KR20040003760A - A manufacturing process of organic fertilizer with an additional humic acid - Google Patents

A manufacturing process of organic fertilizer with an additional humic acid Download PDF

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KR20040003760A
KR20040003760A KR1020020038551A KR20020038551A KR20040003760A KR 20040003760 A KR20040003760 A KR 20040003760A KR 1020020038551 A KR1020020038551 A KR 1020020038551A KR 20020038551 A KR20020038551 A KR 20020038551A KR 20040003760 A KR20040003760 A KR 20040003760A
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humic acid
oil
fertilizer
added
oil cake
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KR1020020038551A
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Korean (ko)
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박준성
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주식회사 삼경화학
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Publication of KR20040003760A publication Critical patent/KR20040003760A/en

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    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B9/00—Screening or protective devices for wall or similar openings, with or without operating or securing mechanisms; Closures of similar construction
    • E06B9/01—Grilles fixed to walls, doors, or windows; Grilles moving with doors or windows; Walls formed as grilles, e.g. claustra
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B9/00—Screening or protective devices for wall or similar openings, with or without operating or securing mechanisms; Closures of similar construction
    • E06B9/01—Grilles fixed to walls, doors, or windows; Grilles moving with doors or windows; Walls formed as grilles, e.g. claustra
    • E06B2009/015—Mounting details

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  • Engineering & Computer Science (AREA)
  • Structural Engineering (AREA)
  • Architecture (AREA)
  • Civil Engineering (AREA)
  • Fertilizers (AREA)

Abstract

PURPOSE: A production method of granular oil cake fertilizer is provided, which is characterized by using humic acid-added binder unlike a conventional binder in forming granules comprising various kinds of oil cakes. Accordingly, the oil cake fertilizer improves soil, promotes the growth of plants, and decreases the use of fertilizers and agricultural chemicals. CONSTITUTION: The humic-acid added oil cake fertilizer is produced by the following steps of: mixing 45% of castor oil cake, 35% of seed oil cake, 10% of bean oil cake and 10% of rice bran oil cake; grinding the mixture to powder with a size of 1.5mm; spraying 10wt.%(based on raw materials) of humic acid-added binder to mixed oil cakes, wherein the humic acid-added binder is obtained by diluting 300g of humic acid with 20L of water to be 0.1wt.%(based on total amounts of oil cakes) of humic acid and adding 10wt.% of prepared humic solution to binders such as molasses, guar gum and carboxymethyl cellulose; forming it to a shape of granule by pelleting machine; cooling at 5deg.C and drying.

Description

휴믹산첨가 혼합유박입상비료의 제조방법{A manufacturing process of organic fertilizer with an additional humic acid}A manufacturing process of organic fertilizer with an additional humic acid}

본 발명은 휴믹산이 첨가된 혼합유박입상비료(이하 '휴믹산 유박비료'라 한다)의 제조방법에 관한 것으로, 보다 상세하게는 아주까리박, 채종박, 야자박, 미강박등의 혼합유박원료를 혼합한 후 펠렛성형과정에서 휴믹산이 첨가된 결착제를 투입하여 냉각 및 건조시켜 비료를 제조함으로써, 토양의 구조를 개선하고 토양을 교정향상시키며, 작물과 미생물의 활력을 촉진시키고, 질소화합물의 용탈을 막아 악취를 경감시키며, 작물의 영양섭취를 최적화시켜 비료와 농약의 사용량을 감소시키는 휴믹산 유박비료의 제조방법에 관한 것이다.The present invention relates to a method for producing a mixed oil thin granular fertilizer (hereinafter referred to as 'humic acid milk fertilizer') in which humic acid is added, and more specifically, mixed mixed milk raw materials such as castor gourd, rapeseed gourd, palm gourd, and rice bran gourd. In the process of pellet molding, the fertilizer added with humic acid is cooled and dried to prepare fertilizers, thereby improving the structure of soils and improving soils, promoting the vitality of crops and microorganisms, and dissolving nitrogen compounds. The present invention relates to a method of preparing humic acid manure fertilizer, which reduces odor and prevents odor and optimizes crop intake.

