KR102025169B1 - Water-Soluble Jade Extract and Preparation Method Thereof - Google Patents

Abstract

The present invention provides a method for producing a water-soluble jade extract, comprising the steps of: purifying powdered jade (S10); adding water to the powdered jade purified in step S10, followed by stirring (S20); sonicating the liquid stirred in the step S20 (S30); and filtering out the water insoluble jade powder in the liquid sonicated in the step S30 (S40).

Description

Water-Soluble Jade Extract and Preparation Method Thereof}

It is an object of the present invention to provide a cosmetic composition comprising a water-soluble jade extract production method and a water-soluble jade extract prepared by the method as an active ingredient.

Far infrared rays, a kind of electromagnetic waves, have a wavelength of 8 ~ 16㎛, which is the most beneficial to the human body. When absorbed by the human body, it penetrates 80 times deeper (4 ~ 5cm) deeper than normal heat and helps to kill various pathogens. Can give In addition, the far infrared rays are radiated to the water and protein molecules constituting the cells in the human body and resonates with a minute vibration about 2,000 times per minute to activate the activity of the cells. In the process of cell activity, heat energy is generated, which increases body temperature.As the body temperature increases, microvascularization expands, blood circulation is activated, and metabolism is strengthened.Tissue regeneration increases, which breaks down blood clots in blood vessels and promotes blood circulation. do. As the blood clears, the hydrogen ion concentration (pH) is improved, which strengthens the ability to improve the constitution from acidic to weak alkaline, and is also effective in relieving stress, which is the cause of adult diseases, by relaxing the action to help mental health.

The effect of far-infrared rays on the human body is to increase the temperature of the subcutaneous layer, the expansion of microvessels, the promotion of blood circulation, the strengthening of metabolism between the blood and the human body and other tissues, the elimination of blood disorders, the increase of tissue regeneration and anticonvulsion capacity. At the same time, it was also found that the sensory nerve suppression of abnormal excitement and autonomic nervous system function were also effective. Far infrared ray is a single wavelength of heat. Far infrared rays are radiated to the surface of human skin, which is almost the same as the vibration wavelength of water in the human body. Thus, resonance or vibration causes normal heat to reach. There is a characteristic that reaches to an uncountable part.

Jade has a property of emitting a large amount of 5-20 μm far-infrared rays, which are growth rays in the ore itself. Far-infrared rays emitted from jade strongly act on the polymerized ring of unsaturated fatty acid, lipid peroxide, contaminated water, etc. in the body. Far-infrared rays emitted from jade separate the double and triple bonds of these pollutants, thereby enhancing and promoting the physiological activity of the human body.

Examples of jade used in the past include agate, glass, amber, quarry, jade, jade, and jade. Jade is divided into jadeite and purgatory. A jadeite is a lead petroleum mineral belonging to the pyroxene family, which is a monoclinic system composed of silicic acid, aluminum oxide, and soda, and its hardness is dense mass like crystal Light is black, cyan, green, transparent or translucent. Nephrite Jade is a monoclinic whissomite mineral of Inosilicates, which is divided into serpentine superbasic purgatory among high-grade surrogate rocks. Purgatory quality is determined by its fine structure, that is, the degree of fineness of hollowstone-sheepstone sperm into fastenings and fibers, and the thinner the fiber, the better the quality.

Although jade is known to have such excellent medical effects due to its scarcity, most of the jade is limited to some jewelry for jewelry, such as necklaces, rings, and bracelets. In addition, since jade is expensive, development of general household goods using jade is relatively weak.

In order to use such jade is processed in a powder state, but to apply to cosmetics, there is a problem that jade powder is difficult to disperse in cosmetics. It is also necessary to increase the far-infrared and anion radiation effects of jade. In addition, asbestos and the like may be detected in the jade powder, and it is necessary to prevent this.

Republic of Korea Patent No. 10-1869971 Republic of Korea Patent No. 10-1593108 Republic of Korea Patent Publication No. 10-2006-0011489

The present invention provides a water-soluble jade extract and a method for producing the same to improve the dispersion efficiency in cosmetics while maximizing the efficacy of jade by maximizing the far-infrared rays and anions emitted from the jade to solve the above problems. It aims to do it.

