KR102212624B1 - Aromatic composition containing extract of colored barley for psychological relaxation - Google Patents

Abstract

The present specification relates to a composition capable of relieving stress, and more particularly, to a composition containing colored barley extract to reduce high beta waves generated when stress occurs, thereby reducing stress and helping psychological stability. Therefore, when the colored barley extract of the present specification is used as a fragrance composition, it can be used to relieve the mental stress that modern people receive in daily life and promote psychological stability to keep the mind stable and healthy.

Description

Perfume composition for stress relief and psychological stability enhancement containing colored barley extract {AROMATIC COMPOSITION CONTAINING EXTRACT OF COLORED BARLEY FOR PSYCHOLOGICAL RELAXATION}

The present specification relates to a perfume composition comprising a colored barley extract.

Recently, forest bathing in which you walk or stay in the forest while breathing in fresh and refreshing air is popular.This is known because when you walk in the dense mountains, a fragrance substance called'phytoncide' is emitted from the trees and has a healthy effect on the human body. have. Research on trees that emit phytoncide is actively underway.

KR2002-0063843 A

Accordingly, the present inventors completed the present invention by discovering a colored barley extract that can bring stability to the mind and body by relieving stress while having high odor preference.

An object of the present specification is to provide a perfume composition capable of bringing stability to the mind and body by having a perfume palatability and a stress relief effect by including a colored barley extract.

In order to achieve the above object, the present specification provides a perfume composition for enhancing stress relief and psychological stability comprising a colored barley extract.

The stress relief fragrance composition according to the present specification contains a colored barley extract as a main component, and has a fragrance effect with a good scent and at the same time relieves stress due to the fragrance effect, thereby bringing a mental and physical stability.

1 is a graph comparing the degree of alpha wave with a comparative example when a liquid perfume composition including amethyst reconnaissance, gemstone, ganghocheong or Jeju barley extract according to the present specification is provided to a subject.
FIG. 2 is a graph comparing the degree of beta wave with a comparative example when a liquid perfume composition including amethyst reconnaissance, gemstone, Kanghocheong or Jeju barley extract according to the present specification is provided to a subject.

In one aspect, the present specification may relate to a composition comprising a colored barley extract as an active ingredient.

In one aspect of the present specification, the composition may be a cosmetic composition.

In one aspect of the present specification, the cosmetic composition may include the perfume composition according to the present specification.

In one aspect of the present specification, the composition may be a perfume composition.

In one aspect of the present specification, the composition may be a composition for relieving stress or promoting psychological stability.

In one aspect of the present specification, the composition may be characterized in that it relieves tension, relaxes, stabilizes and relaxes emotions.

In one aspect of the present specification, one or more selected from the group consisting of colored barley, Naeyeong, Oeyeong, and Younggwa may be used, and preferably Younggwa may be used.

In one aspect of the present specification, the colored barley extract may be extracted by mixing young fruit, naeyoung, and outer young at a weight ratio of 1 to 10:1 to 3:1. The weight ratio may be a weight ratio of 6 to 8: 1.5 to 2.5: 1, or a weight ratio of 6:2:2.

In one aspect of the present specification, the colored barley extract may be one or more extracts selected from the group consisting of water, organic solvents, and mixtures thereof. The organic solvent may be one or more selected from the group consisting of ethanol, butylene glycol, and propylene glycol.

In one aspect of the present specification, the perfume composition is a formulation selected from the group consisting of a solid perfume composition, a liquid perfume composition, a perfume, a bath agent, a gel perfume, a liquid type perfume, a liquid type deodorant, an aerosol type deodorant, a gel type sleeping pack, and a scented candle. It can be.

In one aspect of the present specification, the cosmetic composition is a softening lotion, astringent lotion, nourishing lotion, nourishing lotion, nourishing essence, nourishing cream, massage cream, essence, eye cream, eye essence, cleansing cream, cleansing foam, cleansing water, pack , Gel, powder, makeup base, body lotion, body cream, body oil, body essence, lotion, ointment, gel, cream, patch, and spray may be a formulation selected from the group consisting of.

In one aspect of the present invention, the composition may be characterized by increasing alpha waves (α-wave) and reducing beta waves (β-wave) during brain waves.

In this specification, “alpha-wave” refers to a wave corresponding to a frequency of 8 to 13 Hz in an EEG, which means that it comes out of the occipital region of the brain cortex, and an amplitude of 30 at around 10 Hz in normal adult eyes Waves similar to the circumference of ~50γV appear in the occipital region of both sides with dominant left-right symmetry. The amplitude is slightly increased or decreased with a period of 1 to a few seconds. It occurs when a normal adult is relaxed and at rest.

In the present specification, “beta-wave” refers to a wave having a frequency of 13 Hz or more in brain waves in general, and appears during opening of the eye or mental activity in a normal person, and generally has a low amplitude due to a left-right symmetry and has little regularity. It appears especially in a state of tension or excitement, and can be produced even in a stressful state.

In the present specification, “stress relief” refers to alleviating and reducing the degree of stress, which is a non-specific biological reaction that occurs in the body to various injuries and stimuli inflicted on the living body. In particular, it relieves mental stress caused by external factors. Can mean that. It can also mean relieving and relaxing tension.

In the present specification, "psychological stability" does not mean the stability obtained by the body being in a specific position, unlike physical stability, but rather that the mind is relaxed and uneasy in the psychological aspect, and that the mind is in a stable state or that such a state continues. It can mean. It can also mean a state of mind relaxing away from stress, and it can mean calming and relaxing emotions.

