KR20200113478A - Water-Soluble Jade Extract and Preparation Method Thereof - Google Patents

Abstract

The present invention provides a manufacturing method of a nano-dispersed water-soluble jade extract, comprising the steps of: (S10) purifying a jade powder; (S20) stirring after adding water to the jade powder purified in the step S10; (S30) ultrasonicating the liquid stirred in the step S20; (S40) filtering the jade powder that is not soluble in the liquid ultrasonicated in the step S30; and (S50) pulverizing the solution from which the jade powder has been filtered in the step S40 in a nano grinder.

Description

Nano-dispersed soluble jade extract manufacturing method and cosmetic composition {Water-Soluble Jade Extract and Preparation Method Thereof}

An object of the present invention is to provide a method for preparing a nano-dispersed soluble jade extract and a cosmetic composition comprising a soluble jade extract prepared by the method as an active ingredient.

Far-infrared rays, a kind of electromagnetic wave, have a wavelength of 8~16㎛, which is the most beneficial to the human body, and when absorbed into the human body, it penetrates into the deep skin layer (4~5cm) 80 times deeper than normal heat, helping to kill various pathogens. Can give. In addition, far-infrared rays are radiated to water and protein molecules that make up the cells of the human body, and resonate with minute vibrations about 2,000 times per minute to energize the cells. In the process of cell activity, it generates heat energy and increases body temperature.When body temperature rises, microvessels expand and blood circulation is activated, enhancing metabolism, increasing tissue regeneration, decomposing blood clots in blood vessels, and promoting blood circulation. do. Since the blood becomes clear, it strengthens the ability to improve the constitution from acid to weak alkali by improving the hydrogen ion concentration (pH). Also, it is effective in relieving stress, which is the cause of adult diseases, with a relaxation action that is beneficial to mental health.

The effects of far-infrared rays on the human body include an increase in the temperature of the subcutaneous layer, expansion of microvessels, promotion of blood circulation, enhancement of metabolism between blood and human body and other tissues, elimination of blood disorders, increase in tissue regeneration ability or anticonvulsant ability. It was found to have the effect of suppressing abnormal excitability of the perceptual nerve and adjusting the function of the autonomic nerve at the same time. Far infrared ray is a single thermal wavelength, and the far infrared ray radiated to the surface of human skin is almost similar to the vibration wavelength of water in the human body, so that general heat can reach it through resonance or vibration. It has the characteristic of reaching areas that cannot be reached.

Jade has the property of emitting a large amount of far-infrared rays of 5-20㎛, which is a growing ray from the ore itself. The far-infrared rays emitted from these jades act strongly on the polymerized rings of unsaturated fatty acids, peroxide lipids, and contaminated water in the body. Since the double and triple bonds of these contaminants are separated by far-infrared rays emitted from the jade, the physiological activity of the human body is increased and promoted.

The types of jade used since ancient times include agate, glass, amber, seokwoonghwang, jade, cheonhaseokok, and topaz. Jade is divided into jadeite (硬玉) and purgatory (軟玉). Jadeite is a lead pyroxene mineral belonging to the pyroxene family, and is a monoclinic material composed of silicic acid, aluminum oxide and soda, and its hardness is a dense mass like crystal. And the light is black, cyan, green, and has a transparent or translucent property. Nephrite Jade is a monoclinic fissile mineral of Inosilicates, and is divided into serpentine superbasic purgatory among the paleo-soil marbles. The quality of purgatory is determined by its fine structure, that is, the fine structure of openwork-yanggiseok spermatozoa, and the finer the fiber is, the finer the fiber is, the better the quality is known.

Although jade is known to have excellent medical effects as described above due to its scarcity, it is mostly used only as a jewelry accessory for personal decoration such as necklaces, rings, and bracelets. Also, since jade is a high-priced product, the development of jade as a general household product is relatively weak.

In order to use such jade, it is processed and used in a powder state, but there is a problem in that jade powder is difficult to disperse in cosmetics for application to cosmetics. In addition, there is a need to increase the far-infrared and negative ion radiation effects of jade. In addition, since asbestos may be detected in jade powder, it is necessary to prevent this.

Korean Registered Patent No. 10-1869971 Korean Patent Registration No. 10-1593108 Korean Patent Publication No. 10-2006-0011489

In order to solve the above problems, the present invention maximizes the far-infrared rays or anions emitted from the jade to increase the efficacy of jade, while improving the dispersion efficiency in cosmetics, and a nano-dispersed soluble jade extract and a method for producing the same It aims to provide.

