KR20190066919A - Natural preservative composition and wet tissue - Google Patents
Natural preservative composition and wet tissue Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
Description
본 발명은 천연 방부제 조성물에 관한 것으로서, 보다 상세하게는 식물성 추출물로 제조되어 인체에 무해하면서도 방부효과도 우수한 새로운 조성의 천연 방부제 조성물 및 천연 방부제 조성물이 함침된 물티슈에 관한 것이다.The present invention relates to a natural preservative composition, and more particularly to a natural preservative composition and a natural preservative composition impregnated with a novel composition, which is made of a vegetable extract and is harmless to the human body and has excellent preservative effect.
방부제(Antiseptic)는 물질의 부패를 막는 약제로서, 동식물성 유기물이 미생물 등의 작용에 의하여 부패하는 것을 방지하여 유기물을 장기간 보존가능하게 한다. 이러한 방부제는 식품, 화장품, 의약품을 비롯하여, 여성청결티슈, 클렌징 티슈, 물티슈 등과 같은 다양한 생활용품에 거의 대부분 첨가된다. Antiseptic is a medicine to prevent the decay of the material, and it prevents the vegetable organic material from being decayed due to the action of microorganisms and the like, so that the organic material can be preserved for a long time. Such preservatives are mostly added to a variety of daily necessities such as food, cosmetics, medicines, women's cleansing tissues, cleansing tissues, and wet tissues.
한편, 방부제는 방부제 첨가로 인해 제품의 품질을 손상시키지 않아야 하는 것은 물론이며, 인체에 해가 없어야 한다. 그러나 일반적으로 파라벤류, 페녹시에탄올, CMIT(methylchloroisothiazolinone), 또는 MIT(methylisothia-zolonone) 등과 같은 화학물질들이 방부제의 주성분으로 사용되는데, 이러한 화학물질로 제조된 방부제는 피부 알러지를 유발하거나 내성균을 유발하는 문제를 가질 뿐만 아니라, 심지어는 내분비계통의 장애 및 호르몬교란 등을 통한 발암가능성까지 가지고 있다. On the other hand, the preservative should not impair the quality of the product due to the addition of the preservative, and should be harmless to the human body. However, in general, chemicals such as parabens, phenoxyethanol, methylchloroisothiazolinone (CMIT), or methylisothia-zolonone (MIT) are used as main ingredients of preservatives. Preservatives made from these chemicals cause skin allergies or cause resistant bacteria Not only do they have the problem of endocrine disruption, but they also have the potential for carcinogenesis through hormonal disturbances.
특히, CMIT, MIT는 최근 큰 이슈가 된 가습기용 살균제 사건을 통해 알 수 있는 바와 같이, 폐질환을 일으켜서 사망까지 이르게 하는 독성을 가지고 있다. In particular, CMIT, MIT is poisonous, which can lead to lung disease and lead to death, as evidenced by the recent major disinfectant event for humidifiers.
따라서 인체에 대한 독성이나 부작용을 초래하지 않으면서, 강력한 항균 효과와 방부 효과를 가지는 방부제가 요구된다.Therefore, there is a need for a preservative that has a strong antimicrobial effect and a preservative effect without causing toxicity or side effects to the human body.
본 발명은 상기와 같은 문제점에 착안하여 제안된 것으로서, 본 발명의 목적은 식물성 추출물로 제조되어 인체에 무해하면서도 방부효과가 우수하여 안심하여 사용할 수 있는 새로운 조성의 천연 방부제 조성물 및 천연 방부제 조성물이 함침된 물티슈를 제공하는 것이다. Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made keeping in mind the above problems occurring in the prior art, and it is an object of the present invention to provide a novel natural preservative composition and a natural preservative composition, which are made of plant extracts and are harmless to human body, Thereby providing a wet tissue.
