KR101151383B1 - Ecofriendly and vegitable base oil for space spray type disinfection oil and manufacturing method whichof - Google Patents

Ecofriendly and vegitable base oil for space spray type disinfection oil and manufacturing method whichof Download PDF

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KR101151383B1
KR101151383B1 KR1020120002750A KR20120002750A KR101151383B1 KR 101151383 B1 KR101151383 B1 KR 101151383B1 KR 1020120002750 A KR1020120002750 A KR 1020120002750A KR 20120002750 A KR20120002750 A KR 20120002750A KR 101151383 B1 KR101151383 B1 KR 101151383B1
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oil
parts
vegetable
water
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유정민
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늘푸른(주)
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/02Acyclic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material

Abstract

PURPOSE: A method for manufacturing eco-friendly vegetable base oil for disinfection oil of space spray is provided to enhance disinfection time without environmental pollution. CONSTITUTION: An eco-friendly vegetable base oil for disinfection oil of space spray contains 30-50 weight parts of biodiesel or vegetable oil, 20-50 weight parts of vegetable glycerin, 20-50 weight parts of ethanol or methanol, 1-10 weight parts of sodium hydroxide, and 20-50 weight parts of water. The composition further contains 1-10 weight parts of vegetable nutrient and 1-10 weight parts of deodorizer. The water includes hydrogen water or oxygen water. The deodorizer includes natural phytoncide extract or natural baby powder flavor. A method for preparing the oil comprises a step of mixing vegetable glycerin into biodiesel or vegetable oil(S101); and a step of homogenizing the mixture in water(S103).

Description

공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법{ECOFRIENDLY AND VEGITABLE BASE OIL FOR SPACE SPRAY TYPE DISINFECTION OIL AND MANUFACTURING METHOD WHICHOF}Eco-friendly vegetable base oil for space spray antiseptic disinfectant and its manufacturing method {ECOFRIENDLY AND VEGITABLE BASE OIL FOR SPACE SPRAY TYPE DISINFECTION OIL AND MANUFACTURING METHOD WHICHOF}

본 발명은 살충제 또는 살균제 등이 첨가되어 연무 또는 연막을 통해 공간살포됨에 따라 효과적인 방역을 가능하게 하는 공간살포 방역소독유용 기유 및 그 제조방법에 관한 것으로, 더욱 상세하게는 공간살포시에 확산효과가 우수하고 동일 양의 광물유에 비해 방역사용시간이 증대될 수 있을 뿐만 아니라 생분해로 인해 환경오염물질이 잔존하지 않아 환경오염을 전혀 유발하지 않는 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 관한 것이다.The present invention relates to a space spray antiseptic disinfectant base oil and a method for preparing the same, which are effective spraying as the insecticide or fungicide is added to the space spray through the mist or smoke screen, more specifically, excellent diffusion effect during space spraying The present invention relates to an environmentally friendly vegetable base oil for space spraying and disinfecting toxic oils, which does not cause any environmental pollution due to the fact that biodegradation does not cause any environmental pollutants due to biodegradation.

일반적으로 공간살포 방역소독유는 연무 또는 연막을 통해 공간살포됨에 따라 효과적인 방역을 가능하게 하는 것으로, 경유나 등유와 같은 광물유로 형성되는 기유에 살충제 또는 살균제 등이 첨가되어 제조되고, 열건식 연막기와 같은 연막방역기계 또는 연무방역기계를 통해 최종적으로 공간살포된다.In general, the space spray antiseptic disinfectant oil is to enable effective prevention as space is sprayed through a fume or smoke screen, prepared by adding insecticides or fungicides to the base oil formed of mineral oil such as diesel oil or kerosene, The space is finally distributed through the same smoke screening machine or smoke spraying machine.

광물유를 주성분으로 한 종래의 공간살포 방역소독유는 불쾌한 냄새유발을 물론 인체에 매우 해로울 뿐만 아니라, 특히 가축의 우리, 목초, 농작물 등에 분무확산될 경우에는 동물의 사료, 동물이 섭취하는 목초, 농작물 줄기나 잎 등에 전착되어 냄새에 의해 가축의 식감을 저하시킬 수 있으며, 자연적으로 분해되지 않아 자원을 손상시키는 등 2차 환경공해를 유발시키는 문제점이 있다.Conventional space spray antiseptic disinfectant oil containing mineral oil is not only harmful to human body, but also harmful to human body, especially when it is sprayed and diffused to livestock, grasses, crops, etc. Electrodeposited on stems and leaves may reduce the texture of the livestock due to the smell, and there is a problem of causing secondary environmental pollution, such as damaging resources because it is not naturally degraded.

뿐만 아니라 불순한 광물유는 벤젠, 톨루엔, 크실렌 등의 발암물질이 섞여 있어 사람이나 가축의 건강에 치명적인 문제점이 있을 뿐만 아니라 환경호르몬을 생성시킬 수 있는 위험성이 있다.In addition, impure mineral oil is mixed with carcinogens such as benzene, toluene, and xylene, which is not only a fatal problem for human or livestock health, but also a risk of producing environmental hormones.

이러한 문제점을 해결하기 위하여 한국특허등록 제10-0456808호(2004.11.02.)에 동식물유 46 내지 48중량%에 알콜류 20 중량%, 비이온계면활성제 또는 양성이온계면활성제 30 내지 32중량%, 파인오일 2 내지 3중량%을 순차적으로 첨가 교반하여 균질화시킨 조성물에 대하여 물 50 내지 90 중량%를 소량식 천천히 첨가 30분 이상 유화 내지는 수용화시킴을 특징으로 하는 무공해 연무확산제가 공개되어 있다.In order to solve this problem, Korean Patent Registration No. 10-0456808 (2004.11.02.), 46 to 48% by weight of animal and vegetable oil, 20% by weight of alcohol, 30 to 32% by weight of nonionic surfactant or zwitterionic surfactant, fine A pollution-free mist-diffusing agent is disclosed which emulsifies or solubilizes 50 to 90% by weight of water in a small amount and slowly for at least 30 minutes to a composition homogenized by sequentially adding and stirring 2 to 3% by weight of oil.

