KR102300242B1 - Solid deodorant included pest repellent and its manufacturing method - Google Patents
Solid deodorant included pest repellent and its manufacturing method Download PDFInfo
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- KR102300242B1 KR102300242B1 KR1020190150097A KR20190150097A KR102300242B1 KR 102300242 B1 KR102300242 B1 KR 102300242B1 KR 1020190150097 A KR1020190150097 A KR 1020190150097A KR 20190150097 A KR20190150097 A KR 20190150097A KR 102300242 B1 KR102300242 B1 KR 102300242B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
본 발명은 해충 기피 성분을 포함하는 탈취제 및 그 제조방법에 관한 것으로, 상기 해충 기피 성분을 포함하는 탈취제는 정제수 100중량부에 대하여, 탈취제 34~38 중량부, 젤란검 1.6~2.0 중량부, 천연오일 8~10 중량부, 해충기피제 3~7 중량부, 베타코코인 3~6 중량부, 애플워시 3~6 중량부, 에틸알코올 16~20 중량부를 포함하는 것으로, 본 발명은 인체에 독성을 야기하는 유해성분을 포함하지 않으므로, 인체에 무해하고 친환경적이며, 제품의 안정성 및 신뢰성이 향상된 현저한 효과가 있다.The present invention relates to a deodorant containing a pest repelling component and a method for manufacturing the same, wherein the deodorant containing the pest repelling component is based on 100 parts by weight of purified water, 34 to 38 parts by weight of a deodorant, 1.6 to 2.0 parts by weight of gellan gum, natural Oil 8-10 parts by weight, insect repellent 3-7 parts by weight, beta cocoin 3-6 parts by weight, apple wash 3-6 parts by weight, ethyl alcohol 16-20 parts by weight, the present invention is toxic to the human body Since it does not contain harmful ingredients that cause harm, it is harmless to the human body and eco-friendly, and has a remarkable effect of improving the stability and reliability of the product.
Description
본 발명은 인체에 위해성이 없는 천연식물성 추출물로 제조된 해충 기피제 성분을 포함하는 탈취제에 관한 것으로, 유해한 해충으로부터 인체를 보호하면서, 악취를 제거하는 해충 기피 성분을 포함하는 고체탈취제 및 그 제조방법에 관한 것이다.The present invention relates to a deodorant comprising a pest repellent component prepared from a natural plant extract that is not harmful to the human body, and to a solid deodorant comprising a pest repellent component that removes odor while protecting the human body from harmful pests, and a method for manufacturing the same it's about
일반적으로 탈취제란 냄새를 제거하기 위해서, 악취를 내는 화학 성분을 특정 반응물질로 분해하거나, 흡착해서 중화시키는 형태로 냄새를 제거하는 제품을 뜻한다.In general, a deodorant refers to a product that removes odors in the form of decomposing or adsorbing and neutralizing chemical components that produce odors into specific reactants in order to remove odors.
최근 지카바이러스 등 해충들에 의한 피해가 증가하며, 이에 따라 해충기피제의 중요성 및 필요성이 대두되고있다.Recently, damage caused by pests such as Zika virus is increasing, and accordingly, the importance and necessity of pest repellents are emerging.
그러나, 종래에 사용되는 스프레이형 살충제에는 알레트린, 클로르피리포스라는 독소 등이 포함되어 있고, 이러한 화학물질 중 알레트린은, 비염, 두통 등의 부작용이 있으며, 클로르피리포스는 인지능력장애 등이 나타날 수 있다는 문제점이 있었다.However, spray-type insecticides used in the prior art contain a toxin called allethrin and chlorpyrifos. Among these chemicals, alletrin has side effects such as rhinitis and headache, and chlorpyrifos has cognitive impairment. There was a problem that could appear.
또한, 옷 등에 뿌리는 스프레이형 해충기피제에 포함된 페메트린이라는 성분은 유럽에서 환경호르몬으로 분류되어 금지되고 있으며, 내분비장애 등을 일으키는 등 안정성이 낮다는 문제점이 있었다.In addition, a component called pemethrin contained in a spray-type insect repellent sprayed on clothes, etc. is classified as an environmental hormone and banned in Europe, and there is a problem of low stability, such as causing endocrine disorders.