According to one embodiment of the invention,

Purifying the powder jade (S10);

Adding water to the powder jade purified in step S10 and stirring (S20);

Ultrasonicating the liquid stirred in step S20 (S30); And

It provides a method for producing a solubilized jade extract, characterized in that it comprises the step (S40) of filtering the unacceptable jade powder in the liquid sonicated in the step S30.

In step S40, it is characterized in that it further comprises the step (S50) of filtering the liquid filtered jade powder using a 0.2㎛ size filter.

The step S10,

Adding water to the powder jade and depositing it for 10 minutes at 100 to 300 RPM (S10-1);

After stirring in the step S10-1 and left for 30 minutes (S10-2);

Removing foreign substances floating on the surface of water and separating the powder jade deposited below (S10-3); And

It characterized in that it comprises a step (S10-4) for drying the deposited jade powder separated in the step S10-3 hot air 60 ℃.

In the step S20, the temperature is 100 ℃ to 121 ℃, characterized in that for 1 hour stirring at 15lb psi pressure.

In the step S30, characterized in that the treatment with 40KHz ultrasonic wave for 1 hour.

According to another embodiment of the present invention provides a cosmetic composition comprising the water-soluble jade extract extracted by the manufacturing method as an active ingredient.

According to another embodiment of the present invention, the soft cosmetics, nourishing cosmetics, moisture cream, nutrition cream, massage cream, essence, ampoule, gel, eye cream, cleansing cream, cleansing foam, cleansing water, pack, spray and powder It can provide a cosmetic composition formulated in one or more selected from.

According to an embodiment of the present invention, while maximizing the far-infrared rays and anions emitted from the jade to increase the efficacy of the jade, it is possible to provide a water-soluble jade extract manufacturing method and a cosmetic composition that can improve the dispersion efficiency in the cosmetic. .

1 is a flowchart illustrating a method of preparing a jadeite extract according to an embodiment of the present invention.
Figure 2 is a view showing the asbestos detection test results of the mask pack containing a water jade extract prepared according to an embodiment of the present invention.
Figure 3 is a view showing the far-infrared test report of the mask pack containing a water jade extract prepared according to an embodiment of the present invention.
Figure 4 is a view showing an anion test report of the mask pack containing a water jade extract prepared according to an embodiment of the present invention.

Soluble jade extract manufacturing method according to an embodiment of the present invention includes a powder ore purification step, the solubility (solable) and activation step of the powder jade, and jade aqueous solution separation step.

1. Purification step of powder jade ore

Powdered jade is powdered by grinding ore jade or powdered ore powder is used. The method of powdering may proceed with a mineral crusher (Crusher, 3-Yana mill, etc.) or a pestle, and in this case, powder jade particles are preferably pulverized to 80 mesh or less using a mesh mesh (80 mesh).

1 kg of heterogeneous ore in the form of powder is deposited with water, and then stirred at 100 to 300 rpm for 10 minutes, and left for 30 minutes.

Remove foreign substances on the surface of the water first, and separate only the powder jade deposited below.

The powdered jade deposited is dried at a temperature of 60 ° C. or higher by hot air drying or the like to obtain 960 g of powdered jade.

2. Solubilization and Activation Step of Powder Jade

500 mL of water per 300 g of jade powder was added to the stainless steel bomber, followed by stirring for 1 hour at 121 ° C. and a pressure of 15 lb psi.

After jade powder and supernatant together with 40KHz for 1 hour.

3. Separation Step of Jade Aqueous Solution

The sonicated jade powder and the supernatant were first filtered out of the non-soluble jade powder using a nonwoven fabric, and then 477 mL of the jade extracts that were received using a 0.2 um filter were obtained.

* Performance test result

Figure 2 shows the asbestos test results for the mask pack containing a soluble jade extract prepared by the above production method. Asbestos was not detected when examined by an asbestos test method (KS L 5300: 2009) as shown in FIG. 2. That is, it can be confirmed that asbestos, which has a detection risk in general jade powder, is not detected in the jade extract that is received. Therefore, it can apply to cosmetics etc. safely.