또한 한국특허등록 제10-0930653호(2009.12.01.)에는 바이오디젤 67 내지 75중량%, 식물성 계면활성제 5 내지 3중량% 및 물 28 내지 22중량%로 조성하여 서로 혼합하여 이들을 유화시킨 것을 특징으로 하는 연무 확산제가 공개되어 있다.In addition, the Korean Patent Registration No. 10-0930653 (2009.12.01.) Is composed of biodiesel 67 to 75% by weight, 5 to 3% by weight of vegetable surfactant and 28 to 22% by weight of water mixed with each other to emulsify them A mist spreading agent is disclosed.

그러나 전술한 연무 확산제들의 경우에도 동식물유나 바이오디젤 만으로는 공간살포시에 확산효과가 떨어지는 문제점이 있을 뿐만 아니라 콩기름 자체의 불쾌한 냄새가 유발되는 문제점이 있으며, 살충, 살균과 같은 방역효과 외에 그 어떠한 부가적인 기능이 제공될 수 없는 문제점이 있다.However, even in the case of the mist spraying agents described above, the plant or oil or biodiesel alone has a problem in that the spreading effect is not only decreased during space spraying, but also causes an unpleasant odor of soybean oil itself. There is a problem that the function cannot be provided.

본 발명의 목적은, 식물성기름 또는 바이오디젤을 식물성글리세린과 혼합한 후 호모믹싱기 내에서 물과 균질혼합하여 제조됨에 따라, 공간살포시에 확산효과가 우수하고 동일 양의 광물유에 비해 방역사용시간이 증대될 수 있을 뿐만 아니라 생분해로 인해 환경오염물질이 잔존하지 않아 환경오염을 전혀 유발하지 않는 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법을 제공하는 것이다.It is an object of the present invention, as a vegetable oil or biodiesel is mixed with vegetable glycerin and then homogeneously mixed with water in a homomixer, the diffusion effect is excellent during space spraying and the anti-rusting time compared to the same amount of mineral oil Not only can it be increased, but there is no environmental pollutant remaining due to biodegradation, thus providing an environmentally friendly vegetable base oil for space spray antiseptic disinfectant and its manufacturing method.

본 발명의 목적은, 공간살포되더라도 불쾌한 냄새가 전혀 없으며, 특히 식물들에 영양분을 제공하는 부가기능까지 제공될 수 있도록 한 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법을 제공하는 것이다. It is an object of the present invention to provide an environmentally friendly vegetable base oil for space spray antiseptic disinfection oil and a method for producing the same, which have no unpleasant odor even when sprayed in space, and in particular, an additional function of providing nutrients to plants.

전술한 본 발명의 목적들은, 바이오디젤 또는 식물성기름과, 식물성글리세린과, 에탄올 또는 메탄올과, 수산화나트륨과, 물이 호모믹싱기 내에서 고속교반되어 형성되는 공간살포 방역소독유용 친환경 식물성 기유를 제공함에 의해 달성된다.The above object of the present invention is to provide an eco-friendly vegetable base oil for space spray antiseptic disinfectant oil formed by biodiesel or vegetable oil, vegetable glycerin, ethanol or methanol, sodium hydroxide, and water is rapidly stirred in a homomixer. Is achieved by.

본 발명의 바람직한 특징에 따르면, 상기 바이오디젤 또는 식물성기름 30 내지 50 중량부와, 상기 식물성글리세린 20 내지 50 중량부와, 상기 에탄올 또는 메탄올 20 내지 50 중량부와, 상기 수산화나트륨 1 내지 10 중량부, 상기 물 20 내지 50 중량부가 호모믹싱기 내에서 고속교반되어 형성된다.According to a preferred feature of the invention, the biodiesel or vegetable oil 30 to 50 parts by weight, the vegetable glycerin 20 to 50 parts by weight, the ethanol or methanol 20 to 50 parts by weight, the sodium hydroxide 1 to 10 parts by weight 20 to 50 parts by weight of water is formed by high speed stirring in the homomixer.

본 발명의 바람직한 특징에 따르면, 탈취제 1 내지 10 중량부 또는 식물영양제 1 내지 10 중량부가 호모믹싱기 내에 더 첨가된다.According to a preferred feature of the invention, 1 to 10 parts by weight of deodorant or 1 to 10 parts by weight of phytonutrients are further added in the homomixer.

본 발명의 바람직한 특징에 따르면, 상기 물은 수소수 또는 산소수이고, 상기 탈취제는 천연피톤치드추출액 또는 천연베이비파우더향이고, 상기 식물영양제는 액상비료, 액상비타민수용액 및 미네랄수용액 중 하나이다.According to a preferred feature of the invention, the water is hydrogen water or oxygen water, the deodorant is natural phytoncide extract or natural baby powder flavor, the plant nutrient is one of liquid fertilizer, liquid vitamin solution and mineral solution.

전술한 본 발명의 목적들은, 바이오디젤 또는 식물성기름에 식물성글리세린을 혼합하는 원료혼합단계와, 상기 원료혼합단계를 거친 혼합물을 호모믹싱기 내에서 물과 균질혼합하는 균질혼합단계를 포함하는 공간살포 방역소독유용 친환경 식물성 기유의 제조방법을 제공함에 의해 달성된다.Objects of the present invention described above, the spatial spraying comprising a raw material mixing step of mixing the vegetable glycerin to biodiesel or vegetable oil, and a homogeneous mixing step of homogeneously mixing the mixture and the mixture passed through the raw material mixing step with water in the homomixer It is achieved by providing a method for producing environmentally friendly vegetable base oil for antiseptic disinfectant oil.

본 발명의 바람직한 특징에 따르면, 상기 원료혼합단계에서는 용매로 에탄올 또는 메탄올이 첨가되고 pH조절제로 수산화나트륨이 첨가된다.According to a preferred feature of the invention, in the raw material mixing step, ethanol or methanol is added as a solvent and sodium hydroxide is added as a pH adjuster.

본 발명의 바람직한 특징에 따르면, 상기 원료혼합단계에서는 상기 바이오디젤 또는 식물성기름 30 내지 50 중량부에 상기 식물성글리세린 20 내지 50 중량부가 혼합되고 상기 에탄올 또는 메탄올 20 내지 50 중량부와 상기 수산화나트륨 1 내지 10 중량부가 첨가되며 35 내지 55℃의 온도 및 60 내지 100rpm의 속도로 30 내지 60분간 교반된다.According to a preferred feature of the present invention, in the raw material mixing step, 20 to 50 parts by weight of the vegetable glycerin is mixed with 30 to 50 parts by weight of the biodiesel or vegetable oil, and 20 to 50 parts by weight of the ethanol or methanol and 1 to sodium hydroxide. 10 parts by weight is added and stirred for 30 to 60 minutes at a temperature of 35 to 55 ° C. and a speed of 60 to 100 rpm.