본 발명은 이를 해결하고자 안출된 것으로, 미생물을 배양하여 제조된 탈취제와 천연식물에서 추출된 오일을 함침하고, 이를 겔화시켜 안정성 및 사용성이 향상된 해충 기피 성분을 포함하는 고체탈취제 및 그 제조방법을 제안하고자 하는 것이다.The present invention has been devised to solve this problem, and it is impregnated with a deodorant prepared by culturing microorganisms and oil extracted from natural plants, and gelled thereto. would like to
본 발명은 해충 기피 성분을 포함하는 고체탈취제 및 그 제조방법에 관한 것으로, 상기 해충 기피 성분을 포함하는 고체탈취제는 정제수 100중량부에 대하여, 탈취제 34~38 중량부, 젤란검 1.6~2.0 중량부, 천연오일 8~10 중량부, 해충기피제 3~7 중량부, 베타코코인 3~6 중량부, 애플워시 3~6 중량부, 에틸알코올 16~20 중량부를 포함하는 것을 특징으로 한다.The present invention relates to a solid deodorant containing a pest repelling component and a method for manufacturing the same, wherein the solid deodorant containing the pest repelling component is based on 100 parts by weight of purified water, 34 to 38 parts by weight of a deodorant, 1.6 to 2.0 parts by weight of gellan gum , 8-10 parts by weight of natural oil, 3-7 parts by weight of insect repellent, 3-6 parts by weight of beta cocoin, 3-6 parts by weight of apple wash, 16-20 parts by weight of ethyl alcohol.
또한, 상기 젤란검과 베타코코인의 비율은 1:2인 것을 특징으로 한다.In addition, the ratio of the gellan gum and beta cocoin is characterized in that 1:2.
또한, 상기 천연오일이 편백 및 측백오일인 경우, 상기 해충기피제는 페퍼민트오일인 것을 특징으로 한다.In addition, when the natural oil is cypress and cypress oil, the insect repellent is peppermint oil.
또한, 상기 천연오일이 라벤다오일인 경우, 상기 해충기피제는 제라늄로즈오일인 것을 특징으로 한다.In addition, when the natural oil is lavender oil, the insect repellent is characterized in that the geranium rose oil.
또한, 상기 해충 기피 성분을 포함하는 고체탈취제 제조방법은, 70~80℃ 온도에서 정제수 100중량부에 대하여, 탈취제 34~38 중량부, 천연오일 8~10 중량부, 해충기피제 3~7 중량부, 베타코코인 3~6 중량부, 애플워시 3~6 중량부, 에틸알코올 16~20 중량부, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2~5 중량부가 배합되어, 2시간 동안 교반되어지는 1차 교반단계와, 100~110℃온도에서 젤란검이 중탕되어 용해되는 젤란검용해단계와, 상기 1차 교반단계를 거쳐 제조된 혼합물과 상기 젤란검용해단계를 거쳐 용해된 액상상태의 젤란검이 교반되는 2차 교반단계와, 상기 2차 교반단계를 거친 탈취제가 -10℃ 온도의 냉각저장고에서 응고되는 응고단계를 포함하는 것을 특징으로 한다.In addition, the solid deodorant manufacturing method comprising the pest repellent component is based on 100 parts by weight of purified water at a temperature of 70 to 80 ° C., 34 to 38 parts by weight of a deodorant, 8 to 10 parts by weight of a natural oil, 3 to 7 parts by weight of a pest repellent , Beta cocoin 3-6 parts by weight, Apple wash 3-6 parts by weight, ethyl alcohol 16-20 parts by weight, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2-5 The mixture prepared through the first stirring step in which parts by weight is blended and stirred for 2 hours, the gellan gum dissolving step in which the gellan gum is melted by boiling at 100 to 110° C., and the first stirring step, and the gellan gum It is characterized in that it comprises a second stirring step in which the gellan gum dissolved through the dissolution step is stirred, and a coagulation step in which the deodorant that has undergone the second stirring step is coagulated in a cooling storage at a temperature of -10°C.
따라서 본 발명은 인체에 독성을 야기하는 유해성분을 포함하지 않으므로, 인체에 무해하고 친환경적이며, 제품의 안정성 및 신뢰성이 향상된 현저한 효과가 있다.Therefore, since the present invention does not contain harmful components that cause toxicity to the human body, it is harmless to the human body and environment-friendly, and there is a remarkable effect of improving the stability and reliability of the product.
또한, 본 발명은 고온다습한 환경 및 여름철 차량내부나, 냉동고, 냉장고와 같은 저온의 환경에서도 모두 사용 가능하도록 마련되어, 사용성이 향상된 현저한 효과가 있다.In addition, the present invention is provided so that it can be used in both high-temperature and high-humidity environments and in a vehicle interior in summer, a freezer, and a low-temperature environment such as a refrigerator, there is a remarkable effect of improved usability.
또한, 본 발명은 탈취효율 및 해충기피효율이 우수한 현저한 효과가 있다.In addition, the present invention has a remarkable effect of excellent deodorization efficiency and insect repellent efficiency.
도1은 한국건설생활환경시험연구원에서 발급된 시험성적서이다.
도2는 본 발명에 따른 해충 기피 성분을 포함하는 고체탈취제 제조방법의 흐름도이다.1 is a test report issued by the Korea Construction Living Environment Testing Institute.
2 is a flowchart of a method for manufacturing a solid deodorant comprising a pest repelling component according to the present invention.
