KR102260288B1 - Water-Soluble Jade Extract and Preparation Method Thereof - Google Patents

Abstract

The present invention is a step of purifying powder jade (S10), adding water to the powder jade purified in the step S10 and stirring (S20), sonicating the liquid stirred in the step S20 (S30), the S30 Nano-dispersion water-soluble jade extract comprising the step (S40) of filtering the jade powder that is not solubilized from the liquid sonicated in the step (S40) and the step (S50) of pulverizing the solution in which the jade powder is filtered in the step S40 in a nano grinder (S50) A manufacturing method is provided.

Description

Nano-dispersion water-soluble jade extract manufacturing method and cosmetic composition {Water-Soluble Jade Extract and Preparation Method Thereof}

An object of the present invention is to provide a method for producing a nano-dispersed water-soluble jade extract and a cosmetic composition comprising the water-soluble jade extract prepared by the method as an active ingredient.

Far-infrared rays, a kind of electromagnetic wave, have the most beneficial wavelength for the human body, 8~16㎛, and when absorbed into the human body, it penetrates to the deep skin (4~5cm) 80 times deeper than general heat, helping to kill various pathogens. can give In addition, far-infrared rays are radiated to the water and protein molecules constituting cells in the human body, and resonate with minute vibrations about 2,000 times per minute to activate cell activity. In the process of cell activity, it generates heat energy and raises body temperature. When body temperature rises, microvessels expand and blood circulation is activated to strengthen metabolism, and tissue regeneration increases, decomposing blood clots in blood vessels and promoting blood circulation. do. As the blood becomes clear, the hydrogen ion concentration (pH) is improved to strengthen the ability to improve the constitution from acid to slightly alkaline, and it is also effective in relieving stress, which is the cause of adult diseases, as it has a relaxing action that is helpful for mental health.

The effects of far-infrared rays on the human body are: temperature rise of the subcutaneous layer, expansion of microvessels, promotion of blood circulation, enhancement of metabolism between blood and human body and other tissues, elimination of blood disorders, and increase in tissue regeneration or anticonvulsant ability It was also found to have the effect of suppressing abnormal excitability of the sensory nerve and adjusting the function of the autonomic nerve at the same time. Far infrared ray is one wavelength of heat, and far infrared ray radiated on the surface of human skin is almost similar to the vibrational wavelength of water in the human body, so that general heat can reach through resonance or resonance. It has the characteristic of reaching areas that cannot be reached.

Jade has a property of emitting a large amount of far infrared rays of 5-20㎛, which is a growth ray, from the ore itself. Far-infrared rays emitted from such jade strongly act on the polymerization rings of unsaturated fatty acids, lipid peroxides, and polluted water in the body. Since the double and triple bonds of these pollutants are separated by the far-infrared rays emitted from the jade, the physiological activity of the human body is increased and promoted.

The types of jade used since ancient times include agate, glass, amber, seokunghwang, jade, cheonhaseok jade, and topaz. Jade is divided into jadeite (硬玉) and nephrite (軟玉). Jadeite is a lead pyroxene mineral belonging to the pyroxene family. It is a monoclinic material composed of silicic acid, aluminum oxide and soda, and its hardness is a dense mass like crystal. and light is black, cyan, and green, and has a transparent or translucent property. Nephrite Jade is a monoclinic pyroxene mineral of inosilicates, and is divided into serpentine and ultrabasic nephrite among high-earth marbles. The quality of nephrite is determined by its fine structure, that is, the degree of fineness of openwork amphibole-yanggi-seok spermatozoon and fiber. It is known that the finer the fiber, the better the quality.

Although jade is known to have excellent medical efficacy as described above due to its rarity, it is mostly used limitedly only as jewelry for personal decoration, such as necklaces, rings, and bracelets. In addition, since jade is an expensive product, the development of jade as a general household item is relatively weak.

For the use of such jade, it is processed and used in a powder state, but there is a problem in that the jade powder is difficult to disperse in cosmetics for application to cosmetics. In addition, it is necessary to increase the far-infrared and anion radiation effects of jade. In addition, it is necessary to prevent asbestos and the like may be detected in the jade powder.