본 발명의 바람직한 특징에 따르면, 상기 원료혼합단계와 상기 균질혼합단계 사이에 상기 원료혼합단계를 거친 혼합물을 35 내지 55℃의 온도 및 10 내지 60rpm의 속도로 12 내지 30시간 정도 교반시키는 숙성단계를 더 포함한다.According to a preferred feature of the present invention, the ripening step of stirring the mixture passed through the raw material mixing step between the raw material mixing step and the homogeneous mixing step at a temperature of 35 to 55 ℃ and a speed of 10 to 60 rpm for about 12 to 30 hours It includes more.

본 발명의 바람직한 특징에 따르면, 상기 균질혼합단계에서 상기 물은 수소수 또는 산소수로 형성되고 20 내지 50 중량부의 양으로 혼합되며, 50 내지 80℃의 온도 및 1000 내지 3000rpm의 속도로 30 내지 60분간 고속교반된다.According to a preferred feature of the invention, in the homogeneous mixing step, the water is formed of hydrogen water or oxygen water and mixed in an amount of 20 to 50 parts by weight, at a temperature of 50 to 80 ℃ and a speed of 1000 to 3000 rpm 30 to 60 High speed stirring for minutes.

본 발명의 바람직한 특징에 따르면, 상기 균질혼합단계 이후에 탈취제 1 내지 10 중량부 또는 식물영양제 1 내지 10 중량부를 더 혼합하는 기능성물질혼합단계를 더 포함한다.According to a preferred feature of the invention, after the homogeneous mixing step further comprises a functional material mixing step of further mixing 1 to 10 parts by weight or 1 to 10 parts by weight of plant nutrients.

본 발명의 바람직한 특징에 따르면, 상기 탈취제는 천연피톤치드추출액 또는 천연베이비파우더향이고, 상기 식물영양제는 액상비료, 액상비타민수용액 및 미네랄수용액 중 하나이다.According to a preferred feature of the present invention, the deodorant is natural phytoncide extract or natural baby powder flavor, the plant nutrient is one of liquid fertilizer, liquid vitamin solution and mineral solution.

본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 의하면, 바이오디젤 또는 식물성기름 및 물에 식물성글리세린이 더 포함됨에 따라 공간살포시에 확산효과가 우수하고 동일 양의 광물유에 비해 방역사용시간이 증대될 수 있을 뿐만 아니라 생분해로 인해 환경오염의 염려가 전혀 없는 탁월한 효과가 있다.According to the present invention, environmentally friendly vegetable base oils for space spray antiseptic disinfectant oil and a method for preparing the same are excellent in the effect of spreading during space spraying as biodiesel or vegetable oils and water are further included, and the use of antifouling agents compared to the same amount of mineral oil. Not only can the time be increased, but biodegradation has an excellent effect without any concern about environmental pollution.

또한 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 의하면, 호모믹싱기에 의한 균질혼합에 의해 계면활성제 없이도 바이오디젤 또는 식물성기름과 식물성글리세린의 혼합물과 형성되는 원료가 물과 상분리되지 않게 혼합될 수 있어 계면활성제의 사용에 따른 문제점이 일거에 해소될 수 있는 탁월한 효과가 있다.In addition, according to the present invention, eco-friendly vegetable base oil for space spray antiseptic disinfectant oil and a method for preparing the same, wherein the raw material formed with a mixture of biodiesel or vegetable oil and vegetable glycerin without a phase phase is separated from water by homogeneous mixing by a homomixer. It can be mixed so that there is an excellent effect that can be solved at one time the problem caused by the use of a surfactant.

뿐만 아니라 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 의하면, 천연피톤치드추출액 또는 천연베이비파우더향과 같은 탈취제가 더 첨가됨에 따라 공간살포후 불쾌한 냄새가 전혀 없으며, 액상비료, 액상비타민수용액 또는 미네랄수용액과 같은 식물영양제가 더 첨가됨에 따라 식물생장을 촉진시키는 탁월한 효과가 있다.In addition, according to the environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the invention and a manufacturing method thereof, there is no unpleasant odor after the space spray, as a deodorant such as natural phytoncide extract or natural baby powder flavor is added, liquid fertilizer, liquid vitamin As more nutrients such as aqueous solutions or mineral aqueous solutions are added, there is an excellent effect of promoting plant growth.

도 1은 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유의 제조방법의 공정순서도.
도 2는 경유를 기유로 하는 종래의 공간살포 방역소독유를 열건식 연막기로 공간살포한 사진.
도 3은 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유를 포함하는 공간살포 방역소독유를 열건식 연막기로 공간살포한 사진.
1 is a process flow diagram of a method for producing environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the present invention.
Figure 2 is a space spray photo of the conventional space spraying antiseptic disinfectant oil based on diesel fuel with a heat-drying smoke screen.
Figure 3 is a space spray photo of the space spray antiseptic disinfectant oil containing environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the present invention with a heat-drying smoke screen.

이하에는, 본 발명의 바람직한 실시예를 첨부도면을 참조하여 상세하게 설명하되, 이는 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 발명을 용이하게 실시할 수 있을 정도로 상세하게 설명하기 위한 것이지, 이로 인해 본 발명의 기술적인 사상 및 범주가 한정되는 것을 의미하지는 않는다.
Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings, which are intended to describe in detail enough to be easily carried out by those skilled in the art to which the present invention pertains. This does not mean that the technical spirit and scope of the present invention is limited.

본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유는, 공간살포시에 확산효과가 우수하고 동일 양의 광물유에 비해 방역사용시간이 증대될 수 있을 뿐만 아니라 생분해로 인해 환경오염을 전혀 유발하지 않도록 함과 동시에 공간살포되더라도 불쾌한 냄새가 전혀 없으며, 특히 식물들에 영양분을 제공하는 부가기능까지 제공될 수 있도록 하기 위한 것으로, 바이오디젤 또는 식물성기름과, 식물성글리세린과, 에탄올 또는 메탄올과, 수산화나트륨과, 물이 계면활성제의 첨가없이 호모믹싱기 내에서 고속교반되어 형성된다.Eco-friendly vegetable base oils for space spray antiseptic disinfectant according to the present invention is excellent in diffusion effect during space spraying, and can be used to increase the duration of pesticides compared to the same amount of mineral oil, and also does not cause any environmental pollution due to biodegradation. At the same time, there is no unpleasant odor even if it is space sprayed, especially to provide additional functions to provide nutrients to plants, such as biodiesel or vegetable oil, vegetable glycerin, ethanol or methanol, sodium hydroxide, water It is formed by high speed stirring in the homomixer without adding this surfactant.