상기의 효과를 달성하기 위한 본 발명은 해충 기피 성분을 포함하는 고체탈취제및 그 제조방법에 관한 것으로서, 본 발명의 기술적 구성을 이해하는데 필요한 부분만이 설명되며 그 이외 부분의 설명은 본 발명의 요지를 흩트리지 않도록 생략될 것이라는 것을 유의하여야 한다.The present invention for achieving the above effect relates to a solid deodorant containing a pest repelling component and a method for manufacturing the same, only the parts necessary for understanding the technical configuration of the present invention are described, and the description of other parts is the gist of the present invention It should be noted that will be omitted so as not to distract from
이하, 본 발명에 따른 해충 기피 성분을 포함하는 고체탈취제에 대해 설명한다.Hereinafter, a solid deodorant comprising a pest repelling component according to the present invention will be described.
본 발명에 따른 해충 기피 성분을 포함하는 고체탈취제는, 정제수 100중량부에 대하여, 탈취제 34~38 중량부, 젤란검 1.6~2.0 중량부, 천연오일 8~10 중량부, 해충기피제 3~7 중량부, 계면활성제 6~12 중량부, 휘산보조제인 에틸알코올 16~20중량부를 포함한다.The solid deodorant comprising a pest repellent component according to the present invention, based on 100 parts by weight of purified water, 34 to 38 parts by weight of a deodorant, 1.6 to 2.0 parts by weight of gellan gum, 8 to 10 parts by weight of natural oil, 3 to 7 parts by weight of an insect repellent parts, 6 to 12 parts by weight of surfactant, and 16 to 20 parts by weight of ethyl alcohol as a volatilization aid.
상기 정제수는, 각종 성분들을 용해시키는 역할을 한다.The purified water serves to dissolve various components.
이어서, 본 발명에서 사용되는 상기 탈취제는 친환경 탈취제로, 상기 탈취제는 유기산 생성 미생물을 이용하여 균주를 배양한 후, 균체를 제거한 배양액에 재차 이종의 미생물을 배양한 배양액이다.Subsequently, the deodorant used in the present invention is an eco-friendly deodorant, and the deodorant is a culture solution obtained by culturing a strain using an organic acid-producing microorganism, and then culturing a heterogeneous microorganism again in a culture solution from which the cells are removed.
이러한 탈취제가 34중량부 이하로 첨가되면, 탈취력이 떨어지고, 38중량부를 초과하게되면, 비교적 해충 기피제가 소량 첨가되어지므로 해충기피 효과가 낮아지는 문제점이 있다.When the deodorant is added in an amount of 34 parts by weight or less, the deodorizing power is lowered, and when it exceeds 38 parts by weight, there is a problem in that a relatively small amount of the pest repellent is added, so that the insect repellent effect is lowered.
더욱 상세하게, 상기 탈취제는, (a) 유기산 생성 미생물을 배양액의 pH가 3~5일 때까지 배양하는 단계, (b) 상기 배양액에서 균체를 제거한 다음, 배양 배지를 첨가하고, pH를 9~10으로 조정한 후, 바실러스 속 (Bacillus sp), 아스페르기루스 속(Aspergillus sp) 및 니트로소모나스 속(Nitrosomonas sp)으로 구성된 군에서 선택되는 하나 이상의 미생물을 접종하여 배양하는 단계, (c) 상기 배양액의 pH가 8~85일 때 배양액의 pH를 115~12로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계, (d) 상기 배양액의 pH가 10~105일 때 배양액의 pH를 135~14로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계 및 (e) 상기 배양액의 pH가 12~14일 때 배양을 멈추고 소취제를 수득하는 단계를 거쳐 제조되어진다.More specifically, the deodorant is, (a) culturing the organic acid-producing microorganism until the pH of the culture medium is 3 to 5, (b) removing the cells from the culture medium, then adding the culture medium, and adjusting the pH to 9 ~ After adjusting to 10, inoculating and culturing one or more microorganisms selected from the group consisting of Bacillus sp, Aspergillus sp and Nitrosomonas sp, (c) When the pH of the culture medium is 8 to 85, the pH of the culture medium is adjusted to 115 to 12, a culture medium is added, and one or more microorganisms selected from the group consisting of Bacillus genus, Aspergillus genus and Nitrosomonas genus The step of culturing by inoculating additionally, (d) adjusting the pH of the culture medium to 135 to 14 when the pH of the culture medium is 10 to 105, then adding the culture medium, Bacillus genus, Aspergillus genus and nitro It is prepared through the steps of culturing by additionally inoculating one or more microorganisms selected from the group consisting of the genus Somonas and (e) stopping the culture when the pH of the culture solution is 12 to 14 and obtaining a deodorant.
