05
RO84279A (ro) 1984-05-23
DE3177274D1 (de) 1992-04-16
RO84279B (ro) 1984-07-30
YU43055B (en) 1989-02-28
DK102190D0 (da) 1990-04-25
ES507883A0 (es) 1982-09-01
US4435203A (en) 1984-03-06
RO89367A (ro) 1986-05-30
ES8207159A1 (es) 1982-09-01
MY102225A (en) 1992-05-15
HU187385B (en) 1985-12-28
EP0054431A1 (en) 1982-06-23
IL64481A0 (en) 1982-03-31

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