바이오디젤은 연소를 위한 친환경 연료유로 작용하는 것으로, 콩기름 등의 식물성기름을 원료로 해서 제조되며, 식물성기름 또한 연소를 위한 친환경 연료유로 작용하는 것으로, 옥수수기름, 콩기름 또는 팜유 등으로 형성된다.Biodiesel acts as an environmentally friendly fuel oil for combustion, and is manufactured from vegetable oils such as soybean oil as raw materials, and vegetable oil also acts as an environmentally friendly fuel oil for combustion, and is formed of corn oil, soybean oil, or palm oil.

식물성글리세린은 연소를 위한 친환경 연료유로 작용함과 동시에 연막방역기계 또는 연무방역기계를 통한 공간살포시 공간살포연무량 또는 연막량을 배가시키는 역할을 하는 것으로, 주로 바이오디젤의 제조시 부산물로 나오는 식물성글리세린(순도 99.8%)인 것이 바람직하다. Vegetable glycerin acts as an eco-friendly fuel oil for combustion and at the same time plays a role of doubling the amount of space spray mist or smoke during space spraying through smoke screening machine or smoke spraying machine. It is preferable that it is (purity 99.8%).

바이오디젤 또는 식물성기름과 식물성글리세린은 휘발성이나 폭발적인 연소성이 없어 광물유를 사용하는 동일 양의 공간살포 방역소독유에 비해 더 오래 방역사용을 지속시키는 역할을 한다.Biodiesel or vegetable oils and vegetable glycerin have no volatile or explosive combustibility and play a role of longer lasting protection against the same amount of space spray antiseptic oil using mineral oil.

바이오디젤 또는 식물성기름과 식물성글리세린은 각각 30 내지 50 중량부와 20 내지 50 중량부로 혼합되는 것이 바람직하다.Biodiesel or vegetable oil and vegetable glycerin is preferably mixed in 30 to 50 parts by weight and 20 to 50 parts by weight, respectively.

에탄올 또는 메탄올은 바이오디젤 또는 식물성기름과 식물성글리세린을 서로 녹여 혼합하기 위한 용매로 첨가되는 것으로, 바이오디젤 또는 식물성기름 30 내지 50 중량부에 식물성글리세린 20 내지 50 중량부가 혼합될 경우에 20 내지 50 중량부의 양으로 첨가되는 것이 바람직하다.Ethanol or methanol is added as a solvent for dissolving and mixing biodiesel or vegetable oil and vegetable glycerin, and 20 to 50 weight when 20 to 50 parts by weight of vegetable glycerin is mixed with 30 to 50 parts by weight of biodiesel or vegetable oil. It is preferred to add in negative amounts.

수산화나트륨은 pH조절제로 작용하는 것으로, 바이오디젤 또는 식물성기름 30 내지 50 중량부에 식물성글리세린 20 내지 50 중량부가 혼합됨과 동시에 에탄올 또는 메탄올 20 내지 50 중량부가 첨가될 경우에 수산화나트륨 1 내지 10 중량부가 첨가되는 것이 바람직하다.Sodium hydroxide acts as a pH adjuster, and when 1 to 10 parts by weight of sodium hydroxide is added when 20 to 50 parts by weight of vegetable glycerin is mixed with 30 to 50 parts by weight of biodiesel or vegetable oil. It is preferred to be added.

물은 일반 정제수로도 형성될 수 있지만, 일반물에 비해 10배 이상의 수소가 녹아 있는 수소수 또는 일반물에 비해 10배 이상의 산소가 녹아 있는 산소수로 형성되는 것이 바람직한데, 이러한 수소수나 산소수는 특히 연막방역기계를 통한 공간살포시 폭발적인 연소를 발생시켜 연막의 양을 순간적으로 증대시키는 역할을 한다. 물은 바이오디젤 또는 식물성기름 30 내지 50 중량부, 식물성글리세린 20 내지 50 중량부, 에탄올 또는 메탄올 20 내지 50 중량부, 수산화나트륨 1 내지 10 중량부가 혼합될 경우에 20 내지 50 중량부의 양으로 혼합되는 것이 바람직하다.The water may be formed of general purified water, but is preferably formed of hydrogen water in which 10 times or more of hydrogen is dissolved than general water or oxygen water in which 10 times or more of oxygen is dissolved than general water. Particularly, it acts to increase the amount of smoke instantly by generating explosive combustion during space spraying through smoke screening machine. Water is mixed in an amount of 20 to 50 parts by weight, when 30 to 50 parts by weight of biodiesel or vegetable oil, 20 to 50 parts by weight of vegetable glycerin, 20 to 50 parts by weight of ethanol or methanol, and 1 to 10 parts by weight of sodium hydroxide are mixed. It is preferable.

바이오디젤 또는 식물성기름과, 식물성글리세린과, 에탄올 또는 메탄올과, 수산화나트륨과, 물이 계면활성제의 첨가없이 호모믹싱기 내에서 고속교반되는 것이 바람직한데, 이 경우 공지 구성의 호모믹싱기에 의해 50 내지 80℃의 온도 및 1000 내지 3000rpm의 속도로 30 내지 60분간 고속교반되는 것이 바람직하다.Biodiesel or vegetable oil, vegetable glycerin, ethanol or methanol, sodium hydroxide, and water are preferably stirred at high speed in the homomixer without the addition of a surfactant. It is preferable to stir at high speed for 30 to 60 minutes at a temperature of 80 ° C. and a speed of 1000 to 3000 rpm.