다음으로, 상기 젤란검은 식물성 겔화제로서, 본 발명의 탈취제를 고체화시키는 것으로, 상기 젤란검이 1.6중량부 이하로 첨가되면 탈취제의 고형화가 불완전해지며, 2중량부를 초과하게 되면, 탈취제의 증발속도가 느려서 탈취 및 해충기피효과가 감소하는 문제점이 있다.Next, the gellan gum is a vegetable gelling agent and solidifies the deodorant of the present invention. When the gellan gum is added in an amount of 1.6 parts by weight or less, the solidification of the deodorant is incomplete, and when it exceeds 2 parts by weight, the evaporation rate of the deodorant There is a problem in that the deodorization and insect repelling effect is reduced because the speed is slow.
상기 계면활성제는, 정제수에 다른 성분들이 용해되는 용해도를 증가시키는 역할을 하는 것으로, 상기 계면활성제가 6중량부 이하로 첨가되면, 용해도가 저하되고, 12중량부를 초과하게 되면 탈취력이 떨어지고 기포(거품)가 발생할 우려가 있다.The surfactant serves to increase the solubility of other components dissolved in purified water, and when the surfactant is added in an amount of 6 parts by weight or less, the solubility decreases, and when it exceeds 12 parts by weight, the deodorizing power decreases and bubbles (bubbles) ) may occur.
본 발명에서는 계면활성제로서 베타코코인과 애플워시를 혼합하여 사용하였으며, 베타코코인 3~6중량부와 애플워시 3~6중량부가 포함되도록 한다.In the present invention, a mixture of beta cocoin and apple wash was used as a surfactant, and 3 to 6 parts by weight of beta cocoin and 3 to 6 parts by weight of apple wash were included.
특히, 상기 베타코코인은, 본 발명의 탈취제가 젤란검에 의해 겔화되는 것을 돕는 역할을 한다.In particular, the beta cocoin serves to help the deodorant of the present invention to be gelled by gellan gum.
더욱 상세하게는, 젤란검은 고형화 과정에서 양이온 물질을 필요로하며, 이러한 베타코코인은 양이온 물질로써, 상기 젤란검과 베타코코인의 비율이 1:2일 경우 가장 안정적인 겔화가 진행된다.More specifically, gellan gum requires a cationic material in the solidification process, and beta-cocoin is a cationic material. When the ratio of gellan gum to beta-cocoin is 1:2, the most stable gelation proceeds.
이에 따라 본 발명은 고온고습한 환경에서도 적용가능한 고형안정성을 확보하게 된다.Accordingly, the present invention secures solid stability applicable even in a high-temperature, high-humidity environment.
한편, 상기 에틸알코올(ethyl alcohol)은 휘산보조제의 역할을 하며, 상기 에틸알코올이 16중량부 이하로 첨가되면, 본 발명의 탈취제가 충분히 휘산되지 못하여 탈취 및 해충 기피 효과가 낮아지며, 20중량부를 초과하게 되면, 알코올 향이 너무 강하여 사용자가 불쾌함을 느끼는 문제점이 발생한다.On the other hand, the ethyl alcohol (ethyl alcohol) serves as a volatilization aid, and when the ethyl alcohol is added in an amount of 16 parts by weight or less, the deodorant of the present invention does not sufficiently volatilize, and the deodorization and insect repelling effect is lowered, and the effect is lower than 20 parts by weight When this is done, there is a problem that the user feels uncomfortable because the alcohol smell is too strong.
상기 천연오일은, 100%순도를 가지는 것으로, 본 발명의 탈취제에 향을 향상시키는 역할을 한다.The natural oil, having 100% purity, serves to improve the flavor of the deodorant of the present invention.
상기 천연오일로는, 라벤다오일, 편백오일, 측백오일이 사용되며, 상기 천연오일을 8중량부 이하로 첨가하게 되면, 향이 약해지고, 10중량부를 초과하게 되면, 필요 이상의 사용량을 사용하게 되므로 가격경쟁력이 낮아진다는 문제점이 발생한다.As the natural oil, lavender oil, cypress oil, and chrysanthemum oil are used. When the natural oil is added in an amount of 8 parts by weight or less, the flavor is weakened, and when it exceeds 10 parts by weight, more than necessary amount is used, so price competitiveness There is a problem that this is lowered.
또한, 상기 해충기피제는, 해충을 퇴치하는 역할을 하는 것으로, 상기 해충기피제를 3중량부 이하로 첨가하게 되면, 해충이 싫어하는 냄새가 약해져 해충 퇴치 효과가 감소되며, 7중량부를 초과하게 되면, 겔안정성이 저하되는 문제점이 발생한다.In addition, the pest repellent serves to exterminate pests, and when the pest repellent is added in an amount of 3 parts by weight or less, the odor that pests hate is weakened and the pest repelling effect is reduced, and when it exceeds 7 parts by weight, the gel There is a problem that stability is lowered.