In the present specification, "relax" may mean taking a rest or relaxing psychologically and being relieved or relaxed.

In the present specification, colored barley is also called colored barley, functional barley, or functional colored barley, and is an improved species of barley ( Hordeum vulgare L.). Colored barley has a rich content of natural pigments, such as anthocyanins, and colored barley may be black, purple, blue, yellow, purple, green, or red, but is not limited thereto.

In one aspect of the present specification, the colored barley includes amethyst reconnaissance, jewels and ganghocheong, and Jeju barley.

In this specification, amethyst reconnaissance is a kind of barley ( Hordeum vulgare L.), and is registered by applying for variety protection under the Seed Industry Act (variety protection application number: 2009-208, filing date: 2009.03.10, publication date: March 15, 2009, Registration No.: 4891, Registration Date: March 18, 2014). Amethyst reconnaissance is modeled on Thapgolbori (HB78100-B-17-3-2), which is strong in cold resistance and uniforms, has strong disaster resistance, and has a large number of people.It has a high anthocyanin content, has strong disaster resistance, and is strong and strong. It is raised by carrying out artificial breeding with Haga as a copy. The color of the leaves of amethyst is green, the width is medium and the length is short. The color of the net is purple and the length is short. The length of the net is short and there are small thorns on the edge of the net. The soy sauce is about 75 cm, and the head is about 5.4 cm. Growth habit is semi-erect, and there is no hair on lower leaf sheath. The composition of the ear is six lines, the shape of the ear is rod-shaped, and the number density is close to the medium. 1 The number of establishments is 63, multigrained, and the weight of the thousand grains is 27.2g, which is a small and medium-sized species. Purple reconnaissance contains 60.0 to 180.0 ug/g of anthocyanin, has a higher content of beta glucan than ordinary barley, has a lower lip whiteness of 31.6, and has excellent cookability with 403% spreadability. In this specification, amethyst reconnaissance commercially obtained amethyst reconnaissance barley rice sold by Chungmaek, an agricultural corporation.

In this specification, the bail bill is a kind of barley ( Hordeum vulgare L. ), and is registered by applying for variety protection under the Seed Industry Act (variety protection application number: 2009-286, filing date: 2009.05.22, publication date: 2009.6.15, registration number: 4892, registration date: 2014.3.18). Gemstone is grown by artificial crossing between sticky barley with excellent uniformity and cold resistance, high lip whiteness and vein rate due to its abrasion properties, and excellent cooking characteristics, and northern sticky barley in Hamanguk. The growth habits of jewels are semi-upright, and the lower leaves have hairs and the branches are horizontal. Gemstone contains 180ug/g of anthocyanin. The color of the leaf anthocyanin is very light, and there is no or very little white powder in the leaf sheath. The anthocyanin color at the end of the black is medium, the ear white powder is medium, and the hands are upright. The liver of the plant is long and the ear composition is six lines, and the ear shape is rod-shaped and the number density is medium. The length of the mantle is long, the length of the first segment of contraction is short, and the degree of bend of the first segment of the ear neck is weak. Also, the color of the anthocyanin in the catheter in the outer shell of the seed chamber is dark. The length of flowering glume and flowering glumes compared to the central minority seeds and the author's hair are long. In this specification, Geum-cheong was sold as a seed from the Rural Development Administration's National Institute of Food Science and Technology, and the pulsating feed crop division of the rice field.

In this specification, Kang Ho- cheong is a kind of barley ( Hordeum vulgare L.), which was registered by applying for variety protection under the Seed Industry Act (variety protection application number: 2009-398, filing date: 2012.06.22, publication date: 2012.8.15, Publication number: 2012-430). The growth habit of Kang Ho-cheong is semi-upright, there is no leaf anthocyanin color, and there are almost no white powder of leaf sheath. The color of the anthocyanin at the tip is very light, the ear white powder is medium, and the hand part is semi-upright. The soy sauce of Kang Ho-cheong is medium sauce, the ear composition is six lines, and the ear shape is rod-shaped and the water density is medium. The length of the mantle is short, the length of the first segment of contraction is medium, and the degree of bend of the first segment of the ear neck is medium. In addition, the anthocyanin color of the catheter in the seed shell is medium. In the present invention, Kang Ho-cheong received a pre-sale of seeds from the National Institute of Food Science and Technology's Maelstrom Feed Crop Division.

In this specification, Jeju barley is a kind of barley (Hordeum vulgare L.), and is registered by applying for variety protection under the Seed Industry Act (Variety Protection Application No.: 1998-178, Application Date: 1998.12.04, Application Notice No. ; 2000-136, date of application announcement: 2000.02.15). Jeju barley selected SB77460-B-180, an intermediate model with strong uniform resistance, by artificially crossing the security team-Hagane weapon and Samheung-Yunnan in order to cultivate a new variety of high-quality uniforms. After breeding the line by crossing it with the number, 82552-BK-19J-4-0 was selected, and in 1988, it was announced in the main test of the productivity test, and the productivity and main characteristics were tested. This variety was designated as an encouraged variety in 1993 by conducting a regional adaptation test in 1993. The main morphological characteristic is 2 sets of barley, the ear is vertebral and upright, and the water density is very sparse. The growth habit of the plant is medium type, there is no hair in the leaf sheath of the lower leaf, and the concentration of anthocyanin in the leaf is deep, and there is anthocyanin at the end of the leaf, but the concentration is very light. The water outlet belongs to the Mansuk species, the liver is medium, and the end of the degenerate is round. Jongsil author's hair length is long, and the form of Jongsil bast is opposite to each other, and the parseong is Ⅰ. In the present invention, Jeju barley was pre-sale of seeds from the National Institute of Food Science and Technology's Maelstrom Feed Crop Division.