호모믹싱기 내에는 냄새제거를 위한 탈취제 또는 식물생장을 촉진시키는 식물영양제가 더 첨가되는 것이 바람직한데, 여기서 탈취제는 천연피톤치드추출액 또는 천연베이비파우더향으로 형성되고 1 내지 10 중량부의 양으로 첨가되는 것이 바람직하며, 식물영양제는 액상비료, 액상비타민수용액 및 미네랄수용액(CIM수용액) 중 하나로 형성되고 1 내지 10 중량부의 양으로 첨가되는 것이 바람직하다.It is preferable to further add a deodorant for odor removal or a plant nutrient for promoting plant growth in the homomixer, wherein the deodorant is formed into a natural phytoncide extract or natural baby powder and added in an amount of 1 to 10 parts by weight. Preferably, the plant nutrient is formed of one of the liquid fertilizer, liquid vitamin solution and mineral solution (CIM solution) is preferably added in an amount of 1 to 10 parts by weight.

본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유를 구성하는 각각의 성분들의 중량부 범위는 바이오디젤 또는 식물성기름을 기준으로 각 성분들의 효과와 부작용 가능성을 기준으로 한정된 것으로, 중량비 범위의 상한값은 다른 구성성분의 함량을 전체적으로 고려하여 결정되었고 중량비 범위의 하한값은 그 이하에서는 해당 구성성분의 효과가 떨어지는 문제가 있어, 상술한 바와 같은 수치범위로 한정하였다.The weight range of each component constituting the eco-friendly vegetable base oil for the space spray antiseptic disinfectant according to the present invention is limited based on the effects and potential side effects of each component on the basis of biodiesel or vegetable oil, the upper limit of the weight ratio range is different The lower limit of the weight ratio range was determined in consideration of the content of the constituent as a whole, and there is a problem that the effect of the constituent is less than that, limited to the numerical range as described above.

본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유는 바이오디젤 또는 식물성기름과, 식물성글리세린과, 에탄올 또는 메탄올과, 수산화나트륨과, 물이 호모믹싱기 내에 한꺼번에 투입되어 고속교반되어 형성될 수도 있으나, 아래와 같은 순차적인 제조공정순서를 가지는 제조방법에 의해 제조되는 것이 바람직하다.Eco-friendly vegetable base oil for the space spray antiseptic disinfectant according to the present invention may be formed by biodiesel or vegetable oil, vegetable glycerin, ethanol or methanol, sodium hydroxide and water at a time mixed in a homomixer at high speed stirring, It is preferable to manufacture by the manufacturing method which has a sequential manufacturing process sequence as follows.

이하, 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유의 제조방법을 설명하면 다음과 같다:Hereinafter, a method for preparing an environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the present invention is as follows:

본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유의 제조방법은, 공간살포시에 확산효과가 우수하고 동일 양의 광물유에 비해 방역사용시간이 증대될 수 있을 뿐만 아니라 생분해로 인해 환경오염을 전혀 유발하지 않도록 함과 동시에 공간살포되더라도 불쾌한 냄새가 전혀 없으며, 특히 식물들에 영양분을 제공하는 부가기능까지 제공될 수 있도록 하기 위한 것으로, 도 1에 도시되는 바와 같이 바이오디젤 또는 식물성기름에 식물성글리세린을 혼합하는 원료혼합단계(S101)와, 원료혼합단계(S101)를 거친 혼합물을 호모믹싱기 내에서 물과 균질혼합하는 균질혼합단계(S103)를 포함한다.The method for producing environmentally friendly vegetable base oils for space spray antiseptic disinfectant according to the present invention has an excellent diffusion effect during space spraying and can increase the duration of use of pesticides compared to the same amount of mineral oil, and does not cause any environmental pollution due to biodegradation. At the same time, there is no unpleasant odor even when sprayed in space, and in particular, to provide an additional function of providing nutrients to plants, and to mix vegetable glycerin with biodiesel or vegetable oil as shown in FIG. The raw material mixing step (S101), and the homogeneous mixing step (S103) of homogeneously mixing the water and the mixture passed through the raw material mixing step (S101) in a homomixer.

여기서, 원료혼합단계(S101)는 광물유를 대신하여 불완전연소될 원료를 사전에 제조하는 단계로서, 이 원료혼합단계(S101)에서는 콩기름 등의 식물성기름을 원료로 해서 제조되는 바이오디젤 또는 옥수수기름, 콩기름, 팜유 등과 같은 식물성기름에 바이오디젤의 제조시 부산물로 나오는 식물성글리세린(순도 99.8%)을 혼합한다. Here, the raw material mixing step (S101) is a step of preparing a raw material to be incompletely burned in place of the mineral oil, in this raw material mixing step (S101), biodiesel or corn oil manufactured from vegetable oils such as soybean oil, Vegetable oil, such as soybean oil and palm oil, is mixed with vegetable glycerin (purity 99.8%) which is a by-product of the production of biodiesel.

바이오디젤 또는 식물성기름은 연소를 위한 친환경 연료유로 작용하며 식물성글리세린은 연소를 위한 친환경 연료유로 작용함과 동시에 연막방역기계 또는 연무방역기계를 통한 공간살포시 공간살포연무량 또는 연막량을 배가시키는 역할을 한다. Biodiesel or vegetable oil acts as an eco-friendly fuel oil for combustion and vegetable glycerin acts as an eco-friendly fuel oil for combustion and doubles the amount of space spray mist or smoke when spraying space through smoke screening or smoke spraying machines. do.

바이오디젤 또는 식물성기름과 식물성글리세린은 휘발성이나 폭발적인 연소성이 없어 광물유를 사용하는 동일 양의 공간살포 방역소독유에 비해 더 오래 방역사용을 지속시키는 역할을 한다.Biodiesel or vegetable oils and vegetable glycerin have no volatile or explosive combustibility and play a role of longer lasting protection against the same amount of space spray antiseptic oil using mineral oil.

원료혼합단계(S101)에서는 바이오디젤 또는 식물성기름 30 내지 50 중량부에 식물성글리세린 20 내지 50 중량부가 혼합되는 것이 바람직하며, 공지 구성의 온열교반기에 의해 35 내지 55℃의 온도 및 60 내지 100rpm의 속도로 30 내지 60분간 교반되는 것이 바람직하다.In the raw material mixing step (S101), 20 to 50 parts by weight of vegetable glycerin is preferably mixed with 30 to 50 parts by weight of biodiesel or vegetable oil, and a temperature of 35 to 55 ° C. and a speed of 60 to 100 rpm by a thermal stirrer having a known configuration. It is preferable to stir for 30 to 60 minutes.