유박이라 함은 식물의 종실에서 유지를 채취하고 남은 박을 총칭하는 것으로서, 이 유박에는 질소(N), 인산(P2O5), 가리(K2O)성분이 균형있게 함유돼 있고 탄수화물과 단백질등으로 구성돼 유기질비료로 이용되고 있으며, 상기성분외에 미량요소 성분까지 포함되어 있어 작물 생육전반에 효과를 나타내고 유기질비료로서 토양내의 미생물을 활성화시켜 토질을 개선하며, 수확량증대 및 작물의 상품성 향상에도 효과가 있어 유기복합비료로 사용되고 있다.An oil foil is a generic term for the remaining oil from the oilseeds of the plant, which contains balanced amounts of nitrogen (N), phosphoric acid (P 2 O 5 ), and girly (K 2 O). It is composed of protein and is used as organic fertilizer, and it contains microelements in addition to the above ingredients to show the effect on the whole crop growth, and as organic fertilizer, it improves soil quality by activating microorganisms in soil, increasing yield and improving crop's merchandise. It is effective as an organic compound fertilizer.

또한 유박은 지금까지 분상으로 사용되어 왔으나, 시비시의 문제점이나 비바람에 의한 유실등의 문제등이 발생해 최근에는 사용이 편리한 입상형태로 바뀌어 가고 있다.In addition, although oil has been used as a powder until now, problems such as fertilization and loss due to wind and rain have occurred, and in recent years, it has been changed into an easy-to-use granular form.

그러나 이러한 종래의 입상유박비료는 식물의 종실에 유지를 채취하고 남은 박을 원재료로 하여 펠렛 성형과정을 거치면서 식물유박인 상기 원재료에 단순 결착제만이 투입돼 제조되므로 수분함량이 10%정도의 적은 양으로, 토양에 시비되면 유기물이 분해되는 과정에서 가스가 분출될 수 있고 햇빛, 온도, 수분등의 여러요인에 의해 원재료와 결착제가 분리되며, 이때 종래의 결착제는 토양이나 작물에 별다른 영향을 주지 못하고 분해되는데, 특히 분리된 원재료는 유기물이 분해되는 과정에서 발효조건이나 토양수분등이 적당하지 못하면 하우스 시설재배지역등에서는 가스장애로 인한 작물의 생리장애가 발생시키는 등 작물에 피해를 줄 수 있었다.However, the conventional granular fertilizer fertilizer is produced by adding only a simple binder to the raw material of vegetable oil while the oil is taken from the seed of the plant and the remaining gourd as a raw material, followed by pellet molding. In small amounts, when fertilized in soil, gas may be released during the decomposition of organic matter, and raw materials and binders are separated by various factors such as sunlight, temperature, and moisture. In particular, separated raw materials can damage crops such as physiological disorders caused by gas disturbances in house facility cultivation areas if fermentation conditions or soil moisture are not suitable during the decomposition of organic matter. there was.

또한 기존의 입상유박비료는 상기한 바와 같이 제조시 과립의 성형을 용이하게 하기 위해서 결착제가 투입돼 제조되고 있는데, 상기 결착제는 성분상으로 보면 비료로서 별효과가 없는 당밀등의 점성이 높은 재료들로 구성돼 있고, 토양수분이 유기물 분해과정에서 흡수됨으로써 작물에 수분부족현상이 초래될 수 있었다.In addition, the conventional granulated milk fertilizer is prepared by adding a binder to facilitate the molding of granules as described above. The binder is a high viscosity material such as molasses, which has no effect as a fertilizer. The soil moisture was absorbed during the decomposition of organic matter, resulting in water shortage in crops.