본 발명의 일 특징에 따르면, 정제수 50~60부피부, 구연산 38~48부피부, 알로에 추출물 1~2부피부, 탄산수소나트륨 1~2부피부를 포함하는 것을 특징으로 하는 천연 방부제 조성물이 제공된다.According to one aspect of the present invention, there is provided a natural preservative composition comprising 50 to 60 parts of purified water, 38 to 48 parts of citric acid, 1 to 2 parts of aloe extract, 1 to 2 parts of sodium hydrogencarbonate, do.
본 발명의 다른 특징에 따르면, 상기 천연 방부제 조성물이 함침된 물티슈가 제공된다.According to another aspect of the present invention, there is provided a wet tissue impregnated with the natural preservative composition.
이상과 같은 본 발명에 의한 천연방부제 조성물은 식물추출물(구연산)로 제조되기 때문에 인체에 완전히 무해하고, 내균성도 없으며, 종래 화학약품으로 된 방부제에 뒤떨어지지 않는 우수한 방부성을 가진다.Since the natural preservative composition according to the present invention is made of a plant extract (citric acid), the natural preservative composition according to the present invention is completely harmless to the human body, has no fungus, and has excellent antiseptic properties that are not inferior to preservatives made of conventional chemicals.
따라서 본 발명에 의한 천연 방부제 조성물은 물티슈를 비롯하여 가습기, 화장품, 손세정제, 여성청결제, 클렌징티슈 등과 같은 다양한 제품에 안심하고 사용이 가능하다. Therefore, the natural preservative composition according to the present invention can be used safely for various products such as wet tissues, humidifiers, cosmetics, hand cleaners, female cleaners, cleansing tissues and the like.
특히, 본 발명을 사용하여 물티슈를 제조하면, 피부도 보호되고 항균 및 살균성, 즉, 방부성도 우수한 고품질의 안전성이 우수한 물티슈를 제조할 수 있다. Particularly, when a wet tissue is manufactured using the present invention, it is possible to manufacture a wet tissue having excellent safety and high quality, which is also protected against skin and has antibacterial and bactericidal properties, that is, antiseptic properties.
이하에서 본 발명을 좀 더 구체적으로 설명한다. Hereinafter, the present invention will be described in more detail.
본 발명의 제1실시예에 따르면, 본 발명은 정제수, 구연산, 알로에추출물, 탄산수소나트륨을 포함한다. According to a first embodiment of the present invention, the present invention includes purified water, citric acid, aloe extract, sodium hydrogencarbonate.
구연산 추출 매개체인 매실 등은 다른 과실에 비해 약리성이 매우 우수하며, 특히, 항균, 살균작용이 우수하고, 강한 해독작용을 가진다. 이러한 매실의 이러한 효능은 다른 과실에 비해 특히, 구연산이 주성분으로 다량 함유되어 있기 때문인 것으로 분석된다. The citric acid extraction medium, such as plum, has excellent pharmacological properties compared to other fruits, and has excellent antimicrobial and bactericidal action and strong detoxifying action. This effect of the plums is analyzed as compared with other fruits, especially because citric acid is a major component.
본 발명에서 사용되는 구연산은 다음과 같은 방법들로 제조될 수 있다. 첫째는 매실을 20~40일 정도 저장하여 자연숙성시킴으로써 자가분해에 의해 생화학적으로 매실을 구성하고 있는 세포벽을 파괴시킨 다음, 액상분을 짜서 매실추출물을 만든다. 그리고 열수추출 또는 용매추출방법을 통해 매실추출물을 제조할 수도 있으며, 매실을 당류와 함께 발효시킨 다음, 액상분만 수득하는 방법도 있다. 이러한 다양한 방법으로 구연산을 제조할 수 있다. 청매실보다 황매실의 구연산함량이 높기 때문에 바람직하게는 황매실을 사용하여 구연산을 만들어서 사용한다.The citric acid used in the present invention can be prepared by the following methods. First, the plums are stored for about 20 to 40 days and naturally aged to destroy the cell walls constituting plums biochemically by self-degradation, and liquid extracts are made by squeezing liquid components. In addition, the plum extract can be prepared by hot water extraction or solvent extraction method, and fermentation of the plum with the saccharide, followed by obtaining the liquid part. Citric acid can be prepared by various methods. Since citric acid content of sulfuric plum is higher than that of cheongmajil, citric acid is preferably prepared by using sulfur plum.
