KR101903362B1 - 전이 금속 수산화물의 제조 방법 - Google Patents

전이 금속 수산화물의 제조 방법 Download PDF

Info

Publication number
KR101903362B1
KR101903362B1 KR1020137021135A KR20137021135A KR101903362B1 KR 101903362 B1 KR101903362 B1 KR 101903362B1 KR 1020137021135 A KR1020137021135 A KR 1020137021135A KR 20137021135 A KR20137021135 A KR 20137021135A KR 101903362 B1 KR101903362 B1 KR 101903362B1
Authority
KR
South Korea
Prior art keywords
transition metal
present
range
suspension
metal hydroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020137021135A
Other languages
English (en)
Korean (ko)
Other versions
KR20140047577A (ko
Inventor
우베 클리펠스
지몬 슈뢰들레
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20140047577A publication Critical patent/KR20140047577A/ko
Application granted granted Critical
Publication of KR101903362B1 publication Critical patent/KR101903362B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/80—Compounds containing cobalt, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G51/82—Compounds containing cobalt, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
KR1020137021135A 2011-01-10 2012-01-09 전이 금속 수산화물의 제조 방법 Active KR101903362B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11150470.0 2011-01-10
EP11150470 2011-01-10
PCT/EP2012/050219 WO2012095381A2 (de) 2011-01-10 2012-01-09 Verfahren zur herstellung von übergangsmetallhydroxiden

Publications (2)

Publication Number Publication Date
KR20140047577A KR20140047577A (ko) 2014-04-22
KR101903362B1 true KR101903362B1 (ko) 2018-10-02

Family

ID=45446064

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020137021135A Active KR101903362B1 (ko) 2011-01-10 2012-01-09 전이 금속 수산화물의 제조 방법

Country Status (6)

Country Link
EP (1) EP2663527B1 (enExample)
JP (1) JP5872587B2 (enExample)
KR (1) KR101903362B1 (enExample)
CN (1) CN103282310B (enExample)
TW (1) TW201236978A (enExample)
WO (1) WO2012095381A2 (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HUE060257T2 (hu) * 2008-04-03 2023-02-28 Lg Energy Solution Ltd Új prekurzor lítium kompozit átmenetifém-oxid elõállítására
KR101575024B1 (ko) 2013-02-13 2015-12-07 주식회사 엘지화학 낮은 탭 밀도를 갖는 전이금속 전구체 및 높은 입자 강도를 가진 리튬 전이금속 산화물
CN108432002B (zh) 2016-01-06 2021-06-18 住友金属矿山株式会社 非水类电解质二次电池用正极活性物质及其前驱体、以及它们的制造方法
EP3281915B1 (en) 2016-08-10 2019-02-20 Umicore Precursors for lithium transition metal oxide cathode materials for rechargeable batteries
EP3642160B1 (en) 2017-06-23 2021-01-20 Umicore Beta-nickel hydroxide doped with aluminum
CN108511671B (zh) * 2018-03-12 2021-04-06 中国科学院长春应用化学研究所 一种柔性电极及其制备方法、巨能柔性即用即制储电器件
US11884554B2 (en) 2018-03-27 2024-01-30 Basf Se Process for precipitating a carbonate or (oxy)hydroxide
CN109354077B (zh) * 2018-10-16 2021-05-07 中伟新材料股份有限公司 一种多结晶形态的三元前驱体及其制备方法
EP3659974A1 (en) * 2018-11-27 2020-06-03 Basf Se Process for making a nickel composite hydroxide
EP3659975A1 (en) * 2018-11-28 2020-06-03 Basf Se Process for the manufacture of a nickel composite hydroxide
EP3953305A1 (en) 2019-04-10 2022-02-16 Basf Se Process for precipitating a mixed hydroxide, and cathode active materials made from such hydroxide
FI4038019T3 (fi) 2019-10-01 2024-01-29 Basf Se Menetelmä sekoitetun karbonaatin tai sekoitetun (oksi)hydroksidin saostamiseksi
EP4196444B1 (en) 2020-08-13 2024-07-24 Basf Se Process for precipitating a mixed hydroxide
US20230406722A1 (en) 2020-10-13 2023-12-21 Basf Se Process for making a particulate (oxy)hydroxide, and particulate (oxy)hydroxide and its use
CA3204235A1 (en) * 2021-01-20 2022-07-28 Benjamin Johannes Herbert BERGNER Process for making a particulate (oxy)hydroxide

