KR102090047B1 - Shampoo composition comprising makgeolli fermentation material and mathod for manufacturing the same - Google Patents

Abstract

Disclosed herein is a shampoo composition comprising a makgeolli fermentation product and a method of making the same. The composition comprises a base oil; glycerin; Fermented rice wine; An extract mixture comprising yeast extract, eoseongcho extract, cotyledon extract and green tea extract; And Lactobacillus fermentation product fermenting persimmon, oat, corn, and basil as a strain of genus Lactobacillus, and the composition is excellent in improving the scalp or dandruff without adding side effects or irritation to the scalp or hair.

Description

Shampoo composition containing makgeolli fermentation product and its manufacturing method {SHAMPOO COMPOSITION COMPRISING MAKGEOLLI FERMENTATION MATERIAL AND MATHOD FOR MANUFACTURING THE SAME}

Disclosed herein is a shampoo composition comprising a makgeolli fermentation product and a method of making the same.

In modern society, people who are suffering from itchy scalp and dandruff symptoms are increasing due to stress, pollution of air and water. Frequent staining or perm can cause scalp damage, itching, and inflammation, especially if the user's scalp is sensitive. Since such scalp damage or itchiness may eventually lead to hair loss, and when hair loss progresses, severe psychological pain is also involved, so it is necessary to prevent hair loss by preventing scalp damage or generation of dandruff-causing bacteria and to provide hair with moisturizing and antibacterial properties. Do.

In addition, in recent years, consumers have increased their preference for products containing natural materials rather than synthetic products. Various methods have been developed to improve symptoms such as eczema, for example, by removing the antigen and strengthening the skin barrier function, or by containing an adrenal cortical hormone agent in an external preparation for the skin to weaken the allergic reaction, and as an antibacterial agent 2 Methods such as preventing tea infection have been used. However, despite containing useful components, it may cause problems because it contains chemical components having irritating properties such as chemical preservatives, chemical thickeners, such as synthetic surfactants, artificial flavors, and artificial color parabens, which are detergents. Rather, it is possible to result in counteracting the intrinsic function of raw materials having therapeutic functions. Accordingly, there is a need for a shampoo composition having an effect of improving scalp or dandruff without side effects or irritation to the scalp or hair.

Korean Registered Patent Publication No. 10-1033307

In one aspect, the present specification aims to provide a shampoo composition excellent in improving the scalp or improving dandruff.

In another aspect, the present disclosure aims to provide a method for preparing a shampoo composition having an excellent effect of improving scalp or dandruff.

In one aspect, the technology disclosed herein comprises a base oil; glycerin; Fermented rice wine; An extract mixture comprising yeast extract, Eoseongcho leaf extract, cotyledon leaf extract and green tea leaf extract; And Lactobacillus ( Lactobacillus spp .) Strain provides a shampoo composition comprising a fermented Lactobacillus fermentation of persimmon, oat, corn and basil leaves.

In one exemplary embodiment, the shampoo composition, based on the total weight of the shampoo composition, 0.1 to 1% by weight of base oil; Glycerin 1 to 3% by weight; Makgeolli fermentation product 1 to 10% by weight; 0.5 to 5% by weight of the extract mixture; And 1 to 10% by weight of the fermentation product of Lactobacillus.

In an exemplary embodiment, the extract mixture may further include a beet extract, a tooth extract, a Western Songak extract, and a dry extract.

In one exemplary embodiment, the extract mixture is 5 to 10% by weight of yeast extract, 10 to 15% by weight of Eoseongcho extract, 10 to 15% by weight of cotyledon extract, 10 to 15% by weight of green tea extract, 5 to 10% by weight of beet extract %, 15 to 20% by weight of tooth extract, 10 to 15% by weight of Western Songak extract and 5 to 20% by weight of dry extract.

In one exemplary embodiment, the persimmon juice, oats, corn, and basil may be fermented by mixing in a weight ratio of 6 to 10: 2 to 6: 1 to 3: 1.