그리고 알로에는 백합과의 여러해살이 다육식물로 중동, 마다가스카르, 아프리카 남부가 원산지로 약 200여 종류가 있다. 알로에의 잎에서 나오는 즙은 예로부터 약용으로 이용되어 왔다. 알로에는 건위정장, 소화기계통을 비롯한 각 내장에 작용하는 알로인, 알로에 에모딘, 강알칼리성으로서 체질개선 및 항암작용을 갖는 분자량 약 45만의 고분자 다당체, 항균작용을 갖는 알로에틴, 궤양에 작용하는 알로에 울신, 항종양 항바이러스 작용을 갖는 알로미신 등의 다양한 성분을 함유하고 있다. And Aloe is a perennial plant of lily, with about 200 varieties originating in the Middle East, Madagascar and southern Africa. Juice from aloe leaves has long been used medicinally. Aloe is a high molecular polysaccharide having molecular weight of about 450,000 and having alkanoic action, aloe steroid, aloe steroid, aloe steroid, aloe steroid, aloe steroid, and aloe And allomycin having anti-tumor antiviral activity.
또한, 알로에는 피부보습, 피부진정 등과 같은 피부비용효능을 가지므로 본 발명이 물티슈, 손세정제, 화장품용 방부제로 사용되는 경우에는 알로에에 의한 피부보호효과도 얻을 수 있다. In addition, since aloe has skin-potency effects such as skin moisturizing and skin soothing, when the present invention is used as a wet tissue, a hand cleanser, or a cosmetic preservative, a skin-protecting effect of aloe can be obtained.
본 발명에서는 알로에 잎을 잘라서 얻어지는 액즙을 알로에 추출물로 사용한다. In the present invention, a juice obtained by cutting aloe leaves is used as an aloe extract.
탄산수소나트륨은 백색의 결정덩어리 또는 결정성 분말로서 물에 쉽게 녹아 가수분해된다. 탄산수소나트륨 의약품에는 위산과다에 대한 제산제로 사용되며, 커피와 같은 식용품 및 미용제에도 사용되고, 완충제로서의 기능도 한다. 본 발명에서 탄산수소나트륨이 완충제로서의 기능을 한다.Sodium bicarbonate is easily dissolved in water as a white crystal mass or crystalline powder and hydrolyzed. Sodium bicarbonate medicines are used as antacids for gastric hyperproliferesis. They are also used in foods and cosmetics such as coffee, and also serve as buffering agents. In the present invention, sodium hydrogencarbonate functions as a buffer.
이러한 성분들로 구성되는 본 발명은 바람직하게는 정제수 50~60부피부, 구연산 38~48부피부, 알로에 추출물 1~2부피부, 탄산수소나트륨 1~2부피부를 포함한다. 구연산이 38부피부에서 48피부로 포함되며, 이보다 적게 사용될 경우 항균, 살균효과가 미미하여 본 발명에 의한 방부조성물의 방부성이 저하되어 소요되는 수준의 방부효과를 기대하기 곤란하다. The present invention comprising these components preferably comprises 50 to 60 parts of purified water, 38 to 48 parts of citric acid, 1 to 2 parts of aloe extract, 1 to 2 parts of sodium hydrogencarbonate. Citric acid is contained in 38 parts of skin and 48 parts of skin. When it is used less, antibacterial and bactericidal effect is insignificant, so that the preservative of the preservative composition according to the present invention is lowered and it is difficult to expect a required level of preservative effect.