상기 해충기피제로는 100% 순도를 가지는 제라늄로즈오일, 페퍼민트오일이 사용되어질 수 있으며, 상기 해충기피제가 7중량부를 초과하게 되면, 천연오일을 더 추가하여도 해충퇴치 효과가 상승하지 않으며, 제조 원가는 높아지게 되므로 제조효율이 떨어지게 된다. As the pest repellent, geranium rose oil and peppermint oil having 100% purity may be used. increases, so the manufacturing efficiency decreases.
한편, 상기 천연오일의 종류에 따라 해충기피제로 사용되는 오일의 종류가 달리되며, 이하에서는 천연오일로서 라벤다오일, 편백오일, 측백오일이 사용됨에 따른 본 발명의 실시례를 설명한다.On the other hand, the type of oil used as a pest repellent is different depending on the type of the natural oil. Hereinafter, an embodiment of the present invention in which lavender oil, cypress oil, and cypress oil are used as natural oils will be described.
제1 제조 실시례로서, 상기 천연오일이 라벤다오일인 경우, 상기 해충기피제로는 제라늄로즈오일이 사용되며, 상기 라벤다오일과 제라늄로즈오일의 향취가 잘 어울려 제품의 완성도가 향상되는 효과를 가진다.As a first manufacturing embodiment, when the natural oil is lavender oil, geranium rose oil is used as the insect repellent, and the fragrance of the lavender oil and geranium rose oil goes well with the lavender oil.
상세하게, 제1 제조 실시례에 따른 탈취제는, 정제수 100중량부에 대하여, 탈취제 34~38 중량부, 젤란검 1.6~2.0, 천연오일로서 라벤다오일 8~10 중량부, 해충기피제로서 제라늄로즈오일 3~7 중량부, 계면활성제인 베타코코인 3~6중량부, 계면활성제인 애플워시 3~6중량부, 휘산보조제인 에틸알코올 16~20중량부를 포함한다.In detail, the deodorant according to the first manufacturing example is, based on 100 parts by weight of purified water, 34 to 38 parts by weight of a deodorant, 1.6 to 2.0 parts by weight of gellan gum, 8 to 10 parts by weight of lavender oil as a natural oil, and geranium rose oil as an insect repellent. 3-7 parts by weight, 3-6 parts by weight of beta cocoin as a surfactant, 3-6 parts by weight of apple wash as a surfactant, and 16-20 parts by weight of ethyl alcohol as a volatilization aid.
덧붙여, 제2 제조 실시례로서, 천연오일이 편백 및 측백오일인 경우, 상기 해충기피제로는 페퍼민트오일이 사용되며, 상기 편백 및 측백오일은 페퍼민트오일과 향취가 잘 어울려 제품의 완성도가 향상되는 효과를 가진다.In addition, as a second manufacturing embodiment, when the natural oil is cypress and cypress oil, peppermint oil is used as the insect repellent, and the cypress and arborvitae oil go well with peppermint oil to improve the product's completeness. have
상세하게, 제2 제조 실시례에 따른 탈취제는, 정제수 100중량부에 대하여, 탈취제 34~38 중량부, 젤란검 1.6~2.0, 천연오일로서 편백오일 또는 측백오일 8~10 중량부, 해충기피제로서 페퍼민트오일 3~7 중량부, 계면활성제인 베타코코인 3~6중량부, 계면활성제인 애플워시 3~6중량부, 휘산보조제인 에틸알코올 16~20중량부를 포함한다.In detail, the deodorant according to the second manufacturing embodiment is, based on 100 parts by weight of purified water, 34 to 38 parts by weight of a deodorant, 1.6 to 2.0 parts by weight of gellan gum, 8 to 10 parts by weight of cypress oil or cypress oil as a natural oil, as a pest repellent It contains 3-7 parts by weight of peppermint oil, 3-6 parts by weight of beta cocoin as a surfactant, 3-6 parts by weight of apple wash as a surfactant, and 16-20 parts by weight of ethyl alcohol as a volatilization aid.
이상과 같은 조성물로 제조된 본 발명의 해충 기피 성분을 포함하는 고체 탈취제는 암모니아 및 트리메틸아민에 대한 탈취력을 90% 이상 확보하는 효과를 가진다.The solid deodorant comprising the pest repelling component of the present invention prepared with the composition as described above has the effect of securing 90% or more of deodorizing power against ammonia and trimethylamine.
한편, 본 발명의 해충 기피 성분을 포함하는 고체탈취제는 정제수 100중량부에 대하여, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2~5 중량부를 더 포함하는 것을 특징으로 한다.On the other hand, the solid deodorant containing the pest repellent component of the present invention, 1,3,5-tris (2-hydroxyethyl) hexahydro-1,3,5-triazine 2 to 5 parts by weight with respect to 100 parts by weight of purified water. characterized in that
상기 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine의 카스번호(CAS no)는 4719-04-4이며, 상기 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine이 더 포함됨에 따라 본 발명의 탈취제는 황화수소 및 메틸머캅탄에 대한 탈취력을 90% 이상 확보하는 효과를 가진다.The Cas number (CAS no) of 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine is 4719-04-4, and the 1,3,5-tris(2-hydroxyethyl) As hexahydro-1,3,5-triazine is further included, the deodorant of the present invention has an effect of securing 90% or more of deodorizing power for hydrogen sulfide and methyl mercaptan.