According to an embodiment of the present invention,

Purifying powdered jade (S10);

Adding water to and stirring the powder jade purified in step S10 (S20);

Ultrasonicating the liquid stirred in the step S20 (S30); And

It provides a method for producing a nano-dispersed water-soluble jade extract, characterized in that it comprises a step (S40) of filtering the jade powder not soluble in the sonicated liquid in the step S30.

It characterized in that it further comprises a step (S50) of pulverizing the liquid from which the jade powder has been filtered using a nano-pulverizer in step S40.

The step S10,

Adding water to the powdered jade and immersing it, and then stirring at 100 to 300 RPM for 10 minutes (S10-1);

Stirring in the step S10-1 and leaving it for 30 minutes (S10-2);

Removing foreign substances floating on the water surface and separating the powdered jade deposited below (S10-3); And

It characterized in that it comprises a step (S10-4) of drying the deposited powdered jade separated in step S10-3 with hot air at 60°C.

In the step S20, characterized in that stirring for 1 hour at a temperature of 100 ℃ to 121 ℃, 15lb psi pressure.

In step S30, it is characterized in that the treatment is performed with 40KHz ultrasonic waves for 1 hour.

According to another embodiment of the present invention, there is provided a cosmetic composition comprising the water-soluble jade extract extracted by the above manufacturing method as an active ingredient.

According to another embodiment of the present invention, the group consisting of softening lotion, nutritional lotion, moisture cream, nutrition cream, massage cream, essence, ampoule, gel, eye cream, cleansing cream, cleansing foam, cleansing water, pack, spray and powder A cosmetic composition formulated with one or more selected from can be provided.

According to an embodiment of the present invention, it is possible to provide a nano-dispersed water-soluble jade extract manufacturing method and a cosmetic composition capable of improving the dispersion efficiency in cosmetics while maximizing far-infrared rays or anions emitted from jade to increase the efficacy of jade. I can.

1 is a flow chart showing a method for preparing a soluble hwaok extract according to an embodiment of the present invention.
Figure 2 is a view showing the results of the asbestos detection test of the mask pack containing the extract prepared according to an embodiment of the present invention.
Figure 3 is a view showing a far-infrared test report of the mask pack containing the extract prepared in accordance with an embodiment of the present invention.
4 is a view showing an anion test report of a mask pack containing an extract prepared according to an embodiment of the present invention.

A method for preparing a nano-dispersed water-soluble jade extract according to an embodiment of the present invention includes a step of purifying powdered jade ore, a step of solable and activating powdered jade, and a step of separating an aqueous jade solution.

1. Purification step of powdered jade ore

Powdered jade is pulverized by pulverizing ore jade, or powdered jade ore powder is used. The method of pulverization can be carried out with a mineral crusher (Crusher, 3-Yana mill, etc.) or a mortar, and it is preferable to use the powder jade particles crushed to less than 80 mesh using a mesh net (80 mesh).

1 kg of heterogeneous powdered ore jade was immersed by adding water, stirred at 100 to 300 rpm for 10 minutes, and left for 30 minutes.

Foreign matter floating on the water surface is first removed, and only the powder jade deposited below is separated.

The deposited powdered jade is dried by a method such as hot air drying at 60℃ or higher to obtain 960g of powdered jade.

2. Water solubility and activation step of powdered jade

500mL of water per 300g of jade powder was added, put into a stainless steel bomber, and stirred for 1 hour at 121℃ and 15lb psi pressure.

After that, the jade powder and the supernatant are ultrasonically treated for 1 hour at 40 KHz.

3. Separation step of jade aqueous solution

First, the sonicated jade powder and the supernatant were first filtered through a non-woven fabric to filter out unsoluble jade powder, and then 477 mL of the soluble jade extract was obtained using a 0.2 um filter.

4. The step of pulverizing the jade aqueous solution into nano size

The jade aqueous solution from which jade powder has been filtered is added to a nano pulverizer and pulverized to a nano size to obtain a jade nano-dispersed aqueous solution. It is preferable to use a wet nanoparticle pulverizer for the nano pulverizer. The soluble jade particles can be pulverized into nano-sized so that they can be effectively dispersed and absorbed into the skin. The nano pulverizer can be used with RETSCH's High Energy Ball Mill Emax, Kotobuki's wet nanoparticle pulverizer, and THINKY's arm-310.

