CN105476946B - A kind of preparation method of deodorization pearl powder - Google Patents
A kind of preparation method of deodorization pearl powder Download PDFInfo
- Publication number
- CN105476946B CN105476946B CN201510975286.XA CN201510975286A CN105476946B CN 105476946 B CN105476946 B CN 105476946B CN 201510975286 A CN201510975286 A CN 201510975286A CN 105476946 B CN105476946 B CN 105476946B
- Authority
- CN
- China
- Prior art keywords
- pearl powder
- suspension
- pearl
- deodorization
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Zoology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of preparation method of deodorization pearl powder, the preparation method is：Raw material pearl powder A and deionized water are hybridly prepared into pearl powder suspending liquid A, pearl powder suspending liquid A is placed in air dry oven, dry 18~30h, obtains pearl powder B at 60~100 DEG C；Pearl powder B and deionized water are hybridly prepared into pearl powder suspension B, pearl powder suspension B is placed in air dry oven, dry 18~30h, the pearl powder of drying is crushed with airslide disintegrating mill, gets product deodorization pearl powder afterwards at 60~100 DEG C；Further, eliminating smell agent can be added in the pearl powder suspension B, then carries out subsequent operation；Preparation method technique of the present invention is simple, it can be achieved that property is strong, deodorization positive effect；Used eliminating smell agent non-toxic and safe, it is miscible with water, it is cheap and pollution-free, be conducive to promote and apply.
Description
(1) technical field
The invention belongs to the cosmetics of super quality, a kind of high-grade health medicine field, and in particular to green cleaning deodorization pearl powder
Preparation method.
(2) background technology
Pearl powder is both a kind of jewellery for being used to decorate and a kind of valuable Chinese medicine and cosmetics.The Ming Dynasty of China writes
Name physician's Li Shizhen (1518-1593 A.D.) exists《Compendium of Materia Medica》Described in：" pearl cures mainly：Relieving palpitation.Point mesh, removes skin ocular film.Painting face, makes us moist
Good color；Brothers are applied, remove skin hangnail." pearl powder is combined into by inorganic constituents and organic principle, wherein organic principle is main
It is protein.Protein is made of peptide, and peptide is made of amino acid.Amino acid one shares 22 kinds, wherein having one
Part is sulfur-containing amino acid (SAA), mainly including cystine, cysteine and methionine.These amino acid are for human skin
And skin derivative (nail, hair) play the role of it is indispensable.Major protein in pearl is keratin.Keratin is at it
In the case that peptide chain is unopened, the chemical bond between amino acid is combined closely, almost without any smell；And this peptide
Chain is once opened, amino acid, and especially sulfur-containing amino acid is just directly exposed in air, and it is distinctive to give out these amino acid
Smell, here it is " fishy smell " described in us.The removal of pearl powder fishy smell is always to perplex the problem of pearl powder processing industry.
Chinese invention patent (application number：CN201010522608.2, the applying date：2010.10.28) disclosed in a kind of deodorization
The preparation method of taste pearl powder, this method include crushing pearl process and pearl powder suspension preparation section, pearl powder are suspended
Flavor guide is added in liquid, efficient ventilating drying device will be inserted added with the pearl powder suspension of flavor guide, taken a breath by outer circulation,
The off-flavors in pearl powder are removed, the pearl powder after dry deodorization is crushed again, forms the pearl powder of smelling removal.This method
The flavor guide of selection is one or more in ethanol, ethyl acetate and their aqueous solution, and the flavor guide of selection is organic molten
Agent, remaining flavor guide can pollute pearl powder, possible do harm to huamn body.
The present invention is directed to above-mentioned technical barrier, has designed and developed a kind of preparation method of green cleaning deodorization pearl powder.
(3) content of the invention
In order to solve the problems, such as that the preparation method of existing deodorization pearl powder can not safely and effectively remove fishy smell, the present invention provides
A kind of preparation method of green cleaning deodorization pearl powder, can be widely applied to cosmetic field.
The present invention adopts the following technical scheme that：
A kind of preparation method of deodorization pearl powder, the preparation method carry out as follows：
(1) one time prepared by suspension：Raw material pearl powder A (2000~3000 mesh) and deionized water are hybridly prepared into pearl
Powder suspending liquid A, the concentration of the pearl powder suspending liquid A is 20wt%~80wt% (preferably 30wt%~50wt%)；
(2) suspension dryings：Pearl powder suspending liquid A obtained by step (1) is placed in air dry oven, 60~
Dry 18~30h (preferably 24h), obtains pearl powder B at 100 DEG C；
(3) prepared by secondary suspension：Pearl powder B obtained by step (2) is hybridly prepared into pearl powder with deionized water to suspend
The concentration of liquid B, the pearl powder suspension B are 20wt%~80wt% (preferably 30wt%~50wt%)；
(4) secondary suspension drying：Pearl powder suspension B obtained by step (3) is placed in air dry oven, 60~
Dry 18~30h (preferably 24h), the pearl powder for crushing drying with airslide disintegrating mill afterwards (are crushed to 2000~3000 at 100 DEG C
Mesh), get product deodorization pearl powder.