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009531173A (ja) * 2006-03-31 2009-09-03 ハー．ツェー．スタルク ゲゼルシャフト ミット ベシュレンクテル ハフツング 沈殿により化合物を製造するための装置及び方法
CN101857278A (zh) 2010-06-25 2010-10-13 浙江华友钴业股份有限公司 一种球形碳酸盐的制备方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3136668B2 (ja) * 1991-07-08 2001-02-19 松下電器産業株式会社 水酸化ニッケル活物質粉末およびニッケル正極とこれを用いたアルカリ蓄電池
JP3092222B2 (ja) * 1991-07-08 2000-09-25 松下電器産業株式会社 水酸化ニッケル活物質およびニッケル正極とこれを用いたアルカリ蓄電池
US5700596A (en) * 1991-07-08 1997-12-23 Matsushita Electric Industrial Co., Ltd. Nickel hydroxide active material powder and nickel positive electrode and alkali storage battery using them
JP3644186B2 (ja) * 1997-03-24 2005-04-27 松下電器産業株式会社 電池構成用金属水酸化物製造装置
US6660432B2 (en) 2000-09-14 2003-12-09 Ilion Technology Corporation Lithiated oxide materials and methods of manufacture
ZA200509225B (en) * 2003-05-30 2007-03-28 Jfe Mineral Co Ltd Method for producing composite oxide of metal
JP4929674B2 (ja) * 2004-10-27 2012-05-09 住友化学株式会社 球状ニッケル酸リチウム粒子の製造方法および球状の複合酸化物粒子の製造方法
DE102006049107A1 (de) * 2006-10-13 2008-04-17 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in elektrochemischen Anwendungen
JP5251332B2 (ja) * 2007-07-30 2013-07-31 住友金属鉱山株式会社 非水系電解質二次電池用正極活物質およびその製造方法、並びにこれを用いた非水系電解質二次電池
DE102007039471A1 (de) * 2007-08-21 2009-02-26 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Lithium-Sekundärbatterien
US8551659B2 (en) * 2007-11-12 2013-10-08 Gs Yuasa International Ltd. Active material for lithium secondary battery, lithium secondary battery, and method for producing the same
JP4877660B2 (ja) * 2008-09-30 2012-02-15 株式会社Ｇｓユアサ リチウム二次電池用活物質、その製造方法及びリチウム二次電池
JP2011057518A (ja) * 2009-09-11 2011-03-24 Kansai Shokubai Kagaku Kk 高密度ニッケル・コバルト・マンガン共沈水酸化物及びその製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009531173A (ja) * 2006-03-31 2009-09-03 ハー．ツェー．スタルク ゲゼルシャフト ミット ベシュレンクテル ハフツング 沈殿により化合物を製造するための装置及び方法
CN101857278A (zh) 2010-06-25 2010-10-13 浙江华友钴业股份有限公司 一种球形碳酸盐的制备方法

Also Published As

Publication number Publication date
CN103282310B (zh) 2015-04-29
CN103282310A (zh) 2013-09-04
JP2014510004A (ja) 2014-04-24
JP5872587B2 (ja) 2016-03-01
KR20140047577A (ko) 2014-04-22
WO2012095381A2 (de) 2012-07-19
WO2012095381A3 (de) 2012-11-15
EP2663527A2 (de) 2013-11-20
EP2663527B1 (de) 2014-11-19
TW201236978A (en) 2012-09-16

Similar Documents

Publication Publication Date Title
KR101903362B1 (ko) 전이 금속 수산화물의 제조 방법
US9630842B2 (en) Process for preparing transition metal hydroxides
KR102223214B1 (ko) 구형 입자들, 그것의 제조 및 용도
KR102223228B1 (ko) 구형 입자들, 그것의 제조 및 용도
KR102406752B1 (ko) 리튬 이온 배터리용 캐쏘드 물질의 제조 방법
EP3093272A1 (en) Cathode materials for lithium ion batteries, process for preparing the same and their use in electrochemical cells
KR101963103B1 (ko) 전이 금속 혼합 산화물들을 위한 전구체의 제조 방법
US10526212B2 (en) Mixed transition metal oxides for lithium ion batteries
EP3659975A1 (en) Process for the manufacture of a nickel composite hydroxide
KR101937129B1 (ko) 전이금속 카르보네이트의 제조 방법
US10882878B2 (en) Process for preparing transition metal carbonates
US9171652B2 (en) Process for preparing precursors for transition metal mixed oxides
CN113039668A (zh) 制备涂敷氧化物材料的方法
US8883350B2 (en) Process for preparing precursors for transition metal mixed oxides

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8