KR102135323B1 - mineral sulfur legislation method - Google Patents

Abstract

The present invention relates to a mineral sulfur detoxification method comprising: a first steaming step in which mineral sulfur is ground to an average particle size of 2-10 mm and is placed in a heating vessel and provided with saturated steam for 4-5 hours; a first drying step in which the product obtained from the first steaming is taken out of the heating vessel, and is spread on a drying panel equipped with an electric heater and dried for 24 hours at 30-35°C; a second steaming step in which the product obtained from the first drying is placed back in the heating vessel and steamed for 4-5 hours with acetic acid-containing steam prepared by heating an aqueous acetic acid solution containing 5-10 wt% of acetic acid; a second drying step in which the sulfur obtained from the second steaming is taken out, thinly spread on a drying panel equipped with an electric heater, and dried for 24 hours at 30-35°C; a first detoxification step in which the sulfur obtained thus is rinsed after repeating the first and second drying steps 3-4 times; a second detoxification step in which the sulfur obtained from the first detoxification is immersed in fermented vinegar and heated at 80°C for 2 hours before being taken out and rinsed; a third detoxification step in which the sulfur obtained from the second detoxification is placed in a solution mixture containing water and alcohol in a ratio of 6:4 and is heated at 60°C for 1-2 hour before being taken out and rinsed; and a step in which after the sulfur obtained after the first, second, and third detoxification steps is immersed in water with cypress leaves and green tea leaves and heated at 100°C for two hours, and subsequently, only the sulfur is taken out and rinsed, the rinsed sulfur is then placed and fermented for 24 hours in a heated solution boiled with cypress leaves and green tea leaves, and the sulfur is taken out from the ferment solution and dehydrated for 24 hours in a drying room emitting far-infrared rays before being ground.

Description

Mineral sulfur legislation method

The present invention relates to a method for regulating mineral sulfur, and more specifically, it is first, second, and third detoxified with mineral sulfur, aged and placed in a drying chamber that emits far-infrared rays, and dried to produce fine powder, thereby ensuring safety. In providing sulfur that can be used in the field.

In the present invention, the mineral sulfur is crushed to an average particle size of 2 to 10 mm, placed in a heating container, and the primary steaming step of supplying saturated water vapor for 4 to 5 hours, and after the first steaming, withdrawal from the heating container and drying with an electric heater. The primary drying step of spreading on a panel and drying at 30 to 35° C. for 24 hours, the primary dried one is put back into a heating container, and acetic acid produced by heating an aqueous acetic acid solution containing 5 to 10% by weight of acetic acid is contained. A second drying step of increasing the amount by contact with steam for 4 to 5 hours, and a second drying step of drawing the second increased sulfur and spreading it thinly on a drying panel equipped with an electric heater to dry at 30 to 35° C. for 24 hours; The first and second drying steps are repeated three to four times to perform the first detoxification step, and the first detoxified sulfur is immersed in fermented vinegar, heated at 80° C. for 2 hours, and then withdrawn and washed. The detoxification step and the third decontamination step, in which the second decontaminated sulfur is mixed into a mixed solution of water and alcohol in a ratio of 6:4, heated to 60° C. for 1 to 2 hours, and withdrawn and washed with water. After putting the sulfur that has undergone the tea and tertiary detoxification steps into the water, such as the cypress leaves and green tea leaves, heat it for 2 hours at 100°C, and then withdraw only the sulfur to rinse and wash the washed sulfur with cypress leaves and green tea leaves. It is a mineral sulfur manufacturing method consisting of aging in 24 hours by immersing in a heated solution, extracting sulfur from the aged solution, putting it in a drying chamber where far infrared rays are emitted, dehumidifying and drying for 24 hours, and then grinding.

Conventional legal sulfur is known to feed sulfur to livestock, such as ducks, to eat meat containing sulfur, and it is known to include sulfur components in plants by giving sulfur as a fertilizer, and edible sulfur plants.

However, the above methods have a inconvenience in that when using sulfur for other purposes, it is inconvenient to select an appropriate amount, and when preparing food, making a medicine, or manufacturing a cosmetic, the appropriate amount cannot be properly mixed.

The present invention was developed to solve the above inconvenience.

In the present invention, the mineral sulfur is crushed to an average particle size of 2 to 10 mm, placed in a heating container, and the primary steaming step of supplying saturated water vapor for 4 to 5 hours, and after the first steaming, withdrawal from the heating container and drying with an electric heater. The primary drying step of spreading on a panel and drying at 30 to 35° C. for 24 hours, the primary dried one is put back into a heating container, and acetic acid produced by heating an aqueous acetic acid solution containing 5 to 10% by weight of acetic acid is contained. A second drying step of increasing the amount of contact with steam for 4 to 5 hours, a second drying step of drawing out the second increased sulfur and spreading it thinly on a drying panel equipped with an electric heater to dry it for 24 hours; The primary detoxification step of washing by repeating the secondary drying step 3 to 4 times, and the secondary decontamination step of immersing the primary decontaminated sulfur in fermented vinegar, heating at 80° C. for 2 hours, and then withdrawing and washing, The second decontamination sulfur is placed in a mixed solution of water and alcohol in a ratio of 6:4, heated for 1 to 2 hours at 60°C, and the third decontamination step of drawing and washing with water, and the first, second, and third Put the sulfur that has undergone the decontamination step together with the cypress leaf and green tea leaves and heat it for 2 hours at 100℃, then extract and wash only the sulfur, and put the washed sulfur in the heating solution with the cypress leaf and green tea leaves. This is a mineral sulfur manufacturing method that aging for 24 hours, extracting sulfur from the aging liquid, put it in a drying chamber where far infrared rays are emitted, dehumidify and dry for 24 hours, and then smash.