Further, in preparation method step (3) of the present invention, it can add and remove in gained pearl powder suspension B
Taste agent, and stir evenly, then carry out the operation of step (4).The addition quality of the eliminating smell agent for pearl powder B mass 1%~
8% (preferably 5%)；The eliminating smell agent is hydroxycarboxylic acid or alpha-hydroxy carboxylic acid derivatives, and the hydroxycarboxylic acid is malic acid, breast
The mixture of one or both of acid, citric acid, glycolic, citramalic acid any of the above ratio, the hydroxycarboxylic acid derive
Thing is sodium citrate, one or both of hydroxy acid sodium with the mixture of arbitrary proportion, the preferably described eliminating smell agent is apple
Tartaric acid.
In the present invention, " pearl powder A ", " pearl powder B " is only intended to term without special implication labeled as " A ", " B "
Distinguish the pearl powder being previously mentioned in different step；" pearl powder suspending liquid A ", " pearl powder suspension B " is therewith similarly.
Compared with prior art, the present invention has the advantages that：
(1) preparation method technique of the present invention is simple, it can be achieved that property is strong, deodorization positive effect；
(2) eliminating smell agent non-toxic and safe of the present invention, it is miscible with water, it is cheap and pollution-free, be conducive to promote
Using.
(4) embodiment
Technical scheme is further described in detail below by embodiment, but protection scope of the present invention is not
It is limited to this.
Embodiment 1
(1) one time prepared by suspension：9g raw materials pearl powder (size is 2000~3000 mesh) is chosen, with 21mL deionized waters
As solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：The pearl powder suspension that step (1) is prepared is in 60 DEG C of dryings one of air dry oven
My god, obtain dry pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent malic acid 0.45g, (additive amount is pearl powder gross mass
5%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
80 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 2
(1) one time prepared by suspension：9g raw materials pearl powder (size is 2000~3000 mesh) is chosen, with 21mL deionized waters
As solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：The pearl powder suspension that step (1) is prepared is in 70 DEG C of dryings one of air dry oven
My god, obtain dry pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent citric acid 0.45g, (additive amount is pearl powder gross mass
5%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
80 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 3
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 90 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent lactic acid 0.45g, (additive amount is pearl powder gross mass
5%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
100 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 4
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 60 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent citramalic acid 0.45g, (additive amount is pearl powder gross mass
5%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
100 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 5
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 80 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent malic acid 0.27g, (additive amount is pearl powder gross mass
3%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
60 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 6
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 70 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent malic acid 0.36g, (additive amount is pearl powder gross mass
4%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
70 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 7
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 90 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent malic acid 0.54g, (additive amount is pearl powder gross mass
6%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
80 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 8
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 100 DEG C of air dry oven, obtain drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent sodium citrate 0.45g, (additive amount is pearl powder gross mass
5%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
60 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 9
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 100 DEG C of air dry oven, obtain drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent natrium malicum 0.45g, (additive amount is pearl powder gross mass
5%), the pearl powder suspension for adding eliminating smell agent is stirred evenly, removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
80 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 10
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 80 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent hydroxy acid sodium 0.45g, (additive amount is pearl powder gross mass
5%), by add eliminating smell agent pearl powder suspension stir evenly, remove fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
90 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 11
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 60 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent malic acid 0.27g, (additive amount is pearl powder gross mass
3%) eliminating smell agent citric acid 0.18g (additive amount is the 2% of pearl powder gross mass), is added, the pearl powder for adding eliminating smell agent is hanged
Supernatant liquid stirs evenly, and removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
60 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 12
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 80 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent malic acid 0.27g, (additive amount is pearl powder gross mass
3%) eliminating smell agent lactic acid 0.18g (additive amount is the 2% of pearl powder gross mass), is added, the pearl powder for adding eliminating smell agent is suspended
Liquid stirs evenly, and removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
60 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~3000 mesh).
Embodiment 13
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 70 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again, adding eliminating smell agent sodium citrate 0.27g, (additive amount is pearl powder gross mass
3%) eliminating smell agent hydroxy acid sodium 0.18g (additive amount is the 2% of pearl powder gross mass), is added, the pearl of eliminating smell agent will be added
Powder suspension stirs evenly, and removes fishy smell.