In one exemplary embodiment, the Lactobacillus strain is Lactobacillus pentosus , Lactobacillus plantarum , Lactobacillus casei and Lactobacillus rhamnosus as Lactobacillus rhamsus It may be one or more selected from the group consisting of.

In one exemplary embodiment, the shampoo composition may be to improve scalp or dandruff.

In another aspect, the technology disclosed herein is a method for preparing the shampoo composition, comprising: primary mixing of base oil, glycerin and rice wine fermentation product; Adding the extract mixture including yeast extract, Eoseongcho extract, cotyledon extract and green tea extract to the primary mixture for secondary mixing; And adding a fermentation product of Lactobacillus to the secondary mixture.

In one aspect, the technology disclosed herein has an effect of providing a shampoo composition having an excellent effect of improving scalp or dandruff without applying side effects or irritation to the scalp or hair.

In another aspect, the technology disclosed herein has an effect of providing a method of manufacturing a shampoo composition having an excellent effect of improving scalp or dandruff.

Hereinafter, the present invention will be described in detail.

In one aspect, the technology disclosed herein comprises a base oil; glycerin; Fermented rice wine; An extract mixture comprising yeast extract, eoseongcho extract, cotyledon extract and green tea extract; And Lactobacillus genus ( Lactobacillus spp .) Provides a shampoo composition comprising a fermented Lactobacillus fermentation of persimmon, oat, corn, and basil.

In one exemplary embodiment, the shampoo composition, based on the total weight of the shampoo composition, 0.1 to 1% by weight of base oil; Glycerin 1 to 3% by weight; Makgeolli fermentation product 1 to 10% by weight; 0.5 to 5% by weight of the extract mixture; And 1 to 10% by weight of the fermentation product of Lactobacillus provides excellent scalp improvement or dandruff improvement effect.

In another exemplary embodiment, the shampoo composition, based on the total weight of the shampoo composition, 0.1 to 1% by weight of base oil; 1 to 2% by weight of glycerin; 4 to 8% by weight of fermented rice wine; 2 to 4% by weight of the extract mixture; And 4 to 6% by weight of the fermented product of Lactobacillus.

In one exemplary embodiment, the base oil may be one or more selected from the group consisting of palm oil, camellia seed oil, olive oil, evening primrose oil, jojoba seed oil, avocado oil, apricot seed oil, coconut oil and castor oil.

In the present specification, the makgeolli fermentation product refers to a filtered product of a fermentation product prepared according to a conventional makgeolli manufacturing method, and refers to a fermentation broth obtained by using rice and yeast as the main material.

In one exemplary embodiment, the yeast may include Aspergillus oryzae .

In the present specification, the extract mixture may be obtained by extracting and then mixing each substance to be extracted, or may be extracted together after mixing one or more substances to be extracted.

In the present specification, the extract means not only the crude extract but also the processed product of the extract, for example, drying, concentration, fractionation, purification, and fermentation, including all forms by additional processing. In addition, the extract may be obtained by purchasing a commercially available one, or by appropriately selecting, combining, adding or changing a conventional extraction method used in the art.

In an exemplary embodiment, the extract is, but is not limited to, water, lower alcohol having 1 to 4 carbon atoms (for example, methanol, ethanol, butanol, etc.), ethylene, acetone, hexane, ether, chloroform, ethyl Acetate, butyl acetate, dichloromethane, dimethylformamide (DMF), methylene chloride, dimethylsulfoxide (DMSO), glycerin, butylene glycol, propylene glycol, dipropylene glycol, methylene chloride and diethyl ether. It may be extracted with one or more extraction solvents.

