KR20230024884A - 헬륨 흐름으로부터 원치않는 성분을 분리하는 방법 및 장치 - Google Patents

헬륨 흐름으로부터 원치않는 성분을 분리하는 방법 및 장치 Download PDF

Info

Publication number
KR20230024884A
KR20230024884A KR1020227038409A KR20227038409A KR20230024884A KR 20230024884 A KR20230024884 A KR 20230024884A KR 1020227038409 A KR1020227038409 A KR 1020227038409A KR 20227038409 A KR20227038409 A KR 20227038409A KR 20230024884 A KR20230024884 A KR 20230024884A
Authority
KR
South Korea
Prior art keywords
cooling
helium
cooling medium
cleaned
heat exchanger
Prior art date
Application number
KR1020227038409A
Other languages
English (en)
Korean (ko)
Inventor
한스피터 빌헬름
엘리아스 마이
프랭크 산더
Original Assignee
린데 크라이오테크니크 아게
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 린데 크라이오테크니크 아게 filed Critical 린데 크라이오테크니크 아게
Publication of KR20230024884A publication Critical patent/KR20230024884A/ko

Links

Images

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/08—Separating gaseous impurities from gases or gaseous mixtures or from liquefied gases or liquefied gaseous mixtures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B23/00—Noble gases; Compounds thereof
    • C01B23/001—Purification or separation processes of noble gases
    • C01B23/0036—Physical processing only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0029—Obtaining noble gases
    • C01B2210/0031—Helium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0045—Oxygen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0046—Nitrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0053—Hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0078—Noble gases
    • C01B2210/0081—Neon
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/02—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/20—Processes or apparatus using other separation and/or other processing means using solidification of components
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/40—Processes or apparatus using other separation and/or other processing means using hybrid system, i.e. combining cryogenic and non-cryogenic separation techniques
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/60—Processes or apparatus using other separation and/or other processing means using adsorption on solid adsorbents, e.g. by temperature-swing adsorption [TSA] at the hot or cold end
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/30—Helium
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00—Processes or apparatus involving steps for recycling of process streams
    • F25J2245/02—Recycle of a stream in general, e.g. a by-pass stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2260/00—Coupling of processes or apparatus to other units; Integrated schemes
    • F25J2260/20—Integration in an installation for liquefying or solidifying a fluid stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/30—Quasi-closed internal or closed external helium refrigeration cycle
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2280/00—Control of the process or apparatus
    • F25J2280/02—Control in general, load changes, different modes ("runs"), measurements

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)
KR1020227038409A 2020-04-07 2021-03-30 헬륨 흐름으로부터 원치않는 성분을 분리하는 방법 및 장치 KR20230024884A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20020159.8 2020-04-07
EP20020159 2020-04-07
PCT/EP2021/025121 WO2021204422A1 (de) 2020-04-07 2021-03-30 Verfahren und vorrichtung zum abtrennen unerwünschter komponenten aus einem helium-strom

Publications (1)

Publication Number Publication Date
KR20230024884A true KR20230024884A (ko) 2023-02-21

Family

ID=70227752

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020227038409A KR20230024884A (ko) 2020-04-07 2021-03-30 헬륨 흐름으로부터 원치않는 성분을 분리하는 방법 및 장치

Country Status (5)

Country Link
EP (1) EP4133228A1 (zh)
JP (1) JP2023520804A (zh)
KR (1) KR20230024884A (zh)
CN (1) CN115362341A (zh)
WO (1) WO2021204422A1 (zh)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61140778A (ja) * 1984-12-12 1986-06-27 株式会社神戸製鋼所 Ｈｅの精製方法
JP3143757B2 (ja) * 1992-03-02 2001-03-07 日本酸素株式会社 ヘリウムガス精製装置及びその運転方法
JP2001248964A (ja) * 2000-03-08 2001-09-14 Sumisho Fine Gas Kk ガス精製装置およびガス精製方法
DE102008053846A1 (de) 2008-10-30 2010-05-06 Linde Ag Verfahren zum Abtrennen unerwünschter Komponenten aus einem Helium-Strom
DE102013012656A1 (de) 2013-07-30 2015-02-05 Linde Aktiengesellschaft Verfahren zum Abtrennen unerwünschter Komponenten aus einem Helium-Strom

Also Published As

Publication number Publication date
EP4133228A1 (de) 2023-02-15
WO2021204422A1 (de) 2021-10-14
JP2023520804A (ja) 2023-05-19
CN115362341A (zh) 2022-11-18

Similar Documents

Publication Publication Date Title
US11619443B2 (en) Method for the production of air gases by the cryogenic separation of air with improved front end purification and air compression
CA2256611C (en) Removing carbon dioxide, ethane and heavier components from a natural gas
US4367082A (en) Air separating system
JPH1024209A (ja) 大気空気を処理するための方法および装置
JP3703933B2 (ja) 窒素生成のための、透過による空気分離方法および装置
US20080202160A1 (en) Method and device for fractionated cryocondensation
EP3671087A1 (en) A method and apparatus for eliminating heat bumps following regeneration of adsorbers in an air separation unit
KR20220150985A (ko) 이산화탄소 회수 장치
JPH07280432A (ja) 空気の蒸留のためのプラント及びその方法
EP0718576A1 (fr) Procédé de séparation d'un mélange gazeux par distillation cryogénique
EP0742040A1 (de) Verfahren und Vorrichtung zur Abgasreinigung mit Wärmeaustauschern
KR20230024884A (ko) 헬륨 흐름으로부터 원치않는 성분을 분리하는 방법 및 장치
US4192661A (en) Adsorbing impurities from cryogenic fluid make-up prior to admixing with feed
WO2017056134A1 (ja) 非炭化水素ガス分離装置及び非炭化水素ガス分離方法
DE102013012656A1 (de) Verfahren zum Abtrennen unerwünschter Komponenten aus einem Helium-Strom
JP4270574B2 (ja) 溶剤の回収装置
DE4017611A1 (de) Verfahren zur verfluessigung von gasen
US3097940A (en) Process for purifying gases
JP2773858B2 (ja) 空気を分離する方法および装置
JP2008279377A (ja) Ｖｏｃ冷却回収装置
JP2000230776A (ja) 低温蒸留による空気分離方法および空気分離装置
JP4819527B2 (ja) 水素圧縮装置
DE19527960C2 (de) Verfahren und Vorrichtung zur Desorption von Adsorbern
EP0046366B1 (en) Production of nitrogen by air separation
US2919555A (en) Apparatus for and method of separating gases