KR102304228B1 - 디메틸에테르 반응기의 생성물 스트림에 대한 분리가공방법 - Google Patents

디메틸에테르 반응기의 생성물 스트림에 대한 분리가공방법 Download PDF

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KR102304228B1
KR102304228B1 KR1020167018143A KR20167018143A KR102304228B1 KR 102304228 B1 KR102304228 B1 KR 102304228B1 KR 1020167018143 A KR1020167018143 A KR 1020167018143A KR 20167018143 A KR20167018143 A KR 20167018143A KR 102304228 B1 KR102304228 B1 KR 102304228B1
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stream
dimethyl ether
distillation column
carbon dioxide
condensate
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Korean (ko)
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KR20160106066A (ko
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헬무트 프리츠
안드레아스 페셀
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린데 악티엔게젤샤프트
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1493—Selection of liquid materials for use as absorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/043—Dimethyl ether
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/108—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/502—Carbon monoxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/504—Carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/40—Capture or disposal of greenhouse gases of CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
KR1020167018143A 2014-01-07 2015-01-05 디메틸에테르 반응기의 생성물 스트림에 대한 분리가공방법 Expired - Fee Related KR102304228B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP14000041.5 2014-01-07
EP14000041 2014-01-07
PCT/EP2015/050046 WO2015104238A1 (de) 2014-01-07 2015-01-05 Verfahren zur trenntechnischen bearbeitung eines produktstroms eines dimethyletherreaktors

Publications (2)

Publication Number Publication Date
KR20160106066A KR20160106066A (ko) 2016-09-09
KR102304228B1 true KR102304228B1 (ko) 2021-09-23

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KR1020167018143A Expired - Fee Related KR102304228B1 (ko) 2014-01-07 2015-01-05 디메틸에테르 반응기의 생성물 스트림에 대한 분리가공방법

Country Status (14)

Country Link
US (1) US10246394B2 (https=)
EP (1) EP3092053B1 (https=)
JP (1) JP6621415B2 (https=)
KR (1) KR102304228B1 (https=)
CN (1) CN105873660B (https=)
AU (1) AU2015205697B2 (https=)
BR (1) BR112016015924B1 (https=)
CA (1) CA2930960C (https=)
MX (1) MX365025B (https=)
MY (1) MY189994A (https=)
RU (1) RU2668245C2 (https=)
TW (2) TWI652257B (https=)
WO (1) WO2015104238A1 (https=)
ZA (1) ZA201604051B (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR112016015819B1 (pt) * 2014-01-07 2022-05-31 Linde Aktiengesellschaft Método para o processamento, por tratamento de separação, de uma mistura de gás que é formada a partir de um fluxo de produto de um reator para sintetizar éter de dimetila a partir do gás de síntese
EP3424582A1 (de) * 2017-07-06 2019-01-09 Linde Aktiengesellschaft Verfahren und anlage zur trenntechnischen bearbeitung eines ausgangsgemischs
DE102017010788A1 (de) 2017-11-22 2019-05-23 Linde Aktiengesellschaft Verfahren und Anlage zur Gewinnung von Dimethylether und Kohlendioxid
DE102018003343A1 (de) 2018-04-24 2019-10-24 Linde Aktiengesellschaft Verfahren und Anlage zur Herstellung von Ethanol
US20240375040A1 (en) * 2023-05-09 2024-11-14 Saudi Arabian Oil Company Reactor System having Sorbent to Remove Carbon Dioxide

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19943219A1 (de) 1999-09-09 2001-03-15 Axiva Gmbh Verfahren zur Herstellung von Dimethylether
US20130327086A1 (en) * 2010-10-21 2013-12-12 Bayer Intellectual Property Gmbh Method for the simplified removal of a reaction product from reaction gas mixtures using at least two-fold partial condensation