In order to show the performance of the soluble jade extract according to the present invention, the performance difference with the control prepared by the general manufacturing method was compared. The control was prepared by the following method.

Control group 1 Control 2 Control group 3 designation Jade powder deposit group Ultrasonic Untreated Group Heat-treated group Manufacturing method Put 500mL of water in 300g of jade powder, and immerse at room temperature for 1 hour 500 ml of water was added to 300 g of jade powder, and the mixture was stirred at 60 ° C. for 1 hour and then filtered. 300ml of jade powder, 500mL of water, filtered by 40KHz ultrasonic wave for 1 hour

(1) pH comparison

The pH was tested according to the Standards and Test Methods of the Ministry of Food and Drug Safety and Functional Test Standard VI-2, pH of the formulation, and the following results were obtained, and the pH was different from the test group (this patent method) and the control group. There was little.

Example Control group 1 Control 2 Control group 3 pH 6.8 7.2 6.8 6.8

(2) Comparison of negative ion generation amount

Figure 4 shows the test report measuring the anion generation results of the mask pack containing the jade extract prepared according to an embodiment of the present invention. As shown, when the anion emitted from the measurement object was measured by the number of ions per unit volume using the charged particle measuring device according to the standard test method KFIA-FI-1042 it can be confirmed that the amount of negative ions generated in the embodiment of the present invention is higher than the control group there was.

Example Control group 1 Control 2 Control group 3 Negative ion
(ion / cc) 120 107 114 116

(3) Far infrared rays generation quantity comparison

Figure 3 shows the test report measuring the far-infrared generation results of the mask pack containing the jade extract prepared according to the embodiment of the present invention. As shown, the far-infrared ray was measured using the FT-IR according to the standard test method KFIA-FI-1005, it was confirmed that the anion generation amount of the embodiment of the present invention is high.

Example Control group 1 Control 2 Control group 3 Radiation energy (w / ㎡ · ㎛, 37 ℃) 3.45 × 10 ² 3 × 10 ² 1.15 × 10 ² 1.05 × 10 ²

The present invention relates to a method for producing abundant jade solubilization to contain anion and far-infrared rays to aid the beauty of the skin in cosmetic products, the step of invasive purification of powdered ore jade, and heat to the purified jade powder It is characterized in that it comprises a solubilization and purification step of separating the unsolubilized jade powder by the step of giving energy, such as ultrasonic waves to improve the far infrared emission.

The present invention can be used without sediment by accepting the jade extract, the extract having an anion or far-infrared emission characteristics of jade, may be applicable to various cosmetic formulations in the pH range of 6-8

Claims (7)

Purifying the powder jade (S10);
Adding water to the powder jade purified in step S10 and stirring (S20);
Ultrasonicating the liquid stirred in step S20 (S30);
Filtering the unacceptable jade powder from the liquid sonicated in the step S30 (S40); And
And filtering the liquid filtered out of jade powder using a filter having a size of 0.2 μm in step S40 to obtain an acceptable jade extract (S50),
In the step S20, the temperature is stirred for 1 hour at 100 ℃ to 121 ℃ temperature, 15lb psi pressure,
In the step S30, solubilized jade extract manufacturing method characterized in that the treatment for 1 hour 40KHz ultrasound. delete The method of claim 1,
The step S10,
Adding water to the powder jade and depositing it for 10 minutes at 100 to 300 RPM (S10-1);
After stirring in the step S10-1 and left for 30 minutes (S10-2);
Removing foreign substances floating on the surface of water and separating the powder jade deposited below (S10-3); And
Soluble jade extract manufacturing method comprising the step of drying the deposited powder jade separated in step S10-3 hot air 60 ℃ (S10-4). delete delete Cosmetic composition comprising a water-soluble jade extract extracted by the method of claim 1 as an active ingredient. The method of claim 6,
Cosmetics formulated with one or more selected from the group consisting of softening cream, nourishing cream, moisture cream, nourishing cream, massage cream, essence, ampoule, gel, eye cream, cleansing cream, cleansing foam, cleansing water, pack, spray and powder Composition.

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