In the present invention, the mineral sulfur is first dried with saturated water vapor, dried, and then subjected to secondary drying with steam containing acetic acid 3 to 4 times, followed by immersion in fermented vinegar and heating. After washing with water, put it in a mixture of water and alcohol, heat it, boil it in water with green tea leaves and green tea leaves, rinse it, immerse it again in a heating solution of green tea leaves and green tea leaves, mature, and then draw out to emit far infrared rays It is possible to make a necessary sulfur product by quantitatively supplying to various fields because it is possible to make decontaminated sulfur powder by sequentially performing a method of drying in a drying chamber.

In the present invention, the mineral sulfur is crushed to an average particle size of 2 to 10 mm, placed in a heating container, and the primary steaming step of supplying saturated water vapor for 4 to 5 hours, and after the first steaming, withdrawal from the heating container and drying with an electric heater. First drying step of spreading on a panel and drying at 30~35℃ for 24 hours, and putting the first dried thing back into a heating container, and contains acetic acid components produced by heating an aqueous acetic acid solution containing 5-10% by weight of acetic acid 2nd steaming step to increase steam by contacting steam for 4-5 hours, 2nd drying step to take out the 2nd steamed sulfur from a heating container and spread it thinly on a drying panel equipped with electric heater to dry it for 24 hours. The primary detoxification step of washing by repeating the 2nd step 3-4 times, the 2nd detoxification step of immersing the 1st detoxified sulfur in fermented vinegar, heating at 80°C for 2 hours, and the 2nd decontamination step of washing The 3rd detoxification step of putting the decontaminated sulfur into a mixed solution of water and alcohol in a ratio of 6:4, heating for 1 to 2 hours at 60°C, and drawing and washing with water, and the 1st, 2nd, 3rd decontamination After putting the sulfur that has passed through the steps into water with green tea leaves and green tea leaves, and heating it for 2 hours at 100°C, extract the sulfur and wash it, and then put the green tea leaves and green tea leaves into a heated solution for aging for 24 hours. It is characterized in that it is prepared by drawing the aged sulfur, putting it in a drying chamber where far infrared rays are emitted, drying it for 24 hours, and then pulverizing it.

Mineral sulfur is a nonmetallic element represented by the element symbol S with an atomic number of 16 and an atomic weight of 32.06.

The melting point is 120°C and the specific gravity is 1.92.

It is a crisp crystal of silver and yellow odorless at room temperature, and at high temperature, sulfide is made by combining with almost all metals or hydrogen except gold and platinum.

When ignited, a blue flame is generated, and it is used in the manufacture of raw materials, medicines, pesticides, and pulp of gunpowder and substances.

In addition, sulfur is used to neutralize the acid, and sulfur is also used in pesticide and fertilizer manufacturing because it has an excellent effect on sterilization and insecticidal action of crops.

In addition, sulfur is necessary for the growth factors of animals and plants, but it is toxic, so there is a inconvenience that it cannot be used freely.

The present invention has the advantage of adding a quantity to various fields by removing the toxicity of the mineral sulfur as described above and pulverizing it.

In particular, the present invention, after the primary sulfur is dried by steam with water vapor and dried, and then repeated by steaming with steam containing acetic acid, drying is repeated 3-4 times, then put into fermented vinegar and heated to 80°C. After washing, put it in a mixed solution of water and alcohol, heat it to 60°C, wash it, heat it for 2 hours like a cypress leaf and green tea leaves, wash it, and put it in a rinse solution of the cypress leaf and green tea leaves. Then, by washing and then drying and crushing, decontamination free of foreign matter is achieved, thereby having the advantage of selecting safe sulfur.

Claims (1)

The mineral sulfur is crushed to an average particle size of 2 to 10 mm, placed in a heating container, and the primary steaming step of supplying saturated water vapor for 4 to 5 hours. The primary drying step of drying at 30 to 35° C. for 24 hours, the primary dried ones are put back into a heating container, and the acetic acid component generated by heating the acetic acid aqueous solution containing 5 to 10% by weight of acetic acid is heated to steam. A second increase in stage for 4 to 5 hours of contact, and
A second drying step of drawing the second increased sulfur from the heating vessel and spreading it thinly on a drying panel equipped with an electric heater to dry for 24 hours;
The primary detoxification step of washing by repeating the above-described primary and secondary steaming and drying steps 3 to 4 times, and the primary decontaminated sulfur is immersed in fermented vinegar, heated to 80° C. for 2 hours, and then washed 2 The primary detoxification step and the tertiary detoxification step, in which the second decontaminated sulfur is placed in a mixed solution of water and alcohol in a ratio of 6:4, heated to 60° C. for 1 to 2 hours, and then withdrawn and washed with water. Put the sulfur that has passed through the 2nd and 3rd decontamination steps into the water together with the cypress leaves and green tea leaves, boil them for 2 hours, then extract and wash the sulfur, and then put sulfur in the cypress leaves and green tea leaf decoction for 24 hours. A method of mineral sulfur production, comprising aging, drawing the aged sulfur into a drying chamber where far infrared rays are emitted, dehumidifying and drying for 24 hours, and then grinding.