The method of preparing the colored barley extract used in the present specification is not particularly limited, and in the present specification, the colored barley extract is a leachate obtained by leaching and extruding from colored barley, a concentrate obtained by concentrating part or all of the leachate again. It includes an extract produced by drying the concentrate, or an oil obtained by distillation or containing a chemical substance itself exhibiting the main effect contained in the extract.

The colored barley used in the present specification may be included in the form of an extract, or may be included as a pulverized product of the herbal medicine itself, or a dry crushed product of the herbal medicine, but is not limited thereto. In addition, the colored barley used in the present specification is not limited in its acquisition method, and may be used by cultivation or purchased and used, and may be at least one selected from the group consisting of colored barley, Naeyoung, Oeyoung, and Younggwa.

In the present specification, the term "extract" includes all substances obtained by extracting the components of natural substances, regardless of the extraction method, extraction solvent, extracted component, or form of the extract, and other substances obtained by extracting the components of natural substances are extracted. It is a broad concept that encompasses all substances that can be obtained by processing or processing by a method.

In the present specification, “colored barley extract” includes all substances obtained by extracting the components of colored barley, regardless of the extraction method, extraction solvent, extracted component, or form of the extract, and heat and acid in the process of extracting the component It includes a material obtained through an extraction method including a process of treatment with (acid), base, enzyme, etc., and can also be obtained by extracting the material obtained by extracting the components of colored barley and then processing or treating it by other methods. It is a broad concept that includes all substances that are present.

In one aspect of the present specification, the colored barley extract comprises the steps of washing and drying colored barley; Solvent extraction of dried colored barley; And it can be obtained through the step of filtering the extracted colored barley. In the above, the solvent includes at least one selected from the group consisting of water, an organic solvent, and a mixture of water and an organic solvent. In the above, water includes distilled water or purified water, and the organic solvent is selected from the group consisting of alcohol, acetone, ether, ethyl acetate, diethyl ether, ethyl methyl ketone, and chloroform, for example lower alcohols of C ₁ to C ₅ Including one or more, but is not limited thereto.

The colored barley extract may include a colored barley-C ₁ ~C ₆ alcohol extract, and specifically, the alcohol may be methanol or ethanol.

In the present specification, the colored barley extract may be a crude extract of a solvent selected from the group consisting of water, C ₁ -C ₆ alcohol, and combinations thereof. The C ₁ -C ₆ alcohol may be specifically methanol. When the colored barley is extracted with a solvent, it is preferable to extract by adding a solvent corresponding to about 5 to 15 times that of colored barley, and specifically, it is preferable to add about 10 times more solvent to extract, but is not limited thereto. Heat extraction, cold needle extraction, reflux cooling extraction, or ultrasonic extraction may be used for the extraction, and there is no limitation as long as it is an extraction method that is obvious to those skilled in the art. The extraction may be performed at room temperature, but for more efficient extraction, it may be performed under heated conditions, preferably at a temperature of about 40 to 100°C, more preferably about 80°C, but limited thereto. Not. The extraction time may be preferably performed for about 2 to 4 hours, more preferably about 3 hours, but is not limited thereto, and may vary depending on conditions such as an extraction solvent and extraction temperature. The extraction may be extracted once or more several times in order to obtain a larger amount of the active ingredient, preferably 1 to 5 times, more preferably 3 times continuous extraction to use the combined extract.

In the present specification, the colored barley extract may include a crude extract of colored barley as described above, and may also be included as a soluble fraction of an organic solvent obtained by further extracting the crude extract with an organic solvent having a low polarity. As the organic solvent, hexane, methylene chloride, ethyl acetate, n-butanol, etc. may be used, but the present invention is not limited thereto. The extract extracted by the above method or a soluble fraction of the extract may be used as it is, but may be used in the form of an extract after filtration and concentration, or may be freeze-dried after concentration and used as a lyophilized product.

The colored barley extract of the present specification comprises the steps of slicing and drying colored barley; Adding water, an organic solvent, or a combination thereof to the dried colored barley and performing reflux extraction; After depositing the extract, filtering through a filter cloth; Centrifuging the filtrate to separate the residue and the filtrate; Concentrating the separated filtrate under reduced pressure to obtain a colored barley extract; can be obtained by a method comprising.

In one aspect of the present specification, the colored barley extract is composed of purified water, ethanol, butylene glycol, and propylene glycol so that the colored barley concentrate concentrated under reduced pressure according to the above method is included in 5% by weight based on the total weight of the extract. It may be prepared by dispersion/dissolution using one or more solvents selected from the group.

In addition, in the extraction process of the colored barley extract of the present specification, for example, water or an organic solvent is added to the chopped and dried colored barley, followed by reflux extraction and immersion, and then the residue and the filtrate are separated through filter cloth filtration and centrifugation, The separated filtrate is concentrated under reduced pressure to obtain a colored barley extract. The organic solvent usable in the present specification may be selected from ethanol, methanol, butanol, ether, ethyl acetate, chloroform, or a mixed solvent of these organic solvents and water, and when considering the safety of raw materials, preferably 100% water, 70% ethanol Alternatively, butylene glycol (Butylene Glycol) is used. In this case, the extraction temperature is preferably 18 to 80°C for water, 18 to 40°C for 70% ethanol and butylene glycol, and the extraction time is preferably 6 to 168 hours. If the extraction temperature and extraction time are out of the above, extraction efficiency may decrease or a change in components may occur. After obtaining the extract using the solvent above, a liquid product may be obtained by cooling, heating, and filtering at room temperature by a conventional method known in the art, or the solvent may be further evaporated, spray dried, or freeze-dried.