Republic of Korea Patent No. 10-1869971 Republic of Korea Patent No. 10-1593108 Korean Patent Publication No. 10-2006-0011489

In order to solve the above problems, the present invention is a nano-dispersed water-soluble jade extract capable of maximizing the far-infrared rays or anions emitted from jade, thereby doubling the efficacy of jade, and improving the dispersion efficiency in cosmetics, and a method for manufacturing the same aims to provide

According to one embodiment of the present invention,

Purifying powder jade (S10);

Adding water to the purified jade powder in step S10 and stirring (S20);

ultrasonically treating the liquid stirred in step S20 (S30); And

It provides a nano-dispersed water-soluble jade extract manufacturing method comprising the step (S40) of filtering the jade powder that is not solubilized in the liquid sonicated in the step S30.

It characterized in that it further comprises a step (S50) of pulverizing the liquid from which the jade powder is filtered in the step S40 using a nano grinder.

The step S10 is,

After adding water to the powder jade and immersing it, stirring at 100 to 300 RPM for 10 minutes (S10-1);

After stirring in step S10-1, leaving for 30 minutes (S10-2);

Removing foreign substances floating on the water surface and separating the powder jade deposited below (S10-3); And

It characterized in that it comprises a step (S10-4) of hot air drying the deposited powder jade separated in the step S10-3 60 ℃.

In the step S20, 100 ℃ to 121 ℃ temperature, characterized in that the stirring for 1 hour at 15lb psi pressure.

In the step S30, it is characterized in that it is treated with 40KHz ultrasonic waves for 1 hour.

According to another embodiment of the present invention, there is provided a cosmetic composition comprising the water-soluble jade extract extracted by the above manufacturing method as an active ingredient.

According to another embodiment of the present invention, the group consisting of softening lotion, nutrient lotion, moisture cream, nutrient cream, massage cream, essence, ampoule, gel, eye cream, cleansing cream, cleansing foam, cleansing water, pack, spray and powder It is possible to provide a cosmetic composition formulated with one or more selected from.

According to an embodiment of the present invention, it is possible to provide a method for producing a nano-dispersed water-soluble jade extract and a cosmetic composition that can maximize the effect of the jade by maximizing the far-infrared rays or anions emitted from the jade, and improve the dispersion efficiency in the cosmetic. can

1 is a flowchart showing a method for preparing a water-soluble jade extract according to an embodiment of the present invention.
2 is a view showing the results of the asbestos detection test of the mask pack containing the water-soluble jade extract prepared according to an embodiment of the present invention.
3 is a view showing a far-infrared test report of a mask pack containing a water-soluble jade extract prepared according to an embodiment of the present invention.
4 is a view showing an anion test report of a mask pack containing a water-soluble jade extract prepared according to an embodiment of the present invention.

The nano-dispersion water-soluble jade extract manufacturing method according to an embodiment of the present invention includes a powder jade ore purification step, a solubilization and activation step of powder jade, and a jade aqueous solution separation step.

1. Refining step of powder jade ore

Powder jade is pulverized by crushing ore jade or use jade ore powder in a powder state. The method of pulverization can be carried out with a mineral crusher (Crusher, 3-Yana mill, etc.) or a pestle, etc. In this case, it is preferable to use a powder jade particle pulverized to 80 mesh or less using a mesh network (80 mesh).

1 kg of ore jade in a heterogeneous powder state was deposited by adding water, stirred at 100 to 300 rpm for 10 minutes, and left for 30 minutes.

Remove foreign substances floating on the surface of the water first and separate only the powder jade deposited below.

The deposited powder jade is dried by a method such as hot air drying at 60 ° C. or higher to obtain 960 g of powder jade.

2. Solubilization and activation step of powder jade

After adding 500mL of water per 300g of jade powder, and putting it in a Stainless Steel Bomber, it is stirred for 1 hour at 121℃ and 15lb psi pressure.

Afterwards, the jade powder and the supernatant are sonicated at 40 KHz for 1 hour.

3. Separation of jade aqueous solution

Ultrasonic-treated jade powder and supernatant were first filtered out of unsoluble jade powder using a non-woven fabric network, and then 477 mL of solubilized jade extract was obtained using a 0.2um filter.

4. Grinding the jade aqueous solution to nano size

The jade aqueous solution from which the jade powder has been filtered is put into a nano grinder and pulverized to a nano size to obtain a jade nano dispersion aqueous solution. It is preferable to use a wet nanoparticle grinder for the nano pulverizer. By pulverizing the solubilized jade particles to a nano size, they can be effectively dispersed and absorbed into the skin. As the nano pulverizer, RETSCH's High Energy Ball Mill Emax, Kotobuki wet nano particle pulverizer, THINKY's arm-310, etc. may be used.