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JPS4824368B1 (https=) * 1967-03-28 1973-07-20
DK149326C (da) 1984-01-10 1986-09-15 Haldor Topsoe As Fremgangsmaade til fremstilling af katalysatorer til anvendelse ved ethersyntese
DK158221C (da) * 1987-06-30 1990-09-10 Haldor Topsoe As Fremgangsmaade til fremstilling af eddikesyre, metylacetat, eddikesyreanhydrid eller blandinger deraf
DE3817816A1 (de) * 1988-05-26 1989-11-30 Union Rheinische Braunkohlen Verfahren zur herstellung von dimethylether
JPH03181435A (ja) * 1989-12-08 1991-08-07 Kaoru Fujimoto ジメチルエーテルの製造方法
DK171707B1 (da) * 1995-02-03 1997-04-01 Topsoe Haldor As Fremgangsmåde til fremstilling af dimetylæter i brændstofkvalitet
US5685170A (en) 1995-11-03 1997-11-11 Mcdermott Engineers & Constructors (Canada) Ltd. Propane recovery process
JP2001342159A (ja) * 2000-06-01 2001-12-11 Nkk Corp ジメチルエーテルの製造方法
CN1164550C (zh) * 2001-11-07 2004-09-01 中国五环化学工程公司 一种由合成原料气直接制取二甲醚甲醇水溶液吸收工艺
US6458856B1 (en) * 2001-11-07 2002-10-01 Air Products And Chemicals, Inc. Separation process for one-step production of dimethyl ether from synthesis gas
CN1190405C (zh) * 2002-05-15 2005-02-23 中国科学院工程热物理研究所 精制二甲醚同时回收二氧化碳的分离工艺
RU2256645C2 (ru) * 2002-11-28 2005-07-20 Общество с ограниченной ответственностью "Нефте-газо-химические технологии" Способ получения диметилового эфира
US9139503B2 (en) * 2007-09-10 2015-09-22 Lummus Technology Inc. Method for the production of dimethyl ether
CN101215224B (zh) * 2008-01-07 2010-06-02 烟台同业化工技术有限公司 一种低能耗甲醇制二甲醚方法
EP2531482B1 (en) * 2010-02-04 2017-10-11 Haldor Topsøe A/S Process for the preparation of dimethyl ether
EP2555224B1 (en) * 2011-08-04 2019-12-25 Bruker Daltonik GmbH Arrangement for a removable Ion-optical assembly in a mass spectrometer

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19943219A1 (de) 1999-09-09 2001-03-15 Axiva Gmbh Verfahren zur Herstellung von Dimethylether
US20130327086A1 (en) * 2010-10-21 2013-12-12 Bayer Intellectual Property Gmbh Method for the simplified removal of a reaction product from reaction gas mixtures using at least two-fold partial condensation

Also Published As

Publication number Publication date
MX2016007028A (es) 2016-10-05
CN105873660B (zh) 2019-01-11
BR112016015924B1 (pt) 2022-04-05
CA2930960C (en) 2022-07-12
AU2015205697A1 (en) 2016-07-07
EP3092053B1 (de) 2017-10-25
KR20160106066A (ko) 2016-09-09
US20160332945A1 (en) 2016-11-17
MY189994A (en) 2022-03-22
CN105873660A (zh) 2016-08-17
TWI632951B (zh) 2018-08-21
JP6621415B2 (ja) 2019-12-18
RU2668245C2 (ru) 2018-09-27
CA2930960A1 (en) 2015-07-16
AU2015205697B2 (en) 2018-11-15
JP2017503802A (ja) 2017-02-02
TWI652257B (zh) 2019-03-01
TW201532657A (zh) 2015-09-01
US10246394B2 (en) 2019-04-02
ZA201604051B (en) 2019-11-27
TW201531456A (zh) 2015-08-16
BR112016015924A2 (https=) 2017-08-08
MX365025B (es) 2019-05-20
RU2016127563A3 (https=) 2018-08-09
EP3092053A1 (de) 2016-11-16
RU2016127563A (ru) 2018-02-09
WO2015104238A1 (de) 2015-07-16

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