또한 원료혼합단계(S101)에서는 바이오디젤 또는 식물성기름과 식물성글리세린을 서로 녹여 혼합하기 위한 용매로서 에탄올 또는 메탄올이 첨가되는 것이 바람직하다. 용매로 작용하는 에탄올 또는 메탄올은 바이오디젤 또는 식물성기름 30 내지 50 중량부에 식물성글리세린 20 내지 50 중량부가 혼합될 경우에 20 내지 50 중량부의 양으로 첨가되는 것이 바람직하다.In addition, in the raw material mixing step (S101), ethanol or methanol is preferably added as a solvent for dissolving and mixing biodiesel or vegetable oil and vegetable glycerin. Ethanol or methanol serving as a solvent is preferably added in an amount of 20 to 50 parts by weight when 20 to 50 parts by weight of vegetable glycerin is mixed with 30 to 50 parts by weight of biodiesel or vegetable oil.

또한 원료혼합단계(S101)의 최종 혼합물의 pH는 8 내지 8.5로 유지되는 것이 바람직한데, 이를 위하여 원료혼합단계(S101)에서는 pH조절제로 수산화나트륨이 첨가되는 것이 바람직하다. pH조절제로 작용하는 수산화나트륨은 에탄올 또는 메탄올은 바이오디젤 또는 식물성기름 30 내지 50 중량부에 식물성글리세린 20 내지 50 중량부가 혼합됨과 동시에 에탄올 또는 메탄올 20 내지 50 중량부가 첨가될 경우에 수산화나트륨 1 내지 10 중량부가 첨가되는 것이 바람직하다. In addition, the pH of the final mixture of the raw material mixing step (S101) is preferably maintained at 8 to 8.5, for this purpose, sodium hydroxide is preferably added as a pH regulator in the raw material mixing step (S101). Sodium hydroxide, which acts as a pH regulator, is ethanol or methanol when 20 to 50 parts by weight of vegetable glycerin is mixed with 30 to 50 parts by weight of biodiesel or vegetable oil and at the same time, 20 to 50 parts by weight of ethanol or methanol is added. It is preferable that a weight part is added.

전술한 원료혼합단계(S101) 이후에는 숙성단계(S102)가 행해지는 것이 바람직한데, 이 숙성단계(S102)는 원료혼합단계(S101)에 따른 원료혼합상태를 안정화시키는 단계로, 이 숙성단계(S102)에서는 상기 원료혼합단계를 거친 혼합물을 별도의 탱크 내로 이송시켜 35 내지 55℃의 온도 및 10 내지 60rpm의 속도로 12 내지 30시간 정도 교반시키게 된다.After the above-described raw material mixing step (S101) it is preferable that the aging step (S102) is carried out, this aging step (S102) is a step of stabilizing the raw material mixing state according to the raw material mixing step (S101), this aging step ( In step S102), the mixture passed through the raw material mixing step is transferred into a separate tank and stirred for about 12 to 30 hours at a temperature of 35 to 55 ° C. and a speed of 10 to 60 rpm.

전술한 숙성단계(S102) 이후에는 균질혼합단계(S103)가 행해지는데, 이 균질혼합단계(S103)는 원료혼합단계(S101)만 거치거나 또는 숙성단계(S102)까지 거친 혼합물을 계면활성제의 첨가없이 물과 균일하게 혼합하는 단계로, 공지 구성의 호모믹싱기에 의해 행해진다.After the above-mentioned aging step (S102) is carried out a homogeneous mixing step (S103), the homogeneous mixing step (S103) is a raw material mixing step (S101) only or through the addition of the surface roughening mixture to the ripening step (S102) of the addition of the surfactant In a step of uniformly mixing with water without, it is performed by a homomixer of a known configuration.

균질혼합단계(S103)에서 혼합되는 물은 일반 정제수로도 형성될 수 있지만, 일반물에 비해 10배 이상의 수소가 녹아 있는 수소수 또는 일반물에 비해 10배 이상의 산소가 녹아 있는 산소수로 형성되는 것이 바람직한데, 이러한 수소수나 산소수는 특히 연막방역기계를 통한 공간살포시 폭발적인 연소를 발생시켜 연막의 양을 순간적으로 증대시키는 역할을 한다.The water mixed in the homogeneous mixing step (S103) may be formed of general purified water, but is formed of hydrogen water in which 10 times or more hydrogen is dissolved than normal water or oxygen water in which 10 times or more oxygen is dissolved in comparison with general water. Preferably, such hydrogen water or oxygen water generates explosive combustion during space spraying through the smoke screening machine, and serves to instantly increase the amount of smoke screen.

균질혼합단계(S103)에서 혼합되는 물은 20 내지 50 중량부의 양으로 혼합되는 것이 바람직하며, 균질혼합단계(S103)는 공지 구성의 호모믹싱기에 의해 50 내지 80℃의 온도 및 1000 내지 3000rpm의 속도로 30 내지 60분간 고속교반되는 것이 바람직하다.The water mixed in the homogeneous mixing step (S103) is preferably mixed in an amount of 20 to 50 parts by weight, the homogeneous mixing step (S103) is a temperature of 50 to 80 ℃ and a speed of 1000 to 3000rpm by a known homomixer It is preferable to stir at high speed for 30 to 60 minutes.

전술한 균질혼합단계(S103) 이후에는 기능성물질혼합단계(S104)가 행해지는 것이 바람직한데, 이 기능성물질혼합단계는 냄새제거를 위한 탈취제 또는 식물생장을 촉진시키는 식물영양제를 첨가하는 단계로, 여기서 탈취제는 천연피톤치드추출액 또는 천연베이비파우더향으로 형성되고 1 내지 10 중량부의 양으로 첨가되는 것이 바람직하며, 식물영양제는 액상비료, 액상비타민수용액 및 미네랄수용액(CIM수용액) 중 하나로 형성되고 1 내지 10 중량부의 양으로 혼합되는 것이 바람직하다.After the above-mentioned homogeneous mixing step (S103), it is preferable that the functional material mixing step (S104) is performed, and this functional material mixing step is a step of adding a deodorant for odor removal or a plant nutrient for promoting plant growth, wherein Deodorant is preferably formed from natural phytoncide extract or natural baby powder and added in an amount of 1 to 10 parts by weight, and plant nutrient is formed from one of liquid fertilizer, liquid vitamin solution and mineral solution (CIM solution) and 1 to 10 weight. It is preferred to mix in negative amounts.