It is preferable that the composition of the present specification contains the colored barley extract in an amount of 0.001 to 50% by weight based on the total weight of the composition. More preferably, 0.001 to 10% by weight, 0.1 to 1% by weight, 2 to 5% by weight, or 0.5 to 10% by weight may be used. In the case of 0.001% by weight or less, it is difficult to expect the efficacy, and when 50% by weight is included, a problem in the formulation occurs. Specifically, the colored barley extract is 0.001% by weight or more, 0.01% by weight or more, 0.1% by weight or more, 0.3% by weight or more, 0.5% by weight or more, 0.8% by weight or more, 1% by weight or more, 2% by weight or more based on the total weight of the composition. , 3% or more, 4% or more, 5% or more, 7% or more, 10% or more, 15% or more, 20% or more, 25% or more, 30% or more, 35% or more , Or 40% by weight or more, and 60% by weight or less or 50% by weight or less.

It is preferable that the cosmetic composition of the present specification contains the perfume composition according to the present specification in an amount of 0.001 to 50% by weight based on the total weight of the cosmetic composition. More preferably, it may be included in 0.001 to 10% by weight, 0.1 to 1% by weight, 2 to 5% by weight, or 0.5 to 10% by weight. In the case of 0.001% by weight or less, it is difficult to expect the efficacy, and when 50% by weight is included, a problem in the formulation occurs. Specifically, the perfume composition according to the present specification is 0.001% by weight or more, 0.01% by weight or more, 0.1% by weight or more, 0.3% by weight or more, 0.5% by weight or more, 0.8% by weight or more, based on the total weight of the cosmetic composition according to the present specification. Wt% or more, 2 wt% or more, 3 wt% or more, 4 wt% or more, 5 wt% or more, 7 wt% or more, 10 wt% or more, 15 wt% or more, 20 wt% or more, 25 wt% or more, 30 It may be greater than or equal to weight%, greater than or equal to 35%, or greater than or equal to 40%, and may be less than or equal to 60% or less than or equal to 50% by weight.

The perfume composition of the present specification is not particularly limited in formulation, but a solid perfume composition, liquid perfume composition, perfume, bath agent, gel perfume, liquid type perfume, liquid type deodorant, aerosol type deodorant, gel type sleeping pack, for liquid It may be a spray, perfumed candle (scented candle) composition.

In addition, in each formulation, other components other than the above-described essential components may be appropriately selected and blended by a person skilled in the art without difficulty according to the type or purpose of use of other formulations.

In one aspect of the present specification, the liquid type perfume composition is 0.1 to 10% by weight of colored barley extract and 30 to 40% by weight of ethanol, 2.0 to 3.0% by weight of Emalex N.P. based on the total weight of the composition. -12, 0.1 to 2.0% by weight of Nicole H.C.O-60, 0.01 to 0.1% by weight of Ubinol D-50 and purified water to be 100% by weight may be included. Specifically, the liquid-type perfume composition comprises 2-5% by weight of colored barley extract and 35-38% by weight of ethanol, 2.2-2.5% by weight of Emalex N.P-12, 0.5-% by weight based on the total weight of the composition. It may contain 1.0% by weight of Nicole H.C.O-60, 0.03 to 0.05% by weight of Ubinol D-50, and purified water to be 100% by weight.

The cosmetic composition according to an aspect of the present specification is not particularly limited in formulation, and may be appropriately selected according to the purpose. For example, skin lotion (soft lotion), astringent lotion, skin softener, skin toner, astringent, lotion, milk lotion (nutrition lotion), moisture lotion, nourishing lotion, massage cream, nourishing cream, moisturizing cream, hand cream, foundation , Essence, eye cream, eye essence, nutrition essence, pack, gel, powder, makeup base, soap, cleansing foam, cleansing lotion, cleansing cream, cleansing water, lotion, ointment, gel, cream, patch, spray, body lotion, It may be prepared in one or more formulations selected from the group consisting of body oil, body essence, and body cleanser, but is not limited thereto.

When the formulation of the cosmetic composition according to the present specification is a paste, cream or gel, animal fibers, plant fibers, wax, paraffin, starch, tracant, cellulose derivatives, polyethylene glycol, silicone, bentonite, silica, talc, or zinc oxide as carrier components Etc. may be used.

When the formulation of the cosmetic composition according to the present specification is a powder or spray, lactose, talc, silica, aluminum hydroxide, calcium silicate or polyamide powder may be used as a carrier component, and in particular, in the case of a spray, additional chlorofluoro Propellants such as hydrocarbon, propane/butane or dimethyl ether.

When the formulation of the cosmetic composition according to the present specification is a solution or emulsion, a solvent, a solvating agent or an emulsifying agent is used as a carrier component, such as water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, Propylene glycol, 1,3-butylglycol oil, glycerol aliphatic ester, polyethylene glycol or fatty acid ester of sorbitan.

When the formulation of the cosmetic composition according to the present specification is a suspension, as a carrier component, a liquid diluent such as water, ethanol or propylene glycol, an ethoxylated isostearyl alcohol, a suspending agent such as polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester , Microcrystalline cellulose, aluminum metahydroxide, bentonite, agar or tracanth, and the like may be used.