그리고 구연산이 상기 수분으로 포함되는 경우에 알로에추출물과 탄산수소나트륨이 1~2부피부 포함되는 것이 본 발명에 의한 방부제조성물의 방부효과를 비롯한 전체적인 물성이 가장 우수하다.When citric acid is contained as the above-mentioned water, the whole property including the preservative effect of the preservative composition according to the present invention is most excellent when the aloe extract and sodium hydrogen carbonate are contained in 1 to 2 parts of skin.
< 실험예 1 > <Experimental Example 1>
정제수 60부피부, 구연산 38부피부, 알로에추출물 1부피부, 탄산수소나트륨 1부피부를 혼합하여 천연방부제조성물을 제조하였다. 제조한 천연방부제조성물을 물티슈 원단에 함침시키고, 2ㅧ2cm 크기로 절단하여 시료를 만들었다. 시료를 각각 NA배지 및 PDA배지에 올려놓고 30℃ 배양기에서 24시간 배양하면서 미생물의 성장여부를 관찰하였다. 이와 같은 방법으로 각 배지 당 3차에 걸쳐 테스트하였으며, 그 결과는 표 1과 같다. Purified water 60 parts skin, citric acid 38 parts skin, aloe extract 1 part skin, sodium bicarbonate 1 part skin to prepare a natural preservative composition. The prepared natural preservative composition was impregnated into a wet tissue and cut into a size of 2 cm 2 cm to prepare a sample. The samples were placed on NA and PDA media, respectively, and cultured for 24 hours at 30 ° C in an incubator to observe the growth of the microorganisms. Table 3 shows the results of three tests per each culture medium.
NA배지
NA badge
PDA배지
PDA badge
1차
Primary
0
0
0
0
2차
Secondary
0
0
1
One
3차
Third
5
5
0
0
* Grade Description Colony Count* Grade Description Colony Count
0 No Growth No colonies evident 0 No Growth No colonies evident
1 Very Scant Growth 1~10 colonies 1 Very Scant Growth 1 ~ 10 colonies
2 Scant Growth 10~100 colonies 2 Scant Growth 10 ~ 100 colonies
3 Slight Growth 100~300 colonies 3 Slight Growth 100 ~ 300 colonies
4 Light Growth 300~400 colonies 4 Light Growth 300 ~ 400 colonies
5 Heavy Growth Too many colonies to count, but 5 Heavy Growth Too many colonies to count, but
not enough to cover the total area not enough to cover the total area
of sample streak. of sample streak.
6 Growth Blanket of growth evident. 6 Growth Blanket of growth evident.
DIfficult to Distinguish individual DIfficult to Distinguish individual
colonies. Growth may extend beyond colonies. Growth may extend beyond
of streak. of streak.
표 1을 통해 확인할 수 있는 바와 같이, 상기 사항의 조성물을 사용한 1차시료의 모든 배지에서 Grade "0" 판정을 받았다. 즉, 본 발명에 의한 천연방부제조성물이 방부성이 상당히 우수함을 알 수 있다.As can be seen from Table 1, all of the media of the primary sample using the above composition were subjected to a Grade "0" judgment. That is, it can be seen that the natural preservative composition according to the present invention is very excellent in preservability.
< 실험예 2 > <Experimental Example 2>
실험예 1과 같은 조성으로 제조된 천연방부제조성물을 사용하여 세균과 곰팡이균에 대한 항균성 및 항곰팡이성을 테스트하였다. 배지에 세균 및 곰팡이균을 접종하고, 시료를 2㎖ 적하시키고, 30℃ 배양기에서 2~3일 배양한 후, 미생물의 성장여부를 관찰하였다. The antimicrobial and antifungal properties of bacteria and fungi were tested using the natural preservative compositions prepared in the same composition as in Experimental Example 1. Bacteria and fungi were inoculated in the medium, 2 ml of the sample was added dropwise, and the mixture was incubated for 2-3 days in a 30 ° C incubator. Then, the growth of the microorganisms was observed.