바이오디젤(제조원: GS칼텍스) 4kg과 순도 99.8%의 식물성글리세린 3kg에 에탄올 4kg을 첨가하고 pH 8이 유지되도록 수산화나트륨 0.5kg을 첨가한 후 공지 구성의 온열교반기 내에서 45℃의 온도 및 80rpm의 속도로 40분간 교반시킨 다음, 별도의 탱크 내로 이송시켜 45℃의 온도 및 30rpm의 속도로 24시간 교반시켜 숙성시켰다. 그 다음에 공지 구성의 호모믹싱기 내에 투입한 후 수소수 4kg을 혼합한 후 60℃의 온도 및 2000rpm의 속도로 40분간 고속교반시킨 후, 0.4kg의 천연피톤치드추출물과 0.4kg의 액상비타민수용액을 혼합하여 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유를 제조하였다.To 4 kg of biodiesel (GS Caltex) and 3 kg of vegetable glycerin with a purity of 99.8%, 4 kg of ethanol were added and 0.5 kg of sodium hydroxide was added to maintain a pH of 8, followed by a temperature of 45 ° C. and a temperature of 80 rpm in a known stirrer. After stirring for 40 minutes at a speed, it was transferred to a separate tank and aged by stirring for 24 hours at a temperature of 45 ° C. and a speed of 30 rpm. Then, the mixture was placed in a homomixer of a known configuration, mixed with 4 kg of hydrogen water, and stirred at a high speed for 40 minutes at a temperature of 60 ° C. and 2000 rpm, and then 0.4 kg of natural phytoncide extract and 0.4 kg of liquid vitamin solution were added. Mixing to prepare an environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the present invention.

본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유의 경우 불쾌한 냄새가 전혀 발생되지 않았고, 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유에 살충제를 첨가하고 열건식 연막기로 공간살포해 본 결과, 도 2 및 도 3의 비교에서 알 수 있는 바와 같이, 경유를 기유로 사용한 공간살포 방역소독유보다 훨씬 더 많은 연막이 더 큰 살포범위로 공간살포됨이 확인되었다.Environmentally friendly vegetable base oil for space spray antiseptic disinfectant oil according to the present invention did not generate an unpleasant smell at all, and the insecticide was added to the environmentally friendly vegetable base oil for space spray antiseptic disinfectant oil and space sprayed with a heat-dry smoke screen, As can be seen from the comparison of 2 and 3, it was confirmed that far more smoke spreads in a larger spreading range than the space spray antiseptic disinfectant using light oil as a base oil.

또한 1리터의 양을 기준으로 방역사용시간을 측정해 본 결과, 경유를 기유로 하는 공간살포 방역소독유의 경우 2분정도 연막이 발생되었고 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유를 이용한 공간살포 방역소독유의 경우 2분 30초 정도 연막이 발생됨이 확인되었다. 통상 400리터를 사용한다고 가정할 경우 경유를 기유로 하는 공간살포 방역소독유의 경우 6시간 40분의 방역사용시간을 나타내는 반면에, 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유를 이용한 공간살포 방역소독유의 경우 8시간 20분의 방역사용시간을 나타낸다.In addition, as a result of measuring the pesticide use time on the basis of the amount of 1 liter, the space spray antiseptic disinfectant oil based on diesel generated about 2 minutes smoke smoke and the space using eco-friendly vegetable base oil for the space spray antiseptic disinfectant oil according to the present invention In case of spraying disinfectant oil, smoke was generated for about 2 minutes and 30 seconds. In general, assuming that 400 liters are used for space spray antiseptic disinfectant oil based on diesel oil, while the spray use time is 6 hours 40 minutes, the space spray antifouling using environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the present invention. In case of disinfectant oil, it is used for 8 hours 20 minutes.

따라서, 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 의하면, 바이오디젤 또는 식물성기름 및 물에 식물성글리세린이 더 포함되는 공간살포 방역소독유용 친환경 식물성 기유가 제조됨에 따라 공간살포시에 확산효과가 우수하고 동일 양의 광물유에 비해 방역사용시간이 증대될 수 있을 뿐만 아니라 생분해로 인해 환경오염의 염려가 전혀 없다.Therefore, according to the present invention, an environmentally friendly vegetable base oil for space spray antiseptic disinfectant oil and a method for producing the same, when the space spraying according to the production of an environmentally friendly vegetable base oil for space spray antiseptic disinfectant oil further comprises vegetable glycerin in biodiesel or vegetable oil and water The diffusion effect is excellent and the use time of quarantine can be increased compared to the same amount of mineral oil, and there is no concern about environmental pollution due to biodegradation.

또한 본 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 의하면, 호모믹싱기에 의한 균질혼합에 의해 계면활성제 없이도 바이오디젤 또는 식물성기름과 식물성글리세린의 혼합물과 형성되는 원료가 물과 상분리되지 않게 혼합될 수 있어 계면활성제의 사용에 따른 문제점이 일거에 해소될 수 있을 뿐만 아니라 발명에 따른 공간살포 방역소독유용 친환경 식물성 기유 및 그 제조방법에 의하면, 천연피톤치드추출액 또는 천연베이비파우더향과 같은 탈취제가 더 혼합됨에 따라 공간살포후 불쾌한 냄새가 전혀 없으며, 액상비료, 액상비타민수용액 또는 미네랄수용액과 같은 식물영양제가 더 혼합됨에 따라 식물생장을 촉진시키는 탁월한 효과가 있다.In addition, according to the present invention, eco-friendly vegetable base oil for space spray antiseptic disinfectant oil and a method for preparing the same, wherein the raw material formed with a mixture of biodiesel or vegetable oil and vegetable glycerin without a phase phase is separated from water by homogeneous mixing by a homomixer. It can be mixed so that the problems caused by the use of the surfactant can be solved at once, and according to the environmentally friendly vegetable base oil for space spray antiseptic disinfectant according to the invention and a manufacturing method thereof, deodorant such as natural phytoncide extract or natural baby powder flavor The more mixed there is no unpleasant odor after the space spray, and as the plant nutrients such as liquid fertilizer, liquid vitamin solution or mineral solution is further mixed, there is an excellent effect of promoting plant growth.