In the case of the surfactant-containing cleansing of the cosmetic composition according to the present specification, as carrier components, aliphatic alcohol sulfate, aliphatic alcohol ether sulfate, sulfosuccinic acid monoester, isethionate, imidazolinium derivative, methyltaurate, sarcosinate, Fatty acid amide ether sulfates, alkylamidobetaines, fatty alcohols, fatty acid glycerides, fatty acid diethanolamides, vegetable oils, linoline derivatives, or ethoxylated glycerol fatty acid esters may be used.

In addition to the colored barley extract, the cosmetic composition according to the present specification may further include functional additives and components included in general cosmetic compositions. The functional additive may include a component selected from the group consisting of water-soluble vitamins, oil-soluble vitamins, polymer peptides, polymer polysaccharides, sphingo lipids, and seaweed extract.

In the cosmetic composition of the present specification, in addition to the functional additives, components included in general cosmetic compositions may be blended as needed. Other ingredients included include fats and oils, moisturizers, emollients, surfactants, organic and inorganic pigments, organic powders, ultraviolet absorbers, preservatives, fungicides, antioxidants, plant extracts, pH adjusters, alcohols, pigments, fragrances, blood circulation Accelerators, cooling agents, limiting agents, and purified water.

Hereinafter, the configuration and effects of the present specification will be described in more detail with reference to Examples, Test Examples and Preparation Examples. However, these Examples, Test Examples, and Preparation Examples are provided for illustrative purposes only to aid understanding of the present specification, and the scope and scope of the present specification are not limited by the following examples.

[Preparation Example 1] Preparation of amethyst scout extract

The shredded and shaded amethyst's young, Naeyoung, and Oeyoung were extracted with reflux three times for 24 hours each with a total of 1 kg in a 70% ethanol aqueous solution at a weight ratio of 6:2:2, and then cooled, with Whatman #5 filter paper. Filtered. The filtered extract was concentrated under reduced pressure at 45° C. or lower and freeze-dried at -60° C. for 3 days.

The amethyst extract was prepared by dispersing/dissolving with ethanol so that the reduced pressure concentrate was included in 5% by weight based on the total weight of the amethyst extract.

[Preparation Example 2] Preparation of Gemchal Extract

A gemchal extract was prepared in the same manner as in Preparation Example 1.

[Preparation Example 3] Preparation of Kanghocheong extract

Kanghocheong extract was prepared in the same manner as in Preparation Example 1.

[Preparation Example 4] Preparation of Jeju barley extract

Jeju barley extract was prepared in the same manner as in Preparation Example 1.

[Examples 1 to 4, Comparative Example 1]

After mixing components 1-5 according to the component composition ratio shown in Table 1 below and completely dissolving at 40°C, component 6 was mixed thereto to prepare a liquid type fragrance composition comprising amethyst reconnaissance, gemstone, Kanghocheong or Jeju barley extract. Was prepared.

ingredient Examples 1 to 4
(weight%) Comparative Example 1 (% by weight) 1.ethanol 35 35 2. Extract of any one of Preparation Examples 1 to 4 5 - 3. Emalex N.P-12 2.2 2.2 4. Nicole H. C. Oh-60 0.5 0.5 5. Ubinol D-50 0.03 0.03 6. Purified water to 100 to 100

[Test Example 1] Sensory evaluation for scent

In order to check whether the fragrance of the liquid fragrance composition containing the amethyst reconnaissance, gemstone reconnaissance, Kanghocheong or Jeju barley extract according to Examples 1 to 4 is excellent, 10 males and females each who think they are sensitive to fragrance Was selected and sensory evaluation was conducted. For the sensory evaluation, the liquid perfume of Example 1 was put in an uncontaminated panel room with a width of 3 m, a length of 3 m, and a height of 2 m, and after 24 hours elapsed, 10 sensory assessors of each male and female were placed in the panel room. They were accommodated, and the sensory evaluation was conducted by staying there for 10 minutes to smell the fragrance.

Sensory evaluation was made with respect to the eight questions indicated in the sensory evaluation table of Table 3 below, and the results for Examples 1 to 3 were sequentially described, and the average values for each of 10 males and females are shown in Table 2. For example, the result of Question 1 for Example 1/Example 2/Example 3/Example 4 of Man 1 was described as 1/1/2.