* Performance test result

Figure 2 shows the asbestos test results for the mask pack containing the solubilized jade extract prepared by the manufacturing method. As shown in FIG. 2, asbestos was not detected when tested by the asbestos test method (KS L 5300:2009). That is, it can be confirmed that asbestos, which is a risk of detection in general jade powder, is not detected in the jade extract in which it is soluble. Therefore, it can be safely applied to cosmetics and the like.

In order to show the performance of the solubilized jade extract according to the present invention, the difference in performance with the control prepared by the general manufacturing method was compared. The control group was prepared in the following way.

Control 1 Control 2 Control 3 designation jade powder deposits Ultrasonic untreated group heat untreated group Manufacturing method Add 500 mL of water to 300 g of jade powder, immerse at room temperature for 1 hour, and filter Add 500mL of water to 300g of jade powder, stir at 60℃ for 1 hour, and filter Add 500mL of water to 300g of jade powder, and treat with 40KHz ultrasonic wave for 1 hour.

(1) pH comparison

The following results were obtained by testing the pH according to the Ministry of Food and Drug Safety's functional product standard and test method General Test Method VI-2, the pH of the formulation. Regarding pH, there was no difference between the test group (this patent method) and the control group. There were hardly any.

Example control group 1 control group 2 control group 3 pH 6.8 7.2 6.8 6.8

(2) Comparison of anion generation amount

Figure 4 shows a test report measuring the anion generation result of the mask pack containing the jade extract prepared according to an embodiment of the present invention. As shown, when the number of ions emitted from the measurement object was measured using a charged particle measuring device according to the standard test method KFIA-FI-1042, it can be confirmed that the amount of anion generated in the example of the present invention is higher than that of the control. there was.

Example control group 1 control group 2 control group 3 negative ions
(ion/cc) 120 107 114 116

(3) Comparison of far-infrared radiation

Figure 3 shows the test report measuring the far-infrared generation result of the mask pack containing the jade extract prepared according to the embodiment of the present invention. As shown, as a result of measuring far-infrared rays using FT-IR according to the standard test method KFIA-FI-1005, it was confirmed that the amount of anion generated in Examples of the present invention was high.

Example control group 1 control group 2 control group 3 Radiant energy (w/m2·㎛, 37℃) 3.45×10 ² 3×10 ² 1.15×10 ² 1.05×10 ²

The present invention relates to a method for producing water-rich jade so that it can contain negative ions and far-infrared rays useful for skin beauty in cosmetic products, the step of invasively refining the powdered ore jade, and heat to the purified jade powder , characterized in that it comprises a step of improving the far-infrared emission by giving energy such as ultrasonic waves, and a water-soluble purification step of separating jade powder that is not solubilized.

The present invention can be used without a precipitate by water-solubilizing the jade extract, as an extract having an anion or far-infrared emission characteristic of jade, and can be applied to various cosmetic formulations with a pH of 6-8.

Claims (6)

Purifying powder jade (S10);
Adding water to the purified jade powder in step S10 and stirring (S20);
ultrasonically treating the liquid stirred in step S20 (S30);
Filtering the jade powder not soluble in the liquid sonicated in step S30 (S40); and
In the step S40, the jade aqueous solution from which the jade powder has been filtered is put into a nano grinder and grinded to a nano size (S50);
In the step S20, 100 ℃ to 121 ℃ temperature, 15lb psi pressure, while stirring for 1 hour, nano-dispersion water-soluble jade extract preparation method, characterized in that the treatment with 40KHz ultrasonic wave. The method of claim 1,
The step S10 is,
After adding water to the powder jade and immersing it, stirring at 100 to 300 RPM for 10 minutes (S10-1);
After stirring in step S10-1, leaving for 30 minutes (S10-2);
Removing foreign substances floating on the water surface and separating the powder jade deposited below (S10-3); and
Method for producing a nano-dispersed water-soluble jade extract comprising the step (S10-4) of hot air drying the deposited powder jade separated in the step S10-3. delete delete A cosmetic composition comprising the water-soluble jade extract extracted by the manufacturing method of claim 1 as an active ingredient. The method of claim 5,
Cosmetics formulated with one or more selected from the group consisting of softening lotion, nourishing lotion, moisture cream, nourishing cream, massage cream, essence, ampoule, gel, eye cream, cleansing cream, cleansing foam, cleansing water, pack, spray and powder composition.

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