(4) secondary suspension is dry and crushes：By the pearl powder suspension of the addition eliminating smell agent obtained by step (3) in air blast
80 DEG C of drying box is drying for one day, and the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~300 mesh).
Embodiment 14
(1) one time prepared by suspension：It is 2000~3000 mesh to choose 9g raw material pearl powders size, is made with 21mL deionized waters
For solvent, the pearl powder suspension of compound concentration 30%.
(2) suspension dryings：Pearl powder suspension is drying for one day in 70 DEG C of air dry oven, obtain the treasure of drying
Pearl powder 9g.
(3) prepared by secondary suspension：Pearl powder 9g dry obtained by step (2) is taken, using 21mL deionized waters as solvent,
The pearl powder suspension of compound concentration 30% again.
(4) secondary suspension is dry and crushes：Pearl powder suspension obtained by step (3) is dry in 80 DEG C of air dry oven
Dry one day, the pearl powder of drying is crushed with airslide disintegrating mill, gets product 9g (2000~300 mesh).
Sensory evaluation is carried out to 1~14 finished product deodorization pearl powder of embodiment below, with not carrying out except the pearl powder of raw meat processing
Contrast, fishy smell is 0,1,2,3,4,5 point from high to low, and the scoring of untreated pearl powder is 0 point, and fishy smell is completely without for 5 points, valuation officer
5.
Influence of the different hydroxycarboxylic acids of table 1 to pearl powder deodorization effect
Influence of 2 malic acid concentration of table to pearl powder deodorization effect
Influence of the different alpha-hydroxy carboxylic acid derivatives of table 3 to pearl powder deodorization effect
Influence of the different alpha-hydroxy carboxylic acid derivatives of table 4 to pearl powder deodorization effect
Above example is only the more representational example of the present invention.Obviously, technical scheme is not limited to
Embodiment is stated, there can also be many changes.Those of ordinary skill in the art become from present disclosure is directly derived
Change, be considered as protection scope of the present invention.
Claims (7)
1. a kind of preparation method of deodorization pearl powder, it is characterised in that the preparation method carries out as follows：
(1) one time prepared by suspension：Raw material pearl powder A and deionized water are hybridly prepared into pearl powder suspending liquid A, the pearl
The concentration of powder suspending liquid A is 20wt%~80wt%；
(2) suspension dryings：Pearl powder suspending liquid A obtained by step (1) is placed in air dry oven, at 60~100 DEG C
18~30h of lower drying, obtains pearl powder B；
(3) prepared by secondary suspension：Pearl powder B obtained by step (2) is hybridly prepared into pearl powder suspension B with deionized water,
The concentration of the pearl powder suspension B is 20wt%~80wt%；Eliminating smell agent is added in gained pearl powder suspension B, and is stirred
Mix the pearl powder suspension B for uniformly, obtaining with the addition of eliminating smell agent；
The eliminating smell agent is hydroxycarboxylic acid or alpha-hydroxy carboxylic acid derivatives, and the hydroxycarboxylic acid is malic acid, lactic acid, lemon
The mixture of one or both of acid, glycolic, citramalic acid any of the above ratio, the alpha-hydroxy carboxylic acid derivatives are lemon
One or both of sour sodium, hydroxy acid sodium are with the mixture of arbitrary proportion；
The addition quality of the eliminating smell agent is the 1%~8% of pearl powder B mass；
(4) secondary suspension drying：The pearl powder suspension B that with the addition of eliminating smell agent obtained by step (3) is placed in air dry oven
In, dry 18~30h, the pearl powder of drying is crushed with airslide disintegrating mill, gets product deodorization pearl afterwards at 60~100 DEG C
Powder.
2. the preparation method of deodorization pearl powder as claimed in claim 1, it is characterised in that in step (3), the eliminating smell agent
Add 5% that quality is pearl powder B mass.
3. the preparation method of the deodorization pearl powder as described in one of claim 1~2, it is characterised in that described in step (1)
Raw material pearl powder A be 2000~3000 mesh.
4. the preparation method of the deodorization pearl powder as described in one of claim 1~2, it is characterised in that described in step (1)
The concentration of pearl powder suspending liquid A is 30wt%~50wt%.
5. the preparation method of the deodorization pearl powder as described in one of claim 1~2, it is characterised in that described in step (3)
The concentration of pearl powder suspension B is 30wt%~50wt%.
6. the preparation method of the deodorization pearl powder as described in one of claim 1~2, it is characterised in that in step (4), use gas
Flow pulverizer and crush the pearl powder of drying to 2000~3000 mesh.