Question 1 Question 2 Question 3 Question 4 Question 5 Question 6 Question 7 Question 8 Man 1 1/1/2/1 1/1/1/1 0/1/1/1 2/1/2/1 2/1/2/1 2/2/2/2 1/1/1/1 2/1/2/1 Man 2 1/2/1/1 1/2/1/1 1/0/1/1 2/2/2/1 1/1/1/1 2/1/2/2 1/1/1/1 2/1/1/1 Man 3 2/2/2/2 1/2/2/1 1/2/1/1 2/1/1/2 2/1/2/2 1/1/1/1 2/1/1/2 1/1/0/1 Man 4 2/1/1/1 1/1/2/1 2/1/1/1 1/0/0/1 2/1/2/2 2/1/2/2 1/1/0/1 2/1/1/2 Man 5 2/1/1/1 2/2/1/2 2/2/2/1 1/1/1/1 1/0/0/1 2/2/1/1 2/2/1/1 1/0/1/1 Man 6 2/2/2/1 2/2/2/1 1/0/1/1 2/2/1/1 2/1/1/1 1/0/0/1 2/1/2/1 2/2/1/2 Man 7 1/2/2/2 2/2/2/2 2/1/2/1 2/1/1/2 1/0/1/1 1/1/1/1 1/1/1/1 1/1/1/1 Man 8 2/2/1/2 2/1/1/2 1/1/0/2 1/0/1/1 2/0/1/1 2/2/1/2 2/2/2/2 1/0/1/1 Man 9 1/1/1/1 1/1/2/1 1/1/1/1 2/1/1/1 2/2/2/2 2/2/1/2 1/1/0/1 2/2/1/1 Man 10 1/2/1/1 2/1/2/1 2/1/2/1 1/1/1/1 1/1/1/1 0/0/0/1 0/1/0/1 1/2/2/2 Average 1.5/1.6/
1.4/1.3 1.5/1.5/
1.6/1.3 1.3/0.9/
1.2/1.1 1.6/1.0/
1.1/1.2 1.6/0.8/
1.3/1.3 1.5/1.2/
1.1/1.5 1.3/1.2/
0.9/1.2 1.5/1.1/
1.1/1.3 Question 1 Question 2 Question 3 Question 4 Question 5 Question 6 Question 7 Question 8 Woman 1 2/2/2/2 1/2/2/1 1/1/1/1 2/2/2/2 0/1/1/1 1/1/1/1 0/1/1/1 0/1/0/1 Woman 2 2/1/2/1 1/1/1/1 2/2/1/2 2/3/2/2 1/2/1/1 0/0/1/1 1/0/1/1 1/0/1/1 Woman 3 1/1/1/1 2/1/2/2 2/1/2/2 2/2/1/1 1/2/2/2 1/2/1/1 2/1/2/2 1/2/1/1 Woman 4 1/1/1/1 2/2/1/1 2/2/2/2 1/2/1/2 2/2/2/2 2/2/2/2 2/3/3/2 2/3/2/2 Woman 5 2/2/2/2 2/2/2/2 2/2/2/2 1/2/2/1 1/1/1/1 2/1/2/1 2/3/3/3 1/1/1/1 Woman 6 2/1/1/1 2/2/2/2 1/1/0/1 2/3/3/3 2/1/2/2 1/1/0/2 2/3/2/2 2/3/1/1 Woman 7 2/2/1/1 2/1/2/1 2/1/2/1 2/3/2/2 2/3/3/2 0/1/1/1 2/1/3/2 0/0/0/1 Woman 8 2/2/2/1 2/2/1/1 1/0/1/1 1/2/1/1 2/2/3/2 2/1/1/1 2/2/2/2 1/0/1/1 Woman 9 2/1/2/2 1/2/1/2 2/2/2/2 2/3/3/2 2/3/3/3 1/1/1/1 1/1/0/1 2/1/1/1 Woman 10 2/2/2/1 2/2/2/2 2/2/2/1 1/1/1/2 2/2/1/2 0/0/1/1 1/0/1/2 1/3/2/2 Average 1.8/1.5/
1.6/1.3 1.7/1.7/
1.6/1.5 1.7/1.4/
1.5/1.5 1.6/2.3/1.8/1.8 1.5/1.9/
1.9/1.8 1.0/1.0/
1.1/1.2 1.5/1.5/
1.8/1.8 1.1/1.4/
1.0/1.2

As can be seen from the results of Table 2, it can be seen that the fragrance composition including the amethyst reconnaissance, jewel-cheong, Kanghocheong or Jeju barley extract of the present specification has excellent scent. Therefore, when used as a fragrance composition, there is no effect that causes a feeling of rejection to consumers, but rather provides a good scent to confirm that there is no reluctance to use.

[Test Example 2] Measurement of Physiological/Psychological Effects of Liquid Perfume Composition

In order to objectively evaluate the physiological/psychological effect of the perfume composition, a liquid perfume composition was provided, and brain waves (EEG) of the central nervous system were measured. The specific method is as follows.

1. Subject

The subjects were 20 women in their twenties to thirties who were healthy, do not currently take drugs, and are not intoxicated.

On the day before the experiment, excessive exercise or excessive intake of alcohol was refrained, and on the day of the experiment, smoking, drinks, drugs, and gum intake that may affect the central nervous system and olfactory sense were refrained from ingesting. As an experiment with adult females, it was reported that there was a correlation between the change in the sense of smell according to the female's sexual cycle and the female's menstrual cycle and mood.

2. Experimental sample

As the experimental samples, Examples 1 to 4, which are liquid perfume compositions according to Table 1, were used, and the control group was used as Comparative Example 1. The physiological response was measured while the subjects smelled the fragrance provided during the experiment.

3. Experimental conditions

The experiment was conducted in an olfactory laboratory (4.8 m×3 m×2.4 m), and there are intake and exhaust facilities for the purpose of reducing the adaptation of the sense of smell inside, maximizing the participation of the subject and the influence of the external environment during the experiment. A soundproofing device is installed to rule out the problem. During the experiment, the internal temperature (25°C), humidity (40-50%), and illuminance (150-200 Lx) were kept constant. After the experiment for one condition was completed, the subject was allowed to rest sufficiently so that there was no effect on the adaptation of fragrance and fatigue, and the experiment was conducted after ventilating the interior of the laboratory.

4. How to measure

For EEG, attach electrodes for EEG measurement (GRASS, USA) to the frontal, parietal, temporal, and occipital lobes according to the international 10-20 electrode placement method, and GRASS (USA) equipment, MP 100 system (USA), Acknowledge program ( USA). The resistance value between each measurement part was set to 10 ㏀ or less, and the sampling rate was set to 512 Hz.

5. Experimental method

The subject provided scent with the eyes closed, and physiological signals were measured while smelling the scent. The fragrance container was placed 1-2 cm below the nose and served for 1 minute. In order to exclude the effect of ordering on the scent, the order of providing scent for each subject was performed at random.