상기한 바와 같은 문제점을 해결하기 위한 본 발명의 목적은 아주까리박, 채종박, 야자박, 미강박등의 혼합유박원료를 혼합하여 분쇄과정을 거친 후 입상형성과정인 펠렛성형공정에서 휴믹산이 함유된 결착제를 투입하여 휴믹산 유박비료를제조함으로써, 부수적인 재료인 결착제까지 토양과 작물에 유익한 효과가 있는 휴믹산이 첨가돼 제조되므로 가스장애 현상을 차단할 수 있고, 작물의 수분부족현상과 비료의 과다시비시 발생될 수 있는 농도장애 문제를 방지할 수 있으며, 연작장애와 염류장애를 방지해 토양개량효과를 가져올 수 있고, 작물의 영양섭취를 최적화시켜 비료와 농약의 사용량을 30%까지 감소시키게 되는 휴믹산이 첨가된 혼합유박입상비료의 제조방법을 제공하는데 있다.An object of the present invention for solving the problems as described above is to mix the raw milk raw materials such as castor gourd, rapeseed gourd, palm gourd, rice bran gourd after grinding the granule forming process, the humic acid is contained By manufacturing the humic acid fertilizer by adding the binder, the humic acid, which is beneficial to the soil and crops, is added to the binder, which is an additional material, to prevent gas disturbances, and the lack of water and excessive fertilizer of crops. Concentration problems that can occur during fertilization can be prevented, and soil and salt disorders can be prevented, resulting in soil improvement, and nutrient intake of crops is optimized to reduce the use of fertilizers and pesticides by 30%. It is to provide a method for producing a mixed oil thinning fertilizer to which humic acid is added.

상기한 바와 같은 목적을 달성하기 위한 본 발명의 실시예를 하기에서 보다 상세하게 설명하면 다음과 같다.When explaining the embodiment of the present invention for achieving the above object in more detail as follows.

본 발명에 따른 휴믹산이 첨가된 혼합유박비료 제조방법은 아주까리박 45%, 채종박 35%, 야자박 10%, 미강박 10%의 혼합유박 원재료를 혼합기내에서 고르게 혼합하고 해머밀(Hammer Mill)로 입경 1.5mm 이하로 분쇄하여 분말상태로 만들어 분쇄된 상기 원재료를 펠렛기기에 투입한 후, 300kg의 휴믹산유박비료 제조시 필요한 양인 300g의 휴믹산을 20ℓ의 물에 용해하여 상기 원재료대비 휴믹산의 유효성분량이 0.1% 되도록 한 휴믹산 수용액을 당밀, 구아검, CMS등의 결착제에 상기 결착제총량의 10%를 첨가시키고 휴믹산이 함유된 상기 결착제의 양을 원재료대비 10%가 되도록 하여 스팀기로 펠렛기내의 원재료에 분무하고,Humic acid-added mixed milk fertilizer manufacturing method according to the present invention evenly mixed raw materials of mixed raw milk gourd 45%, rape seed gourd 35%, palm gourd 10%, rice bran 10% in a mixer and hammer mill (Hammer Mill) The raw material was pulverized to a particle size of less than 1.5mm and put into the pellet machine, and then 300g of humic acid, which is required for preparing 300 kg of humic acid fertilizer, was dissolved in 20 l of water, and the effective amount of humic acid compared to the raw materials. The aqueous humic acid solution to 0.1% is added to a binder such as molasses, guar gum and CMS, and 10% of the total amount of the binder is added and the amount of the binder containing humic acid is 10% of the raw materials. To the raw materials of

펠렛기기의 좁은 노즐을 통해 배출된 비료를 과립형으로 형성하는 펠렛성형과정을 거쳐 5℃에서 냉각시키고 건조기로 건조하여 목적지에 시비한다. 이때 상기 혼합유박의 보증성분은 질소전량(T-N) 4%, 인산전량(T-P2O5) 2%, 가리전량(T-K2O) 1%로 하여 성분합량이 7%가 되도록 한다After the pellet forming process to form the fertilizer discharged through the narrow nozzle of the pellet machine into granular form, it is cooled at 5 ° C., dried in a dryer and fertilized at the destination. At this time, the guarantee component of the mixed oil foil is 4% of nitrogen (TN), 2% of phosphate (TP 2 O 5 ) and 1% of gallic acid (TK 2 O) so that the total amount of components is 7%.