일반적으로 항균, 항곰팡이성을 가지는 시료 주변에는 미생물이 성장하지 못하는 inhibition zone이 형성되는데, 본 실험에서는 inhibition zone의 크기를 시료의 항균성, 항곰팡이성의 척도로 삼았다. 그 결과는 표 2와 같다. In general, an inhibition zone is formed in which the microorganism does not grow around the sample having antibacterial and antifungal properties. In this experiment, the size of the inhibition zone was regarded as a measure of the antibacterial and antifungal properties of the sample. The results are shown in Table 2.
Blank
Blank
시료
sample
E. coli
E. coli
-
-
2.35mm
2.35mm
S. aur
S. aur
-
-
1.25mm
1.25mm
* 사용균주 : Escherichia coli, Staphylococcus aureus* Strain used: Escherichia coli, Staphylococcus aureus
이러한 실험결과 표 2를 통해 확인할 수 있는 바와 같이, 본 발명에 의한 천연방부제조성물을 사용한 시료에서 항균 및 항곰팡이성이 모두 우수함을 알 수 있다. As shown in Table 2, it can be seen that the antibacterial and antifungal properties of the samples using the natural preservative composition according to the present invention are excellent.
이상과 같은 조성을 가지는 본 발명에 의한 천연방부제 조성물은 식물추출물을 사용하여 인체에 무해하고, 내균성도 없으며, 방부성도 상당히 우수하다. 본 발명에 의한 천연방부제 조성물은 물티슈용 방부제로 사용이 바람직하나. 가습기, 화장품, 손세정제, 여성청결티슈, 클렌징티슈 등과 같은 다양한 용도의 방부제로 사용이 가능하다. The natural preservative composition according to the present invention having the above composition is harmless to the human body, has no durability, and has excellent antifogging properties by using a plant extract. The natural preservative composition according to the present invention is preferably used as a preservative for wet tissues. It can be used as a preservative for various purposes such as humidifier, cosmetics, hand cleaner, female clean tissue, cleansing tissue and the like.
이하에서는 본 발명의 다른 실시예를 설명하되, 전술한 실시예와 동일한 구성 및 효과에 대해서는 설명을 생략한다.Hereinafter, other embodiments of the present invention will be described, and the same structures and effects as those of the above-described embodiments will not be described.
본 발명의 제2실시예에서는 동백꽃잎추출물, 다시마추출물, 우슬초추출물이 추가가 포함된다.In the second embodiment of the present invention, a camellia flower extract, a seaweed extract, and a hyssop extract are added.
동백꽃잎은 동백꽃의 잎으로서, α-스피나스테롤(α-spinosterol)과 같은 스테로이드(steroid)류, 향균성분인 카멜리딘(camellidin) 등을 함유하고 있으며, 항균, 양혈(凉血) 및 지혈(止血) 작용이 있어 피를 맑게 해주며 피가 나는상처에 효과가 있다. 타박상이나 멍든 것에도 어혈(瘀血)을 제거시키며 타박상을 풀어준다.Camellia petals are leaves of camellia, containing steroids such as α-spinosterol and camellidin, which are antibacterial components. Antibacterial, bloody and hemostatic Hemostatic) action, which cleanses blood and is effective for blooded wounds. It also removes bruises and bruises from bruises and bruises and releases bruises.
다시마는 항균작용을 하는 후코이단(fucoidan), 혈당 강하 및 응고 작용을 하는 라미닌(laminine), 보습 및 습윤제, 보수제로 쓰이는 마니톨(mannitol), 활성산소를 억제시켜 항암작용 및 노화방지와 피부미용 개선 효과를 주는 알긴산(alginic acid) 성분에 의해 다양한 생리기능을 하며, 산성 피부를 알칼리성으로 바꿔준다The sea tangle is composed of fucoidan which is antibacterial, laminin which lowers blood sugar and coagulation, humectant and humectant, mannitol which is used as a repair agent, anti-cancer activity by inhibiting active oxygen, anti-aging and skin beauty improvement Alginic acid has a variety of physiological functions and changes the acidity of the skin to alkaline.