6. Analysis method

In the experiment, a total of 20 female subjects were measured and data was analyzed. Brain waves were analyzed by the power spectrum by the FFT method, and then α/(α+β+θ+δ) and β/(α+β+θ+δ) were calculated according to the frequency band.

7. Experiment results

The central nervous response according to the fragrance was measured by EEG and the ratio of the relative alpha wave and the relative beta wave was analyzed. 1 is a result of analyzing the relative alpha wave ratio after use of the perfume composition of the present specification.

According to the results of FIG. 1, the example showed a higher ratio of alpha waves that appear upon sedation/relaxation compared to the comparative example.

Alpha waves are brain waves that appear when a person is in a comfortable state, and the fact that the ratio is high means that the subject is comfortable accepting the proposed scent, and the scent that is highly activated alpha waves makes the human body feel relaxed, calm, and comfortable.

2 is a result of analyzing the ratio of the relative beta wave according to the use of the perfume composition of the present specification.

According to the results of FIG. 2, the ratio of the relative beta wave decreased when the Example was presented rather than the Comparative Example. Beta waves are brain waves that appear when anxious or tense, and the high rate means that the test subject is tense or aroused. It can be supported that the manufacturing example has a relaxing effect.

Therefore, it was confirmed that the fragrance composition containing the amethyst reconnaissance, Kang Ho-cheong, Gum-cheong, or Jeju barley extract according to the present specification showed an effect of increasing the alpha wave and decreasing the beta wave of the subject, thereby reducing stress and psychological It was confirmed that there is an effect of enhancing stability.

An example of the formulation of the composition according to an aspect of the present specification is described below, but it can be applied to various other formulations, which is not intended to limit the present specification, but is intended to be described in detail.

[Formulation Example 1] Solid Perfume Composition

A solid flavor composition was prepared by adding 8 g of the extract of any one of Preparation Examples 1 to 4, 100 g of tatrium bicarbonate powder, and 30 g of citric acid powder, mixed uniformly, put in a mold, pressed and hardened for 5 hours.

[Formulation Example 2] Liquid fragrance composition

A liquid perfume composition was prepared in an amount according to Table 3 below by a conventional method in the art.

ingredient Content (% by weight) ethanol 35 The extract of any one of Preparation Examples 1 to 4 5 Emalex N.P-12 2.2 Nicole H. C. Oh-60 0.5 Ubinol D-50 0.03 Purified water to 100

[Formulation Example 3] Perfume

Perfume was prepared in the amount according to Table 4 below by a conventional method in the art.

ingredient Content (% by weight) The extract of any one of Preparation Examples 1 to 4 20 Alcohol 78 water 2 Pigment Appropriate amount Discoloration inhibitor Appropriate amount

[Formulation Example 4] Bath agent

The bath agent in the amount according to Table 5 below was prepared by a conventional method in the art. Alternatively, the ingredients excluding the fragrance were stirred with a V-type mixer until they became uniform, and then amethyst reconnaissance, jewel chapel, Kanghocheong or Jeju barley extract was added, and the mixture was sufficiently stirred until it became more uniform to obtain a bath agent.

ingredient Content (% by weight) The extract of any one of Preparation Examples 1 to 4 One Sodium hydrogen carbonate 70 Anhydrous sodium sulfate 28.8 Pigment Y-202-1 0.2

[Formulation Example 5] Gel fragrance

A gel fragrance was prepared in an amount according to Table 6 below by a conventional method in the art. Or carrageenan, propylene glycol, and propylarapene were mixed, water was added while stirring, and the mixture was heated until it reached about 80°C while warmly stirring. After that, set it to about 65℃, and while stirring it at 3000rpm using a homogenizer, add amethyst reconnaissance, gemstone, ganghocheong or Jeju barley extract to make a uniform phase, then flow into a predetermined container, and then naturally cool the gel. A fragrance was prepared.

ingredient Content (% by weight) The extract of any one of Preparation Examples 1 to 4 5.0 Carrageenan 3.0 Propylene glycol 2.0 Profile Paraben 0.3 water 89.7

[Formulation Example 6] Liquid type fragrance

A liquid type fragrance was prepared in an amount according to Table 7 below by a conventional method in the art. Alternatively, each component was mixed except for water, and water was added while stirring warmly to obtain a fragrance. In addition, polyoxyethylene nonylphenyl ether EO-13 was used as a surfactant.

ingredient Content (% by weight) The extract of any one of Preparation Examples 1 to 4 3.0 95% ethanol 25.0 Surfactants 5.0 water 67.0

[Formulation Example 7] Liquid type deodorant

A liquid type deodorant was prepared in an amount according to Table 8 below by a conventional method in the art. Alternatively, each component other than water was mixed and water was added while warmly stirring to obtain a deodorant (liquid type). In addition, polyoxyethylene nonylphenyl ether EO-10 was used as a surfactant.

ingredient Content (% by weight) The extract of any one of Preparation Examples 1 to 4 5.0 95% ethanol 10.0 Surfactants 10.0 1% anisaldehyde (ethanol solution) 65.0 water 10.0

[Formulation Example 8] Aerosol type deodorant

An aerosol type was prepared in the amount according to Table 9 below by a conventional method in the art. Alternatively, components other than liquefied petroleum gas were mixed and stirred to make it uniform, and a predetermined amount was put into an aerosol container and a valve was mounted, and then liquefied petroleum gas was injected to obtain a deodorant (aerosol type).

ingredient Content (% by weight) The extract of any one of Preparation Examples 1 to 4 5.0 95% ethanol 20.0 Liquefied petroleum gas (4.0kg/cm ² , 20℃) 25.0 1% anisaldehyde (ethanol solution) 10.0 water 40.0

[Formulation Example 9] Flexible lotion (skin lotion)

According to the composition shown in Table 10 below, a flexible lotion was prepared by a conventional method.