S101 : 원료혼합단계
S102 : 숙성단계
S103 : 균질혼합단계
S104 : 기능성물질혼합단계
S101: Raw material mixing step
S102: ripening step
S103: homogeneous mixing step
S104: Functional substance mixing stage

Claims (11)

바이오디젤 또는 식물성기름 30 내지 50 중량부와, 식물성글리세린 20 내지 50 중량부와, 에탄올 또는 메탄올 20 내지 50 중량부와, 수산화나트륨 1 내지 10 중량부, 물 20 내지 50 중량부가 호모믹싱기 내에서 1000 내지 3000rpm의 속도로 고속교반되어 형성되는 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유.30 to 50 parts by weight of biodiesel or vegetable oil, 20 to 50 parts by weight of vegetable glycerin, 20 to 50 parts by weight of ethanol or methanol, 1 to 10 parts by weight of sodium hydroxide and 20 to 50 parts by weight of water in a homomixer Eco-friendly vegetable base oil for space spray antiseptic disinfectant, characterized in that it is formed by high speed stirring at a speed of 1000 to 3000rpm. 청구항 1에 있어서,
탈취제 1 내지 10 중량부 또는 식물영양제 1 내지 10 중량부가 상기 호모믹싱기 내에 더 첨가되는 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유.
The method according to claim 1,
Eco-friendly vegetable base oil for space spray antiseptic disinfectant, characterized in that 1 to 10 parts by weight of deodorant or 1 to 10 parts by weight of plant nutrients are further added to the homomixer.
청구항 2에 있어서,
상기 물은 수소수 또는 산소수이고, 상기 탈취제는 천연피톤치드추출액 또는 천연베이비파우더향이고, 상기 식물영양제는 액상비료, 액상비타민수용액 및 미네랄수용액 중 하나인 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유.
The method according to claim 2,
The water is hydrogen water or oxygen water, the deodorant is natural phytoncide extract or natural baby powder flavor, the plant nutrient is one of the liquid fertilizer, liquid vitamin solution and mineral aqueous solution, environmentally friendly plant for space spray antiseptic disinfectant Base oil.
바이오디젤 또는 식물성기름에 식물성글리세린을 혼합하는 원료혼합단계; 및
상기 원료혼합단계를 거친 혼합물을 호모믹싱기 내에서 물과 균질혼합하는 균질혼합단계를 포함하고,
상기 원료혼합단계에서는 용매로 에탄올 또는 메탄올이 첨가되고 pH조절제로 수산화나트륨이 첨가되며,
상기 원료혼합단계에서는 상기 바이오디젤 또는 식물성기름 30 내지 50 중량부에 상기 식물성글리세린 20 내지 50 중량부가 혼합되고 상기 에탄올 또는 메탄올 20 내지 50 중량부와 상기 수산화나트륨 1 내지 10 중량부가 첨가되며 35 내지 55℃의 온도 및 60 내지 100rpm의 속도로 30 내지 60분간 교반되는 공간살포 방역소독유용 친환경 식물성 기유의 제조방법.
Raw material mixing step of mixing vegetable glycerin with biodiesel or vegetable oil; And
And a homogeneous mixing step of homogeneously mixing the water mixture in the homomixer with the raw material mixture step.
In the raw material mixing step, ethanol or methanol is added as a solvent and sodium hydroxide is added as a pH adjuster,
In the raw material mixing step, 20 to 50 parts by weight of the vegetable glycerin is mixed with 30 to 50 parts by weight of the biodiesel or vegetable oil, 20 to 50 parts by weight of the ethanol or methanol and 1 to 10 parts by weight of sodium hydroxide are added, and 35 to 55 parts by weight. Method for producing environmentally friendly vegetable base oil for space spray antiseptic disinfectant which is stirred for 30 to 60 minutes at a temperature of 60 ℃ and a speed of 60 to 100rpm.
청구항 4에 있어서,
상기 원료혼합단계와 상기 균질혼합단계 사이에 상기 원료혼합단계를 거친 혼합물을 35 내지 55℃의 온도 및 10 내지 60rpm의 속도로 12 내지 30시간 정도 교반시키는 숙성단계를 더 포함하는 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유의 제조방법.
The method of claim 4,
Space between the raw material mixing step and the homogeneous mixing step of the mixture passed through the raw material mixing step at a temperature of 35 to 55 ℃ and a speed of 10 to 60 rpm for a further 12 to 30 hours, characterized in that the space further comprises a space Method for producing eco-friendly vegetable base oils for spray disinfection and sterilization.
청구항 5에 있어서,
상기 균질혼합단계에서 상기 물은 수소수 또는 산소수로 형성되고 20 내지 50 중량부의 양으로 혼합되며, 50 내지 80℃의 온도 및 1000 내지 3000rpm의 속도로 30 내지 60분간 고속교반되는 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유의 제조방법.
The method according to claim 5,
In the homogeneous mixing step, the water is formed of hydrogen water or oxygen water and mixed in an amount of 20 to 50 parts by weight, and is stirred at high speed for 30 to 60 minutes at a temperature of 50 to 80 ° C. and a speed of 1000 to 3000 rpm. Method for producing eco-friendly vegetable base oils for space spray antiseptic disinfectant.
청구항 4 내지 청구항 6 중 어느 하나의 항에 있어서,
상기 균질혼합단계 이후에 탈취제 1 내지 10 중량부 또는 식물영양제 1 내지 10 중량부를 더 혼합하는 기능성물질혼합단계를 더 포함하는 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유의 제조방법.
The method according to any one of claims 4 to 6,
After the homogeneous mixing step 1 to 10 parts by weight of deodorant or 1 to 10 parts by weight of plant nutrients further comprises a functional material mixing step of producing an environmentally friendly vegetable base oil for space spray antiseptic disinfectant.
청구항 7에 있어서,
상기 탈취제는 천연피톤치드추출액 또는 천연베이비파우더향이고, 상기 식물영양제는 액상비료, 액상비타민수용액 및 미네랄수용액 중 하나인 것을 특징으로 하는 공간살포 방역소독유용 친환경 식물성 기유의 제조방법.
The method of claim 7,
The deodorant is a natural phytoncide extract or natural baby powder flavor, wherein the plant nutrient is a liquid fertilizer, liquid vitamin solution and mineral aqueous solution, characterized in that the manufacturing method of environmentally friendly vegetable base oil for space spray antiseptic disinfectant.
삭제delete 삭제delete 삭제delete
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KR20180062787A (en) 2016-12-01 2018-06-11 주식회사 비코에너지 Eco-friendly cloud spread agent for preventing plant pest and plant disease
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