이하에서는 본 발명의 해충 기피 성분을 포함하는 고체탈취제가 제조되는 고체탈취제 제조방법에 대해 간략하게 설명하고자 한다.Hereinafter, a method for preparing a solid deodorant comprising a pest repelling component of the present invention is briefly described.
도2에 도시된 바와 같이, 상기 고체탈취제는, 1차 교반단계(S100), 젤란검용해단계(S200), 2차 교반단계(S300), 응고단계(S400)를 순차적으로 거쳐 제조된다.As shown in FIG. 2, the solid deodorant is manufactured through a first stirring step (S100), a gellan gum dissolving step (S200), a second stirring step (S300), and a coagulation step (S400) sequentially.
먼저, 1차 교반단계(S100)란, 70~80℃ 온도에서, 정제수 100중량부, 탈취제 34~38 중량부, 천연오일 8~10 중량부, 해충기피제 3~7 중량부, 베타코코인 3~6 중량부, 애플워시 3~6 중량부, 에틸알코올 16~20 중량부, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2~5 중량부가 배합되어, 2시간 동안 교반되어지는 단계이다.First, the first stirring step (S100) is, at a temperature of 70-80° C., 100 parts by weight of purified water, 34-38 parts by weight of a deodorant, 8-10 parts by weight of natural oil, 3-7 parts by weight of a pest repellent, 3 parts by weight of beta cocoin ~6 parts by weight, apple wash 3-6 parts by weight, ethyl alcohol 16-20 parts by weight, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2-5 parts by weight are blended, It is a step that is stirred for 2 hours.
상기 1차교반단계에서 각각의 성분들이 교반되는 온도가 70℃ 이하일 경우에는 각각의 성분들이 정제수에 용해되는 용해도가 떨어지며, 80℃를 초과할 경우에는 에너지가 낭비된다는 문제점이 있다.When the temperature at which each component is stirred in the first stirring step is below 70°C, the solubility of each component dissolved in purified water decreases, and when it exceeds 80°C, there is a problem in that energy is wasted.
이어서, 젤란검용해단계(S200)는, 100~110℃온도에서 젤란검이 중탕되어 용해되는 단계이다.Next, the gellan gum dissolving step (S200) is a step in which the gellan gum is melted by boiling at a temperature of 100 to 110°C.
상기 젤란검용해단계에서, 젤란검이 중탕되는 온도가 100℃ 이하일 경우에는 젤란검이 충분히 용해되지 않고, 110℃를 초과할 경우에는 에너지가 낭비된다는 문제점이 있다.In the gellan gum dissolving step, when the temperature at which the gellan gum is bathed is 100° C. or less, the gellan gum is not sufficiently dissolved, and when it exceeds 110° C., there is a problem in that energy is wasted.
다음으로, 2차 교반단계(S300)는, 상기 1차 교반단계(S100)를 거쳐 제조된 혼합물과 상기 젤란검용해단계(S200)를 거쳐 용해된 액상상태의 젤란검이 교반되는 단계이다.Next, the second stirring step (S300) is a step in which the mixture prepared through the first stirring step (S100) and the gellan gum dissolved through the gellan gum dissolving step (S200) are stirred.
상기 2차 교반단계에서, 상기 혼합물과 젤란검이 교반되면서 겔화가 진행된다.In the second stirring step, gelation proceeds while the mixture and gellan gum are stirred.
마지막으로, 응고단계(S400)는 2차 교반단계를 거친 탈취제가 -10℃ 온도의 냉각저장고에서 응고되는 단계이다.Finally, the coagulation step (S400) is a step in which the deodorant that has undergone the secondary stirring step is coagulated in a cooling storage at a temperature of -10°C.
본 발명의 탈취제는 상기 응고단계를 거쳐 완전하게 고체화되어 진다.The deodorant of the present invention is completely solidified through the coagulation step.
이러한 단계를 거쳐 제조된 본 발명의 해충 기피 성분을 포함하는 고체탈취제는 인체에 독성을 야기하는 유해성분을 포함하지 않으므로, 인체에 무해하고 친환경적이며, 고온다습한 환경 및 여름철 차량내부나, 냉동고, 냉장고와 같은 저온의 환경에서도 모두 사용 가능하도록 마련되어, 사용성이 향상된 현저한 효과가 있다.The solid deodorant containing the pest repelling component of the present invention manufactured through these steps does not contain harmful components that cause toxicity to the human body, so it is harmless to the human body and eco-friendly, and in a high-temperature and high-humidity environment and in the interior of a vehicle or a freezer in summer, It is provided so that it can be used even in a low-temperature environment such as a refrigerator, and there is a remarkable effect of improved usability.