In one exemplary embodiment, the method for preparing the extract is hot water extraction, supercritical extraction, subcritical extraction, cold immersion extraction, high temperature extraction, reflux cooling extraction, high pressure extraction, ultrasonic extraction or adsorption including XAD and HP-20 Conventional extraction methods in the art, such as extraction using a resin, can be used. Specifically, while heating, reflux extraction or reflux extraction at room temperature may be performed, but is not limited thereto. In addition, the extraction solvent may be extracted by adding a solvent corresponding to about 1 to 15 times of the dry matter, and specifically, it may be extracted by adding a solvent of about 10 times, but is not limited thereto. In addition, the number of extractions may be 1 to 5 times, and specifically, it may be repeatedly extracted 3 times, but is not limited thereto, and the extraction time may be 2 to 100 hours, specifically 10 to 70 hours, It is not limited.

In an exemplary embodiment, the yeast extract is fermented with yeast, such as Saccharomyces cerevisiae , in a culture medium, and then centrifuged the yeast and the culture solution to remove the supernatant, and the obtained yeast component is distilled. After washing with may be obtained by extracting hot water.

In an exemplary embodiment, the extract mixture may further include a beet extract, a tooth extract, a Western Songak extract, and a dry extract.

In an exemplary embodiment, the extract mixture may further include beetroot extract, chia seed extract, oleander leaf extract and dried leaf extract.

In one exemplary embodiment, the extract mixture is 5 to 10% by weight of yeast extract, 10 to 15% by weight of Eoseongcho extract, 10 to 15% by weight of cotyledon extract, 10 to 15% by weight of green tea extract, 5 to 10% by weight of beet extract %, 15 to 20% by weight of tooth extract, 10 to 15% by weight of Western Songak extract, and 5 to 20% by weight of dry extract, to provide excellent scalp improvement or dandruff improvement effect.

Lactobacillus fermentation in the present specification means a filtrate of fermentation fermented with a Lactobacillus strain.

In one exemplary embodiment, the persimmon, oats, corn and basil are fermented by mixing in a weight ratio of 6 to 10: 2 to 6: 1 to 3: 1, or 6 to 8: 3 to 5: 1 to 2: 1 This may be most desirable in terms of improving the scalp or improving dandruff.

In one exemplary embodiment, the Lactobacillus strain is Lactobacillus pentosus , Lactobacillus plantarum , Lactobacillus casei and Lactobacillus rhamnosus as Lactobacillus rhamsus It may be one or more selected from the group consisting of.

In one exemplary embodiment, the shampoo composition may be to improve scalp or dandruff. The shampoo composition according to the present specification has high safety to the scalp or hair without applying side effects or irritation to the scalp or hair.

The shampoo composition according to the present specification is an interface comprising at least one selected from the group consisting of natural surfactants, anionic surfactants, nonionic surfactants, cationic surfactants and amphoteric surfactants commonly used in the art. It may contain an active agent.

In one exemplary embodiment, the composition is an aliphatic alcohol sulfate, an aliphatic alcohol ether sulfate, a sulfosuccinic acid monoester, isethionate, an imidazolinium derivative, methyltaurate, sarcosinate, fatty acid amide ether sulfate as carrier components, Alkylamidobetaines, aliphatic alcohols, fatty acid glycerides, fatty acid diethanolamides, linoline derivatives or ethoxylated glycerol fatty acid esters and the like can be used.

In another aspect, the technology disclosed herein is a method for preparing the shampoo composition, comprising: primary mixing of base oil, glycerin and rice wine fermentation product; Adding the extract mixture including yeast extract, Eoseongcho extract, cotyledon extract and green tea extract to the primary mixture for secondary mixing; And adding a fermentation product of Lactobacillus to the secondary mixture.

In an exemplary embodiment, the makgeolli fermentation product is prepared by cooking rice, preparing godubap, or rice cake, followed by stirring while adding yeast and water thereto; Heating after fermentation; And cooling and then filtering to obtain a filtrate.

In one exemplary embodiment, the Lactobacillus fermentation product is inoculated with Lactobacillus strains in persimmon, oat, corn, and basil, and fermented at 35 to 40 ° C for 1 to 20 days, more preferably 3 to 10 days, followed by filtration. It can be prepared, including the step of obtaining a filtrate.