Ingredients Content (% by weight) The extract of any one of Preparation Examples 1 to 4 0.2 glycerin 3.0 Butylene glycol 2.0 Propylene glycol 2.0 Carboxyvinyl polymer 0.1 PEG-12 nonylphenyl ether 0.2 Polysorbate 80 0.4 ethanol 10.0 Triethanolamine 0.1 Preservatives, colors, flavors Appropriate amount Purified water Balance

[Formulation Example 10] Nutritional lotion (milk lotion)

Nutrient cosmetic water was prepared by a conventional method according to the composition shown in Table 11 below.

Ingredients Content (% by weight) The extract of any one of Preparation Examples 1 to 4 1.0 glycerin 3.0 Butylene glycol 3.0 Propylene glycol 3.0 Carboxyvinyl polymer 0.1 Beeswax 4.0 Polysorbate 60 1.5 Caprylic/Capric Triglyceride 5.0 Squalane 5.0 Solvitasesquioleate 1.5 Floating paraffin 0.5 Cetearyl alcohol 1.0 Triethanolamine 0.2 Preservatives, colors, flavors Appropriate amount Purified water Balance

[Formulation Example 11] Nourishing Cream

A nutrient cream was prepared by a conventional method according to the composition shown in Table 12 below.

Ingredients Content (% by weight) The extract of any one of Preparation Examples 1 to 4 2.0 glycerin 3.0 Butylene glycol 3.0 Floating paraffin 7.0 Beta glucan 7.0 Carbomer 0.1 Caprylic/Capric Triglyceride 3.0 Squalane 5.0 Cetearyl glucoside 1.5 Sorbitan Stearate 0.4 Polysorbate 60 1.2 Triethanolamine 0.1 Preservatives, colors, flavors Appropriate amount Purified water Balance

[Formulation Example 12] Massage Cream

A massage cream was prepared by a conventional method according to the composition shown in Table 13 below.

Ingredients Content (% by weight) The extract of any one of Preparation Examples 1 to 4 2.0 glycerin 8.0 Butylene glycol 4.0 Floating paraffin 45.0 Beta glucan 7.0 Carbomer 0.1 Caprylic/Capric Triglyceride 3.0 Beeswax 4.0 Cetearyl glucoside 1.5 Sesqui oleic acid sorbitan 0.9 Vaseline 3.0 paraffin 1.5 Preservatives, colors, flavors Appropriate amount Purified water Balance

[Formulation Example 13] Pack (gel type sleeping pack)

A pack was prepared by a conventional method according to the composition shown in Table 14 below.

Ingredients Content (% by weight) The extract of any one of Preparation Examples 1 to 4 0.2 glycerin 4.0 Polyvinyl alcohol 15.0 Hyaluronic acid extract 5.0 Beta glucan 7.0 Allantoin 0.1 Nonyl phenyl ether 0.4 Polysorbate 60 1.2 Ethanol preservative 6.0 Preservatives, colors, flavors Appropriate amount Purified water Balance

As described above, a specific part of the present specification has been described in detail, and it is clear that this specific technology is only a preferred embodiment for those of ordinary skill in the art, and the scope of the present specification is not limited thereto. Accordingly, it will be said that the substantial scope of the present specification is defined by the appended claims and their equivalents.

Claims (13)

A fragrance composition comprising a colored barley extract as an active ingredient. The composition of claim 1, wherein the colored barley is at least one selected from the group consisting of amethyst reconnaissance, gemstone, Kanghocheong and Jeju barley. The composition of claim 1, wherein the composition increases alpha wave (α-wave) and decreases beta wave (β-wave) during brain waves. The composition according to claim 1, wherein the colored barley is at least one selected from the group consisting of colored barley, Naeyoung, Oeyoung, and Younggwa. The composition of claim 1, wherein the extract is at least one extract selected from the group consisting of water, an organic solvent, and a mixture thereof. The composition of claim 5, wherein the organic solvent is at least one selected from the group consisting of ethanol, butylene glycol and propylene glycol. The composition of claim 1, wherein the composition comprises 0.001 to 10% by weight of the extract based on the total weight of the composition. The composition of claim 1, wherein the composition comprises 2 to 5% by weight of the extract based on the total weight of the composition. The composition of claim 1, wherein the perfume composition is a formulation selected from the group consisting of solid perfume composition, liquid perfume composition, perfume, bath agent, gel perfume, liquid type perfume, liquid type deodorant, aerosol type deodorant, gel type sleeping pack, and scented candle. . The composition of claim 1, wherein the composition is a composition for relieving stress or promoting psychological stability. A cosmetic composition comprising the perfume composition according to any one of claims 1 to 10. The composition of claim 11, wherein the cosmetic composition comprises 0.001 to 10% by weight of the perfume composition based on the total weight of the cosmetic composition. The method of claim 11, wherein the cosmetic composition is a softening lotion, astringent lotion, nutrition lotion, nutrition lotion, nutrition essence, nutrition cream, massage cream, essence, eye cream, eye essence, cleansing cream, cleansing foam, cleansing water, pack, gel , Powder, makeup base, body lotion, body cream, body oil, body essence, lotion, ointment, gel, cream, patch, and spray composition.

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