* Performance test result

2 shows the results of the asbestos test for the mask pack containing the soluble jade extract prepared by the above manufacturing method. Asbestos was not detected when tested by the asbestos test method (KS L 5300:2009) as shown in FIG. 2. That is, it can be confirmed that asbestos, which is at risk of detection in general jade powder, is not detected in the soluble jade extract. Therefore, it can be safely applied to cosmetics and the like.

In order to show the performance of the soluble jade extract according to the present invention, the difference in performance with the control prepared by the general manufacturing method was compared and tested. The control was prepared by the following method.

Control 1 Control 2 Control 3 designation Jade powder invasion group Ultrasound untreated group Heat untreated group Manufacturing method Add 500mL of water to 300g of jade powder, soak for 1 hour at room temperature, and then filter Add 500mL of water to 300g of jade powder, stir at 60℃ for 1 hour, and then filter A liquid filtered by adding 500mL of water to 300g of jade powder and treating it with 40KHz ultrasonic waves for 1 hour

(1) pH comparison

The pH was tested in accordance with the Ministry of Food and Drug Safety's Functional Product Standards and Test Method General Test Method VI-2, the pH of the formulation, and the following results were obtained, and the difference between the test group (this patent method) and the control group was There was little.

Example Control 1 Control 2 Control 3 pH 6.8 7.2 6.8 6.8

(2) Comparison of anion generation amount

Figure 4 shows a test report measuring the negative ions generation results of the mask pack containing the jade extract prepared according to an embodiment of the present invention. As shown, it can be confirmed that the amount of anion generated in the examples of the present invention is higher than that of the control when the anions emitted from the measurement object are measured as the number of ions per unit volume using a charged particle measuring device according to the reference test method KFIA-FI-1042. there was.

Example Control 1 Control 2 Control 3 Negative ions
(ion/cc) 120 107 114 116

(3) Comparison of far-infrared rays generation

Figure 3 shows a test report measuring the far-infrared generation results of the mask pack containing the jade extract prepared according to an embodiment of the present invention. As shown, as a result of measuring the far-infrared rays using FT-IR according to the reference test method KFIA-FI-1005, it was confirmed that the amount of negative ions generated in the examples of the present invention was high.

Example Control 1 Control 2 Control 3 Radiation energy (w/㎡·㎛, 37℃) 3.45×10 ² 3×10 ² 1.15×10 ² 1.05×10 ²

The present invention relates to a manufacturing method of water-soluble jade so that a cosmetic product can contain negative ions and far-infrared rays that are useful for the beauty of the skin, the step of invasively purifying powdered ore jade, and heat to the purified jade powder. It characterized in that it comprises a step of improving the far-infrared emission by applying energy such as ultrasonic waves, and a water-soluble purification step of separating the unwatered jade powder.

The present invention can be used without sediment by water-soluble jade extract, as an extract having anion or far-infrared emission characteristics of jade, and may be applicable to various cosmetic formulations with a pH ranging from 6 to 8

Claims (6)

Purifying powdered jade (S10);
Adding water to and stirring the powder jade purified in step S10 (S20);
Ultrasonicating the liquid stirred in the step S20 (S30);
Filtering the jade powder that is not soluble in the sonicated liquid in step S30 (S40); And
In the step S40, the step of pulverizing the jade aqueous solution from which the jade powder has been filtered into a nano-sized nano-sized (S50); Method for producing a nano-dispersed water-soluble jade extract comprising a. The method of claim 1,
The step S10,
Adding water to the powdered jade and immersing it, and then stirring at 100 to 300 RPM for 10 minutes (S10-1);
Stirring in the step S10-1 and leaving it for 30 minutes (S10-2);
Removing foreign substances floating on the water surface and separating the powdered jade deposited below (S10-3); And
A method for preparing a nano-dispersed soluble jade extract comprising the step of drying the deposited powdered jade separated in step S10-3 with hot air at 60°C (S10-4). The method of claim 1,
In the step S20, a method for preparing a nano-dispersed water-soluble jade extract, characterized in that stirring for 1 hour at a temperature of 100° C. to 121° C. and a pressure of 15 lb psi. The method of claim 1,
In the step S30, the method for producing a nano-dispersed soluble jade extract, characterized in that the treatment with 40KHz ultrasonic waves for 1 hour. A cosmetic composition comprising the water-soluble jade extract extracted by the method of claim 1 as an active ingredient. The method of claim 5,
Cosmetics formulated with one or more selected from the group consisting of softening lotion, nutrient lotion, moisture cream, nutrition cream, massage cream, essence, ampoule, gel, eye cream, cleansing cream, cleansing foam, cleansing water, pack, spray and powder Composition.

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