Hereinafter, the present invention will be described in more detail through examples. These examples are only for illustrating the present invention, it will be apparent to those skilled in the art that the scope of the present invention is not to be construed as limited by these examples.

Example.

Rice flour was prepared at 100 ° C or higher, and then stirred while loosening by adding 500 g of yeast and 1,000 ml of water. Then, fermentation at 25 ° C. for 3 days, heating and cooling, followed by filtration to obtain a makgeolli fermentation product.

In addition, persimmon, oat, corn, and basil were mixed in a weight ratio of 8: 5: 2: 1, and then inoculated with Lactobacillus plantarum strain (KCTC3103) at 1 × 10 ^7-8 cfu / ml for 3 days at 37 ° C. Cultured for a while. After incubation for 2 days after cultivation, the filtrate was obtained by filtration, and the pH of the filtrate was adjusted to 6.5, followed by freeze-drying to obtain a Lactobacillus fermentation product.

After primary stirring by mixing castor oil and glycerin as base oil in the makgeolli fermentation product, yeast ( Saccharomyces cerevisiae ) extract, Houttuynia cordata extract, Perilla Frutescens extract, Green tea ( Camellia sinensis ) extract, The beet ( Beta vulgaris ) root extract, chia ( Salvia hispanica ) seed extract, Hedera helix leaf extract and dried ( Trapa japonica ) leaf extract were mixed and stirred for a second time. The extract was obtained by hot water extraction of each extraction target material. Subsequently, an active ingredient of the shampoo composition was prepared by adding the fermented product of Lactobacillus.

The shampoo was prepared by a conventional shampoo manufacturing method according to the composition of Table 1 below using the active ingredient of the shampoo composition. Specifically, a surfactant and ethylene glycol distearate were added to purified water, heated to 80 ° C. to dissolve uniformly, and then slowly cooled to 40 ° C. with stirring. Then, the active ingredient and the rest of the components of the prepared shampoo composition were added and mixed, and then cooled to room temperature while stirring to prepare a shampoo.

ingredient Example 1 Comparative Example 1 Comparative Example 2 Ammonium lauryl sulfate 10 10 10 Polyoxyethylene lauryl ammonium sulfate 5 5 5 Cocoamidopropylbetaine 2 2 2 Ethylene glycol distearate 1.5 1.5 1.5 Cocoyl monoethanolamide 0.8 0.8 0.8 Rice wine fermentation 5 5 5 Lactobacillus fermentation 5 5 - Extract mixture A
(Yeast extract, Eoseongcho extract, cotyledon extract and green tea extract) - 3 - Extract mixture B
(Yeast extract, Eoseongcho extract, cotyledon extract, green tea extract, beetroot extract, chia seed extract, oleander leaf extract and dry leaf extract) 3 - 3 glycerin 2 2 2 Polyquaternium-10 0.2 0.2 0.2 Castor oil 0.3 0.3 0.3 Spices 0.8 0.8 0.8 Citric acid 0.1 0.1 0.1 Dimethicone One One One water to 100 to 100 to 100

Experimental Example 1. Scalp improvement effect

30 men and women aged 25 to 55 who feel the itching of the scalp relatively relatively are randomly divided into three groups of 10 each, and the shampoos of Example 1, Comparative Example 1 and Comparative Example 2 are taken once every 2 days for 2 weeks. After using it, the effect of improving the scalp, including the improvement of itching of the scalp, was evaluated through the following evaluation criteria, and the average value is shown in Table 2 below.

[Evaluation standard]

Very good-5 points

Excellent-4 points

Normal-3 points

The effect is negligible-2 points

No effect-1 point

division Example 1 Comparative Example 1 Comparative Example 2 Scalp improvement effect 4.1 3.3 2.9

As can be seen from Table 2, the shampoo of Example 1 exhibited a better scalp improvement effect compared to the shampoos of Comparative Example 1 (with extract mixture A) and Comparative Example 2 (without Lactobacillus fermentation product).