그리고 우슬초(牛膝草)는 비름과로 우경(牛莖) 또는 쇠무릎이라고도 하며, 식품, 의약, 화장품에 널리 사용되어왔고, L-아세트산 보르닐(L-bornyl acetate), isopinocampheol, 피노캠폰(pinocamphone) 등이 들어가 있는 히솝유 (hyssop oil)는 항진균(抗眞菌) 작용이 우수하며, 항균제(抗菌劑), 진경제(鎭痙劑) 효과가 있다.And hyssop (牛 草草) is also known as umbrella, 牛 莖, or knee, and has been widely used in foods, medicines and cosmetics. L-bornyl acetate, isopinocampheol, pinocamphone Hyssop oil is excellent in antifungal action, and has antimicrobial and antispasmodic effects.
본 실시예에서는 이러한 동백꽃잎, 다시마, 우슬초의 유효성분들이 함유된 동백꽃잎추출물, 다시마추출물, 우슬초추출물이 더 포함된다. 이들 동백꽃잎추출물, 다시마추출물, 우슬초추출물은 각각 동백꽃잎, 다시마, 우슬초를 용매추출방법으로 추출한 것이다. In this embodiment, the camellia petal extract, kelp extract, and hyssop extract are further included, which contain such effective components as Camellia petal, Kelp, and Hyssop. These camellia flower extracts, sea tangle extracts, and hyssoproth extracts were obtained by solvent extraction of camellia petals, kelp and hyssop, respectively.
이들 동백꽃잎추출물, 다시마추출물, 우슬초추출물을 각각 1~2부피부 포함되며, 이들이 상기 양 미만으로 포함되면 각 추출물에 의한 효과를 기대하기 곤란하고, 상기 양을 초과하여 추가되면 상대적으로 매실추출물의 양이 과도하게 감소되므로 바람직하지 않다. These camellia flower extracts, sea tangle extracts, and hyssoproth extracts each contain 1 to 2 parts of skin. When these components are contained in an amount less than the above amount, it is difficult to expect the effect of each extract. If the amount exceeds the above amount, The amount is undesirably reduced.
본 실시예에서는 이들 추출물들이 더 함유됨에 따라 각 추출물들에 의한 시너지효과를 얻을 수 있으므로 방부제조성물의 항균, 살균성이 향상되어 방부기능이 더욱 향상된다. 또한, 본 실시예에 의한 방부제 조성물은 피부보호기능도 향상되므로, 물티슈, 손세정제, 화장품, 여성청결제, 클렌징티슈 등과 같이 피부와 직접 닿는 제품에 사용이 한층 더 적합하다. In this embodiment, as the extracts are further contained, the synergistic effect by each of the extracts can be obtained, so that the antimicrobial and bactericidal properties of the preservative composition are improved and the preservative function is further improved. Also, since the preservative composition according to the present embodiment has improved skin protection function, it is more suitable for use in a product directly contacting the skin such as a wet tissue, a hand cleanser, a cosmetic product, a female cleanser, a cleansing tissue and the like.
Claims (3)
Purified water 50 to 60 parts Skin, citric acid 38 to 48 parts Skin, aloe extract 1 to 2 parts Skin, sodium hydrogencarbonate 1 to 2 parts The natural preservative composition is characterized by comprising skin.
[Claim 2] The natural preservative composition according to claim 1, further comprising 1 to 2 parts of a camellia flower extract, a seaweed extract, and a hyssop extract.
A wet tissue impregnated with the natural preservative composition according to claim 1 or 2.
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