상기 본 발명의 실시예에 의한 시비방법은 300평의 농경지에 대하여 무처리구와 기존의 입상유박 처리구, 휴믹산이 첨가된 혼합유박처리구등의 3가지로 구분해, 무처리구를 제외하고 각각 300kg으로 시비량을 정하여 시비하고, 시비후 30일이 경과한 후에 토양의 pH, 유효인산함량, 양이온치환용량(CEC), 마그네슘함량을 분석하였다.The fertilizing method according to the embodiment of the present invention is divided into three types, such as untreated, conventional granular oil-treated, and mixed mixed oil-treated with humic acid, and fertilized by 300 kg, except for untreated. After 30 days of fertilization, the soil pH, effective phosphate content, cation exchange capacity (CEC) and magnesium content were analyzed.

토양의 pH 분석은 토양과 증류수를 1:5의 비율로 희석하여 pH 미터로 분석하였고, 토양의 유효인산함량의 측정은 브레이 1번(Bray No. test)으로 측정하였다.Soil pH analysis was performed by diluting the soil and distilled water at a ratio of 1: 5 and analyzed by a pH meter, and the measurement of the effective phosphorus content of the soil was determined by Bray No. 1 (Bray No. test).

휴믹산 첨가유무에 따른 유박비료 시비 토양의 pH 변화PH Change of Fertilizer Fertilized Soil with and without Humic Acid 무 처리구No treatment 기존 입상유박 처리구Existing granular oil processing 휴믹산첨가 유박처리구Humic Acid Addition Foil Processing Area 토양 pHSoil pH 5.35.3 5.65.6 6.16.1 pH 변화량pH change -- +0.3+0.3 +0.8+0.8

휴믹산 첨가 유박처리구에서 pH 변화량은 +0.8로 기존 입상유박처리구보다 높게 나타나, 약산성 토양에서 유박이 분해되면서 생성되는 유기산과 함께 유기태질소, 인산, 가리성분이 용출되면서 휴믹산성분과 결합돼 pH상승의 효과가 생겼다고 볼 수 있다. 특히 휴믹산은 약알칼리성으로 약산성토양에서 pH를 다소 상승시키는 효과가 있다는 것이 상기 실험결과에 의해 입증된다고 할 수 있다.The pH change in humic acid added humic acid treatment group was +0.8, which was higher than that of conventional granular oil treatment group, and organic nitrogen, phosphoric acid, and garlic acid were eluted together with organic acid produced by decomposing oil foil in weakly acidic soils. Can be seen that. In particular, it can be said that the humic acid is weakly alkaline and has an effect of slightly increasing the pH in the weakly acidic soil.

휴믹산 첨가유무에 따라 토양의 유효인산함량(mg/kg)에 미치는 영향Effect of Humic Acid on Soil Effective Phosphorus Content (mg / kg) 무 처리구No treatment 기존 입상유박 처리구Existing granular oil processing 휴믹산첨가 유박처리구Humic Acid Addition Foil Processing Area 유효인산함량Effective Phosphate Content 6565 7272 8585 유효인산 변화량Effective Phosphate Change -- +7+7 +20+20

휴믹산 첨가 유박처리구에서 유효인산의 함량이 무 처리구에 비해서는 20ppm이 높게 나타났으며, 기존 입상유박처리구와 비교해서는 13ppm이 높게 나타났는데 이는 토양내에서 휴믹산이 고정된 인산을 가용화시켜 유효인산의 함량이 상대적으로 높게 나타나는 것으로서, 이것은 휴믹산이 미생물의 활성을 높이고 유기산의 생성을 용이하게 함으로써 불용화된 성분을 가용화시키는 역할을 담당하고 있음을 나타내는 것이다.The content of effective phosphoric acid in humi acid added oil-treated oil was higher than that of non-treated oil, and it was 13ppm higher than conventional granular oil-treated oil, which was obtained by solubilizing phosphoric acid fixed in humic acid in soil. This relatively high level indicates that humic acid plays a role in solubilizing insoluble components by enhancing microbial activity and facilitating the production of organic acids.