Experimental Example 2. Effect of improving dandruff

Thirty males aged 20 to 40 with a lot of dandruff were selected and randomly divided into three groups of 10 each to use the shampoos of Example 1, Comparative Example 1 and Comparative Example 2 once a day for 2 months. Then, the effect of improving dandruff through the following dandruff reduction rate was evaluated and shown in Table 3 below.

Specifically, it was made to shampoo with a normal shampoo before the start of the test, and the dandruff accumulated for 3 days after the washing was collected, and the weight of the collected dandruff and the shampoos of Example 1, Comparative Example 1 and Comparative Example 2 were limited to 2 days. After washing three times and collecting dandruff accumulated for 3 days after the test of 1 month, the weight of the collected dandruff was measured. The accumulated dandruff was collected and measured directly from the scalp with a vacuum suction device, and the average value of the calculated dandruff reduction rate is shown in Table 3 below.

Dandruff reduction rate (%) = {weight of dandruff (mg) before test start-weight of dandruff 1 month after test start} × 100 / weight of dandruff before test start (mg)

division Example 1 Comparative Example 1 Comparative Example 2 Dandruff improvement effect 56.23 17.38 14.75

As can be seen in Table 3, the shampoo of Example 1 had a very good effect of improving dandruff compared to the shampoos of Comparative Example 1 (with extract mixture A) and Comparative Example 2 (without Lactobacillus fermentation product).

As described above, since a specific part of the present invention has been described in detail, for those skilled in the art, this specific technique is only a preferred embodiment, and the scope of the present invention is not limited thereby. It will be obvious. Therefore, the substantial scope of the present invention will be defined by the appended claims and their equivalents.

Claims (8)

Base oil;
glycerin;
Fermented rice wine;
An extract mixture comprising yeast extract, eoseongcho extract, cotyledon extract and green tea extract; And
Shampoo composition comprising Lactobacillus fermentation product fermenting persimmon, oat, corn and basil with Lactobacillus spp . Strain.
According to claim 1,
The shampoo composition is based on the total weight of the shampoo composition,
0.1 to 1% by weight of base oil;
Glycerin 1 to 3% by weight;
Makgeolli fermentation product 1 to 10% by weight;
0.5 to 5% by weight of the extract mixture; And
Shampoo composition comprising 1 to 10% by weight of Lactobacillus fermentation.
According to claim 1,
The extract mixture will further include a beet extract, tooth extract, Western Songak extract and dry extract, shampoo composition.
According to claim 3,
The extract mixture is yeast extract 5 to 10% by weight, Eoseongcho extract 10 to 15% by weight, cotyledon extract 10 to 15% by weight, green tea extract 10 to 15% by weight, beet extract 5 to 10% by weight, tooth extract 15 to 20 Shampoo composition comprising, by weight, 10 to 15% by weight of Western Songak extract and 5 to 20% by weight of dry extract.
According to claim 1,
The persimmon juice, oats, corn and basil are fermented by mixing in a weight ratio of 6 to 10: 2 to 6: 1 to 3: 1.
According to claim 1,
The strain of genus Lactobacillus is selected from the group consisting of Lactobacillus pentosus , Lactobacillus plantarum , Lactobacillus casei and Lactobacillus rhamnosus . , Shampoo composition.
According to claim 1,
The shampoo composition is to improve the scalp or dandruff, shampoo composition.
A method for producing a shampoo composition according to any one of claims 1, 2, and 5 to 7,
First mixing base oil, glycerin and rice wine fermentation;
Adding the extract mixture including yeast extract, Eoseongcho extract, cotyledon extract and green tea extract to the primary mixture for secondary mixing; And
Method of manufacturing a shampoo composition comprising the step of adding a fermentation product of Lactobacillus to the secondary mixture.