상술한 바와 같이, 본 발명에 의한 해충 기피 성분을 포함하는 고체탈취제를 상기의 바람직한 실시 예를 통해 설명하고, 그 우수성을 확인하였지만 해당 기술분야의 당업자라면 하기의 특허청구범위에 기재된 본 발명의 사상 및 영역으로부터 벗어나지 않는 범위 내에서 본 발명을 다양하게 수정 및 변경시킬 수 있음을 이해할 수 있을 것이다.As described above, the solid deodorant comprising a pest repellent component according to the present invention has been described through the above preferred embodiment, and its excellence has been confirmed, but those skilled in the art will appreciate the spirit of the present invention described in the claims below. And it will be understood that various modifications and variations of the present invention can be made without departing from the scope thereof.
Claims (4)
탈취제 34~38 중량부, 젤란검 1.6~2.0 중량부, 편백 및 측백오일8~10 중량부, 페퍼민트오일 3~7 중량부, 베타코코인 3~6 중량부, 애플워시 3~6 중량부, 에틸알코올 16~20 중량부, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2~5 중량부를 포함하되,
상기 탈취제는,
(a) 유기산 생성 미생물을 배양액의 pH가 3~5일 때까지 배양하는 단계, (b) 상기 배양액에서 균체를 제거한 다음, 배양 배지를 첨가하고, pH를 9~10으로 조정한 후, 바실러스 속 (Bacillus sp), 아스페르기루스 속(Aspergillus sp) 및 니트로소모나스 속(Nitrosomonas sp)으로 구성된 군에서 선택되는 하나 이상의 미생물을 접종하여 배양하는 단계, (c) 상기 배양액의 pH가 8~85일 때 배양액의 pH를 115~12로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계, (d) 상기 배양액의 pH가 10~105일 때 배양액의 pH를 135~14로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계 및 (e) 상기 배양액의 pH가 12~14일 때 배양을 멈추고 소취제를 수득하는 단계를 거쳐 제조되는 것을 특징으로 하는 해충 기피 성분을 포함하는 고체탈취제.
With respect to 100 parts by weight of purified water,
34 to 38 parts by weight of deodorant, 1.6 to 2.0 parts by weight of gellan gum, 8 to 10 parts by weight of cypress and cypress oil, 3 to 7 parts by weight of peppermint oil, 3 to 6 parts by weight of beta cocoin, 3 to 6 parts by weight of apple wash, 16-20 parts by weight of ethyl alcohol, including 2-5 parts by weight of 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine,
The deodorant is
(a) culturing the organic acid-producing microorganism until the pH of the culture medium is 3 to 5, (b) removing the cells from the culture medium, adding a culture medium, and adjusting the pH to 9 to 10, Bacillus genus (Bacillus sp), the step of culturing by inoculating one or more microorganisms selected from the group consisting of Aspergillus sp and Nitrosomonas sp, (c) the pH of the culture medium is 8 to 85 After adjusting the pH of the culture medium to 115 to 12 when , (d) when the pH of the culture medium is 10 to 105, after adjusting the pH of the culture medium to 135 to 14, a culture medium is added, and selected from the group consisting of Bacillus genus, Aspergillus genus and Nitrosomonas genus A solid deodorant comprising a pest repelling component, characterized in that it is prepared through the steps of culturing by additionally inoculating one or more microorganisms to be used and (e) stopping the culture when the pH of the culture medium is 12 to 14 and obtaining a deodorant .
탈취제 34~38 중량부, 젤란검 1.6~2.0 중량부,라벤다오일 8~10 중량부, 제라늄로즈오일 3~7 중량부, 베타코코인 3~6 중량부, 애플워시 3~6 중량부, 에틸알코올 16~20 중량부, 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2~5 중량부를 포함하되,
상기 탈취제는,
(a) 유기산 생성 미생물을 배양액의 pH가 3~5일 때까지 배양하는 단계, (b) 상기 배양액에서 균체를 제거한 다음, 배양 배지를 첨가하고, pH를 9~10으로 조정한 후, 바실러스 속 (Bacillus sp), 아스페르기루스 속(Aspergillus sp) 및 니트로소모나스 속(Nitrosomonas sp)으로 구성된 군에서 선택되는 하나 이상의 미생물을 접종하여 배양하는 단계, (c) 상기 배양액의 pH가 8~85일 때 배양액의 pH를 115~12로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계, (d) 상기 배양액의 pH가 10~105일 때 배양액의 pH를 135~14로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계 및 (e) 상기 배양액의 pH가 12~14일 때 배양을 멈추고 소취제를 수득하는 단계를 거쳐 제조되는 것을 특징으로 하는 해충 기피 성분을 포함하는 고체탈취제.