7. the preparation method of deodorization pearl powder as claimed in claim 1, it is characterised in that the eliminating smell agent is malic acid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510975286.XA CN105476946B (en) | 2015-12-22 | 2015-12-22 | A kind of preparation method of deodorization pearl powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510975286.XA CN105476946B (en) | 2015-12-22 | 2015-12-22 | A kind of preparation method of deodorization pearl powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105476946A CN105476946A (en) | 2016-04-13 |
| CN105476946B true CN105476946B (en) | 2018-05-08 |
Family
ID=55664466
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510975286.XA Active CN105476946B (en) | 2015-12-22 | 2015-12-22 | A kind of preparation method of deodorization pearl powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105476946B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106619727A (en) * | 2016-11-28 | 2017-05-10 | 湖州珍露生物制品有限公司 | Pearl powder and preparation method thereof |
| CN110432488A (en) * | 2019-09-16 | 2019-11-12 | 海南京润珍珠科技有限公司 | A kind of preparation method of deodorization pearl powder |
| CN116762962A (en) * | 2023-05-09 | 2023-09-19 | 南京珠聚堂科技有限公司 | Polypeptide, application of polypeptide and composition containing polypeptide |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1541655A (en) * | 2003-04-30 | 2004-11-03 | 北京自然爱康生物技术发展有限公司 | Nano-scale pearl powder preparation method |
| CN101961350A (en) * | 2010-10-28 | 2011-02-02 | 浙江欧诗漫集团德清生物科技有限公司 | Preparation method of fishy smell-removed pearl powder |
| CN101966140A (en) * | 2010-10-28 | 2011-02-09 | 浙江欧诗漫集团德清生物科技有限公司 | Method for preparing fishy smell removed submicron pearl powder with regular geometric shape |
-
2015
- 2015-12-22 CN CN201510975286.XA patent/CN105476946B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1541655A (en) * | 2003-04-30 | 2004-11-03 | 北京自然爱康生物技术发展有限公司 | Nano-scale pearl powder preparation method |
| CN101961350A (en) * | 2010-10-28 | 2011-02-02 | 浙江欧诗漫集团德清生物科技有限公司 | Preparation method of fishy smell-removed pearl powder |
| CN101966140A (en) * | 2010-10-28 | 2011-02-09 | 浙江欧诗漫集团德清生物科技有限公司 | Method for preparing fishy smell removed submicron pearl powder with regular geometric shape |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105476946A (en) | 2016-04-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105476946B (en) | A kind of preparation method of deodorization pearl powder | |
| CN106309280B (en) | A kind of Ginger P.E and its preparation method and application | |
| KR101565778B1 (en) | Manufacturing Method of Antibiosis Soap Containing Xinc Oxide of Nano Size and Antibiosis Soap Thereof | |
| WO2017148180A1 (en) | Rosemary moisturizing solution and manufacturing method therefor | |
| CN102617897A (en) | Preparation method of rubber gloves containing natural vanilla extracts | |
| CN1522688A (en) | Compositions containing a cosmetically active organic acid and a legume product | |
| JP2013027383A (en) | Oral food producing negative hydrogen ion after eating | |
| CN107737039A (en) | Containing ginger without silicone oil without sulfate health-care shampoo and its preparation technology | |
| KR102093620B1 (en) | Functional salt with effective component hot-melt mixed and preparation method thereof | |
| CN108707502B (en) | Preparation method and application of alligator oil | |
| CN103919119B (en) | Double glue Ganoderma spore powder with cellular wall broken of a kind of antioxidative and preparation method thereof | |
| CN106214557A (en) | The preparation method of purely-natural liquid shampoo | |
| CN109833248A (en) | A kind of preparation method of antibacterial permanent tooth health-care toothpaste | |
| CN108066181A (en) | Whitening anti-aging skin conditioner | |
| KR20180110357A (en) | Cosmetic composition for preventing oxidative stress comprising nephrite water and nephrite powder | |
| CN106754138A (en) | Multiple-ear rock Ke's extract Processing wine | |
| CN105267108A (en) | Premna microphylla skin-protecting gel facing preparation | |
| CN106580743A (en) | DHA essence original substance and preparation method of same | |
| CN106434049A (en) | Method for preparing dendrobe enzyme handmade soap | |
| JP5709371B2 (en) | Noodle food | |
| CN108514532A (en) | A kind of compound grape skin active skull cap components face mask cream and preparation method thereof | |
| CN103859383A (en) | Ecologic health food and making method thereof | |
| KR101437059B1 (en) | Cosmetic composition that contains phellinus linteus and natural conjugated materials with skin whitening effect | |
| KR102483898B1 (en) | Natural flour soap composition containing rice bran oil and manufacturing method thereof | |
| CN107296879A (en) | It is a kind of to increase the composition and preparation method of bone density preventing bone rarefaction |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |