KR101825358B1 - Method of producing a cosmetic sulfur additive - Google Patents

Abstract

The present invention relates to a method for manufacturing a sulfur additive for cosmetic products. The sulfur additive manufacturing method consists of a sulfur toxicity removal and grinding step, a Sparassis crispa extract preparing step, and a grinding and mixing step sequentially executed to prepare the sulfur additive for cosmetic products. The sulfur toxicity removal and grinding step comprises: a first step of adding mineral sulfur in a steamer after grinding the sulfur in a predetermined size, steaming the sulfur for four or five hours by adding saturated steam thereto, heating and drying the sulfur at a predetermined temperature for 24 hours after arranging the sulfur drawn out from the steamer on an electric drying panel in a flat shape; and a second step of adding the sulfur in the steamer back again, supplying steam including acetic acid generated by heating water containing the acetic acid to the sulfur to steam the sulfur for four or five hours, and removing the sulfur from the steamer to repeat the process at least three to four times of arranging the sulfur on the electric drying panel in the flat shape and drying the sulfur at the predetermined temperature for 24 hours. The first and second steps are executed to remove toxicity and impurities contained in the sulfur before grinding the sulfur by using a nano-scale grinder in a nano-particle size. The Sparassis crispa extract preparing step is for grinding Sparassis crispa extract preparing step, stirring the ground Sparassis crispa extract preparing step with an alcohol/water solution for 10-12 hours, and adding the mixture in a high-pressure extractor, and extruding the mixture under a low pressure. The grinding and mixing step is for mixing the sulfur powder without toxicity and the extract of Sparassis crispa at a predetermined ratio, adding the mixture to the nano-scale grinder, and grinding the mixture in a nano-particle size.

Description

FIELD OF THE INVENTION [0001] The present invention relates to a method for producing a cosmetic sulfur additive,

The present invention relates to a method for producing a sulfur additive for use in cosmetics, and more particularly, to a method for preparing a sulfur additive for use in the manufacture of cosmetics, and more particularly, a method for preparing sulfuric acid by mixing sulfur with mushroom extract and pulverizing the mixture with a nanomill.

To this end, the present invention is characterized in that the mineral sulfur is crushed to a predetermined size and put into a steamer, saturated steam is added in one step for 4 to 5 hours, drawn out from the steamer, spread on an electric drying panel, heated and dried for 24 hours, , And the steam containing acetic acid generated by heating the water containing acetic acid in two stages is supplied, and the steam is supplied for 4 to 5 hours. Then, the steam is drawn out from the steamer and heated and dried for 24 hours at a constant temperature A method of disintegrating sulfur to remove toxic poisons and foreign substances contained in sulfur and then pulverizing it into a nanoparticle size by putting it into a nanomill mill;

The blossom mushroom was crushed and mixed with alcohol-containing water for 10 to 12 hours. The mixture was added to a high-pressure extruder and then subjected to a low-speed extrusion process. The blended mushroom extract was mixed with the decantered sulfur powder and the blossom mushroom extract. And then pulverizing and mixing the mixture while pulverizing the mixture into nanoparticle size.

Sulfur is an indispensable constituent of the living body corresponding to atomic number 16, period 6 group (group) 3 cycles of elements. It is a proved mineral that has been used for the long time in the healing of disease, Glucan, glycogen, chitosan, ergosterol, and trehalose. Betaglucan in particular is more abundant than other mushrooms because of its antibacterial, anti-inflammatory, anti-cancer effect and immunity .

However, since mineral sulfur is a toxic substance, it is very dangerous to use it directly in the human body, so it must be used as an admiral. Since the detoxified sulfur has the function of decontaminating heavy metals, harmful substances and chemical poison, it is used as an antidote, muscle pain remedy, , Anti-depressants, anti-inflammatory drugs, and external preparations for skin, as well as methods of admiral administration are well known. Therefore, collagen nutrition cream, skin, body lotion and shampoo which are mainly composed of sulfur are sold, It is known that the antitumor effect is good because of a large amount of beta-glucan.
It is known that Zygomycetum mushroom has a large amount of beta-glucan and 1,3-components, thus increasing the number of leukocytes and natural killer cells, thus giving a powerful immunocidal effect. It is known to have antimicrobial action and immunity, hypoglycemic action, skin regeneration and moisturizing effect, lowering of cholesterol It is widely known that there is action.

Prior art (1) Published patent publication No. 10-2009-0084369 Prior art (2) Published patent publication No. 10-2011-0114846 Prior art (3) Published patent publication No. 10-2016-0001953

In the present invention, the harmful poison and foreign matter are removed by breaking the mineral sulfur, and the extraction method of the extract of the Zygomy mushroom is developed by a new method, and the decolorized sulfur powder and the Zygomy mushroom extract are mixed in a weight ratio of 10: 1, And the mixture is pulverized and mixed while being pulverized together. Thus, it is possible to provide a sulfur additive for cosmetics which is excellent in performance when used as an additive for cosmetics and which is prevented from being precipitated and separated.

In the present invention, mineral sulfur is pulverized to a size of 2 to 10 mm in average particle diameter and is put into a steamer and saturated steam is supplied for 4 to 5 hours for 4 to 5 hours to be firstly steamed, then drawn out from the steamer and spread on an electric drying panel, Dried, and further put into a steamer. The acetic acid-containing aqueous solution containing 5 to 10% by weight of acetic acid was heated, and the steam containing acetic acid produced was supplied for 4 to 5 hours to be secondarily drained, drawn out from the steamer, The process of drying at a constant temperature for 24 hours is repeated at least three to four times to remove the harmful toxicity and foreign matter by collapsing the sulfur tissue by the steam containing saturated steam and acetic acid and then putting it into a nano- The crushed mushroom was crushed to a mean particle size of 2 to 5 mm and then an aqueous alcohol solution having an alcohol concentration of 10 to 20 wt% was applied to the crushed material in an amount of 100 The mixture was stirred for 10 to 12 hours and then placed in a high-pressure extractor. The mixture was extruded at a rate of 30 mℓ per 6 hours through a 0.03 mm-size extruder to produce a low-speed extruded mushroom extract And a powder mixing step of mixing the decanted sulfur powder and the extract of Zanthoxylum mushroom at a weight ratio of 10: 1, adding the nanosized powder to the nanoparticles, and pulverizing and mixing the nanoparticles to obtain a sulfur additive of the present invention .

According to the present invention thus manufactured, the mineral sulfur is crushed to a size of 2 to 10 mm and put in a steamer, and saturated steam is supplied for 4 to 5 hours to carry out a first steam, and the steam is drawn out and spread on an electric drying panel, And the acetic acid-containing vapor obtained by heating an aqueous solution of acetic acid containing 5 to 10% by weight of acetic acid is supplied, and the mixture is drawn for 4-5 hours and drawn out and spread on an electric drying panel to be dried. , Sulfur is decomposed due to vapor containing steam and acetic acid component, so that harmful toxic substances contained in the inside and foreign matters such as heavy metals are removed, dried and increased repeatedly by repeating the steps of toxicity And foreign matters can be removed at the same time, and since the powder is in a state of powder, it is easy to crush the nano-state with a nano crusher. The mixture was stirred for 10 to 12 hours and then placed in a high-pressure extractor. The mixture was extruded through a hole having an extrusion hole size of 0.03 mm for 30 hours, The extracted extract solution in which the glycogen, chitosan, ergosterol, tregalose and beta-glucan components contained in the mushroom of Brassica juncea can be prepared in an appropriate manner can be prepared. The extracted sulfur powder and the extract of Zanthoxylum mushroom : 1, and they are mixed together in a nano-crusher while being pulverized into nano-sized particles, whereby a particulate additive without separation and precipitation can be produced, which is advantageous in that it can be conveniently used in cosmetics production.

In addition, the additive of the present invention can be used to make cosmetic products by mixing an amount of 0.05% by weight with cosmetics, so that the inflammatory dermatitis caused on the skin can be calmed, the antibacterial effect can be exerted, , Promote cell growth, prevent skin aging, improve wrinkles in the skin, enhance keratin function of skin tissue according to the action of known becaglucan 1, 3 and accumulate in skin tissue, It is able to make skin healthy by detoxifying and it acts to aggregate the amino acid chain of enzyme called collagenase which is involved in collagen molecules that lead to the elasticity of skin tissue, thereby enhancing skin elasticity. Which not only contributes to the action of raising newborns but also enhances skin regeneration and protection and antibacterial effects Has the advantage that the product can be prepared, could see the calming effect on the dermatitis as a result of using the present invention below to create a sulfur body wash lotion,
(Before using sulfur body lotion for sulfur body) (after using sulfur body lotion for sulfur body body)

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Furthermore, by removing the detergent by the method of the present invention, it is possible to obtain the effect that the heavy metal is not detected in the detoxified sulfur powder.
Table 1
Heavy metal residual test results

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BRIEF DESCRIPTION OF THE DRAWINGS FIG.
Figure 2 shows an example of a high-
Figure 3 shows an example of drying sulfur in an electric panel dryer
Fig. 4 shows an example of a crushed mushroom
Fig. 5 is an illustration of an example of a mushroom extract.

In the present invention, the mineral sulfur is pulverized to a size of 2 to 10 mm in average particle diameter and is introduced into the steamer, and the saturated steam is fed for 4 to 5 hours. The steam is drawn out from the steamer after the first steamer is spread over the electric dryer panel, , A second step of supplying steam containing acetic acid produced by heating an aqueous solution of acetic acid containing 5 to 10% by weight of acetic acid for 4 to 5 hours by adding primary dried sulfur into a steamer, The second drying step of extracting from the steamer after spreading and spreading on the electric drying panel and drying it at a constant temperature for 24 hours is repeated at least three to four times to bring the sulfur into contact with the steam containing steam and acetic acid components, To remove the harmful poison and foreign matter, and the toxicity and foreign matter are removed by repeating the steps of heating and drying, and the mixture is added to a nano crusher to produce nano-sized fine particles And 10 parts by weight of an aqueous alcohol solution having an alcohol concentration of 10 to 20% by weight was added to an agitator in an amount of 10 to 12 parts by weight per 100 parts by weight of the crushed product. And stirring the mixture for 10 to 12 hours. The mixture was put into a high-pressure extractor and extruded at a rate of 30 mℓ for 6 hours through a 0.03 mm-size extruder to extract the active ingredient thoroughly. A step of mixing the decontaminated sulfur powder and the powdery mushroom extract at a weight ratio of 10: 1, and pulverizing and mixing the same into a nanoparticle size by putting the same into a nanorodilizer to carry out the precipitation-free mixing to be.

Meanwhile, since the high pressure extractor used in the present invention is sold in the market, a detailed description thereof will be omitted, and it is preferable that the electric dry panel is adjusted so as to emit heat of 25 to 30 ° C constantly.

Claims (1)

Mineral sulfur is pulverized into an average particle size of 2 ~ 10mm and placed in a steamer. The first step of supplying saturated steam for 4 ~ 5 hours, the first step is taken out from the steamer, and the product is spread on an electric drying panel and dried at a constant temperature for 24 hours A second step of supplying the steam containing acetic acid produced by heating an aqueous acetic acid solution containing 5 to 10% by weight of acetic acid to the steamer for 4 to 5 hours, A second drying step in which the green tea leaves are drawn out from the steamer and spread on the electric drying panel and dried at a constant temperature for 24 hours, and the method is repeated three to four times to remove harmful poison and foreign substances, The granules were crushed to have an average particle size of 2 to 5 mm and then placed in a stirrer. An alcohol aqueous solution having an alcohol concentration of 10 to 20% by weight was added to 100 parts by weight of the crushed material 10 to 12 parts by weight and stirring for 10 to 12 hours, stirring the mixture into a high-pressure extractor and extruding the mixture at a slow speed of 30 mℓ for 6 hours through a 0.03 mm-size extruder, A step of mixing the decontaminated sulfur powder and the extract of Zanthoxylum mushroom at a weight ratio of 10: 1, and a step of pulverizing and mixing the mixture with the nanoparticles while pulverizing the same into nanoparticles.

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