With respect to 100 parts by weight of purified water,
34-38 parts by weight of deodorant, 1.6-2.0 parts by weight of gellan gum, 8-10 parts by weight of lavender oil, 3-7 parts by weight of geranium rose oil, 3-6 parts by weight of beta cocoin, 3-6 parts by weight of apple wash, ethyl 16-20 parts by weight of alcohol, including 2-5 parts by weight of 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine,
The deodorant is
(a) culturing the organic acid-producing microorganism until the pH of the culture medium is 3 to 5, (b) removing the cells from the culture medium, adding a culture medium, and adjusting the pH to 9 to 10, Bacillus genus (Bacillus sp), the step of culturing by inoculating one or more microorganisms selected from the group consisting of Aspergillus sp and Nitrosomonas sp, (c) the pH of the culture medium is 8 to 85 After adjusting the pH of the culture medium to 115 to 12 when , (d) when the pH of the culture medium is 10 to 105, after adjusting the pH of the culture medium to 135 to 14, a culture medium is added, and selected from the group consisting of Bacillus genus, Aspergillus genus and Nitrosomonas genus A solid deodorant comprising a pest repelling component, characterized in that it is prepared through the steps of culturing by additionally inoculating one or more microorganisms to be used and (e) stopping the culture when the pH of the culture medium is 12 to 14 and obtaining a deodorant .
100~110℃온도에서 젤란검이 중탕되어 용해되는 젤란검용해단계;
상기 1차 교반단계를 거쳐 제조된 혼합물과 상기 젤란검용해단계를 거쳐 용해된 액상상태의 젤란검이 교반되는 2차 교반단계;
상기 2차 교반단계를 거친 탈취제가 -10℃ 온도의 냉각저장고에서 응고되는 응고단계;를 포함하되,
상기 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine 2~5 중량부를 포함하되,
상기 탈취제는,
(a) 유기산 생성 미생물을 배양액의 pH가 3~5일 때까지 배양하는 단계, (b) 상기 배양액에서 균체를 제거한 다음, 배양 배지를 첨가하고, pH를 9~10으로 조정한 후, 바실러스 속 (Bacillus sp), 아스페르기루스 속(Aspergillus sp) 및 니트로소모나스 속(Nitrosomonas sp)으로 구성된 군에서 선택되는 하나 이상의 미생물을 접종하여 배양하는 단계, (c) 상기 배양액의 pH가 8~85일 때 배양액의 pH를 115~12로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계, (d) 상기 배양액의 pH가 10~105일 때 배양액의 pH를 135~14로 조정한 후, 배양 배지를 첨가하고, 바실러스 속, 아스페르기루스 속 및 니트로소모나스 속으로 구성된 군에서 선택되는 하나 이상의 미생물을 추가로 접종하여 배양하는 단계 및 (e) 상기 배양액의 pH가 12~14일 때 배양을 멈추고 소취제를 수득하는 단계를 거쳐 제조되는 것을 특징으로 하는 해충 기피 성분을 포함하는 고체탈취제 제조방법.
Based on 100 parts by weight of purified water at 70-80°C, 34-38 parts by weight of deodorant, 8-10 parts by weight of natural oil, 3-7 parts by weight of insect repellent, 3-6 parts by weight of beta cocoin, 3-6 parts by weight of apple wash 1st stirring step in which parts by weight, 16-20 parts by weight of ethyl alcohol, and 2-5 parts by weight of 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine are mixed and stirred for 2 hours ;
Gellan gum dissolving step in which gellan gum is melted by boiling at a temperature of 100~110℃;
a second stirring step in which the mixture prepared through the first stirring step and the gellan gum dissolved through the gellan gum dissolving step are stirred;
A coagulation step in which the deodorant that has undergone the secondary stirring step is coagulated in a cooling storage at a temperature of -10°C; including,
Containing 2-5 parts by weight of the 1,3,5-tris(2-hydroxyethyl)hexahydro-1,3,5-triazine,
The deodorant is
(a) culturing the organic acid-producing microorganism until the pH of the culture medium is 3 to 5, (b) removing the cells from the culture medium, adding a culture medium, and adjusting the pH to 9 to 10, Bacillus genus (Bacillus sp), the step of culturing by inoculating one or more microorganisms selected from the group consisting of Aspergillus sp and Nitrosomonas sp, (c) the pH of the culture medium is 8 to 85 After adjusting the pH of the culture medium to 115 to 12 when , (d) when the pH of the culture medium is 10 to 105, after adjusting the pH of the culture medium to 135 to 14, a culture medium is added, and selected from the group consisting of Bacillus genus, Aspergillus genus and Nitrosomonas genus A solid deodorant comprising a pest repelling component, characterized in that it is prepared through the steps of culturing by additionally inoculating one or more microorganisms to be used and (e) stopping the culture when the pH of the culture medium is 12 to 14 and obtaining a deodorant manufacturing method.
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