시비토양에서의 양이온치환 용량(CEC)의 변화(cmol/kg)Change in Cationic Replacement Capacity (CEC) in Fertilized Soil (cmol / kg) 무처리구No treatment 기존 입상유박 처리구Existing granular oil processing 휴믹산첨가 유박처리구Humic Acid Addition Foil Processing Area CECCEC 1515 1919 2525 CEC 변화량CEC variation -- +4+4 +10+10

토양에서 유기물이 분해되면서 부식질이 생성되는데, 이것은 작물의 영양분 흡수능력을 나타내는 지표인 양이온 치환용량(CEC)을 상승시키는 효과가 있으며, 특히 휴믹산은 고농축된 부식산의 일종으로 보비력을 높이는등의 토양개량효과가 있다.The decomposition of organic matter in the soil produces humus, which increases the cation substitution capacity (CEC), which is an indicator of the nutrient absorption capacity of crops. In particular, humic acid is a type of highly concentrated humic acid. There is an improvement effect.

상기 실험결과에서 볼 수 있듯이 휴믹산첨가 유박처리구가 무처리구나 기존 입상유박처리구보다 양이온치환용량(CEC)이 현저히 높게 나타난 것으로 보아 휴믹산이 첨가된 유박비료가 작물의 영양분흡수능력을 높이는 효과가 크다고 볼 수있다As can be seen from the above experimental results, the humic acid-added milk meal treated group had no higher cation exchange capacity (CEC) than the non-treated or conventional granulated milk treated group. have

토양에서의 마그네슘의 함량(cmol/kg)Magnesium content in soil (cmol / kg) 무처리구No treatment 기존 입상유박처리구Existing granular oil processing equipment 휴믹산첨가 유박처리구Humic Acid Addition Foil Processing Area 마그네슘 함량Magnesium content 1.81.8 2.02.0 2.22.2 마그네슘 변화량Magnesium Variation -- +0.2+0.2 +0.4+0.4

상기한 실험결과에서 보면 휴믹산첨가 유박처리구가 무처리구나 기존 입상유박처리구보다 마그네슘함량이 높게 나타났으며 이는 휴믹산첨가 유박비료가 토양에서 마그네슘함량을 증대시킬 수 있음을 나타내주는 증거라고 할 수 있다.In the above experimental results, the humic acid-added oil-treated manure showed higher magnesium content than the untreated or conventional granular oil-treated oil, which is evidence that the humic acid-added oil fertilizer could increase the magnesium content in the soil.

또한 휴믹산은 구용성 마그네슘이나 난용성 마그네슘의 형태를 작물이 수용하기 쉬운 형태로 만들어주는 효과가 있다고도 볼 수 있다.Humic acid also has the effect of making soluble magnesium or poorly soluble magnesium into an acceptable form for crops.

기존 유박비료처리구와 휴믹산첨가 유박비료처리구의 상승효과 비교Comparison of the synergistic effect between the conventional milk fertilizer treatment and the humic acid added oil 기존 입상유박 처리구Existing granular oil processing 휴믹산첨가 유박처리구Humic Acid Addition Foil Processing Area 비 고Remarks PH 상승효과PH synergy ++++ ++++ + : 효과가 약간있음++ : 효과가 있음+++ : 효과가 매우큼+: Slightly effective ++: effective +++: very effective 유효인산 상승효과Effective Phosphorus Synergy ++++ ++++++ CEC 상승효과CEC synergy ++++ ++++++ 마그네슘 상승효과Magnesium synergistic effect ++ ++++

본 발명은 상기 표에서 나타난 바와 같이 휴믹산첨가 유박비료 처리구가 기존 입상유박비료 처리구에 비해서 상대적으로 각 성분별 상승효과가 큰 것으로 나타났는데, 이는 유기물의 분해시 발생되는 유기산이 휴믹산과 결합되어 토양산성화를 방지하는 것이며, 미생물의 활성을 증대시켜 각종 불용성 영양분을 가용화 시키는 등 휴믹산이 첨가된 유박비료가 기존 유박비료에 비해 시비에 따른 뛰어난 토양개량효과를 얻을 수 있음을 입증하는 것이다.The present invention showed that the humic acid-added milk fertilizer treatment group has a greater synergistic effect for each component as compared to the conventional granular milk fertilizer treatment group, which is combined with humic acid and soil acidification. To improve the microbial activity, solubilizing various insoluble nutrients, such as humic acid added fertilizer fertilizer is proved that the superior soil improvement effect according to the fertilizer can be obtained.

상기한 바와 같은 결과를 종합적으로 비교ㆍ검토하여 볼때,When comparing and reviewing the results as described above comprehensively,

본 발명은 입상형태로 제조되므로 입자내부에 형성되는 기공에 의한 모세관현상으로 수분의 보유가 가능하게 돼 유박을 분해하는 미생물의 활성을 높일 수 있는 효과가 있고, 유박과 휴믹산이 서로 유기적으로 결합돼 작물에 필요한 만큼의 성분이 공급되고 우수한 보비력을 지니고 있어 공급된 후 잔존하는 양분의 유실을 막을 수 있으며, 연작장애와 염류장애를 방지해 토양환경 개선효과를 가져올 수 있고, 병충해 및 부작용을 경감시켜 주는등의 다양한 효과가 있다.Since the present invention is manufactured in a granular form, the capillary phenomenon caused by the pores formed in the particles enables the retention of moisture, thereby increasing the activity of microorganisms that break down the oil foil, and the oil foil and the humic acid are organically combined with each other. It is supplied with as many ingredients as needed for crops and has excellent binding power to prevent the loss of nutrients remaining after being supplied, and to prevent soil disorders and salt disorders, and to improve the soil environment, and to reduce pests and side effects. There are various effects such as giving.

Claims (1)

혼합유박원료를 혼합하여 입경 1.5mm로 분쇄하는 과정을 거친 후 펠렛기에 투입하여 입상비료를 성형하게 되는 혼합유박비료의 제조방법에 있어서,In the method of manufacturing a mixed milk fertilizer is mixed with the mixed milk raw material raw material and then pulverized to a particle diameter of 1.5mm and put into a pellet machine to form a granular fertilizer, 상기 분쇄과정을 거친 혼합유박 원재료를 펠렛기에 투입한 후 상기 원재료대비 유효성분량이 0.1% 되도록 한 휴믹산을 물에 용해시킨 휴믹산수용액을 결착제 대비 10%로 하여 결착제에 첨가시키고, 상기 휴믹산함유 결착제의 성분량을 원재료대비 10%로 하여 스팀기로 펠렛기내의 원재료에 분무하는 과정을 거치게 되는 것을 특징으로 하는 휴믹산 첨가 혼합유박입상비료의 제조방법.After adding the mixed oil and milk raw materials passed through the pulverization process to a pellet machine, the humic acid aqueous solution in which the humic acid in which the effective amount is 0.1% compared to the raw material is dissolved in water is added to the binder as 10% of the binder, and the humic acid-containing binder is added. A method of producing a humic acid-added mixed oil thinning fertilizer, characterized in that the amount of the agent is 10% of the raw material, and is sprayed onto the raw material in the pellet machine with a steam machine.
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KR101346599B1 (en) * 2012-11-21 2014-01-16 주식회사 이앤티 Processing method of organic fertilizer of pellet type
CN103936473A (en) * 2013-01-18 2014-07-23 黄泉水 Humic acid soil conditioner (fertilizer) for planting green food
TWI472505B (en) * 2013-11-21 2015-02-11 Wellness Top Technology Co Ltd Organic fertilizer against pathogenic bacteria and its manufacturing method
KR101688766B1 (en) * 2016-03-31 2017-01-03 경상남도 Organic fertilizer including Thermal polyaspartic acid manufacturing method

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102763685A (en) * 2012-07-17 2012-11-07 中国热带农业科学院热带生物技术研究所 Banana vascular wilt resistant fermentation liquor and preparation method and application thereof
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CN103936473A (en) * 2013-01-18 2014-07-23 黄泉水 Humic acid soil conditioner (fertilizer) for planting green food
TWI472505B (en) * 2013-11-21 2015-02-11 Wellness Top Technology Co Ltd Organic fertilizer against pathogenic bacteria and its manufacturing method
KR101688766B1 (en) * 2016-03-31 2017-01-03 경상남도 Organic fertilizer including Thermal polyaspartic acid manufacturing method

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