KR101797852B1 - Perfume composition for expressing the fragrance of nelumbo nucifera habitat in songnisan - Google Patents

Abstract

The present invention relates to a perfume composition that reproduces the spatial flavor of Solanthus sinensis community. The present invention relates to a perfume composition that reproduces the spatial flavor of Solanthus sinensis community, extracting optimal solvents based on the intrinsic fragrance components of the Solanthus spinach community excluding allergen components, And a perfume composition having excellent palatability.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a perfume composition which reproduces the spatial flavor of Lotus Polyglainaceae community. ≪ Desc / Clms Page number 1 >

The present invention relates to a perfume composition that reproduces the spatial flavor of Solanthus sinensis community. The present invention relates to a perfume composition that reproduces the spatial flavor of Solanthus sinensis community, extracts optimal contents based on the intrinsic fragrance components of the Solanthus spinach community excluding allergen components, And a perfume composition having excellent palatability.

The desire to spend the time of healing in the nature leaving the everyday space to the modern people living busy life is getting bigger, but there are many modern people who do not even have enough time to leave the forest and leave for the forest. The present inventors have conceived the present invention to provide a method of easily healing time within a short time by providing a space-recreating perfume composition that appears to be in a real forest.

The present inventors have selected Korean Solanum lotus flower community as an area having a Korean beauty and healing sensation and perfume composition which gives an image of space and a distinctive feeling by inventing a perfume composition recreating the space perfume.

Lotus ( Nelumbo nucifera ) is a perennial herbaceous plant belonging to the water lily family. Its roots extend long to the side, are columnar, have many nodes, and the ends are particularly thick in autumn. The leaves come out from the rhizome and rise high on the water, close to the circle, white green, vein spreads all over and it is about 40㎝ in diameter and does not get wet. Petioles (petioles) are circumferential and have short thorn like projections. Flowers bloom in July and August, 15-20 cm in diameter, light pink or white, and the flower has a thorn like petiole, and one flower at the end. Calyx is green and early fall, petal is 8 ~ 12㎝ long and width is 3 ~ 7㎝, obovate obtuse, and the surface is flat and large, spongy, length and diameter are 10cm each. The fruit is elliptical and 2㎝ long and can be eaten.

Mt. Esu is one of the main distribution areas of lotus, with a lot of about 4,000 lotus flowers in a 16,000 square meter area, and its scenery and flavor are famous, and it is loved by many people.

There are many ways to reproduce spatial incoherence. For example, a solvent extraction method in which a plant in the space is collected by a commonly used method to make a fragrance ingredient into an absolute form, and a steam distillation method in which a fragrance ingredient is made into essential oil. However, the above methods require high heat in the extraction process, or the process is complicated and takes a lot of time, which may be different from the original flavor. In addition, it does not meet the object of the present invention because it reproduces the fragrance of the plant rather than reproducing the perfume of the space itself.

In the present invention, the dynamic headspace method used for analyzing the spatial fragrance component does not require a solvent and does not require a pretreatment step, so that the fragrance component in the actual space can be directly analyzed.

The dynamic headspace method is a method in which air is circulated through a resin for a predetermined period of time using a collection device equipped with a resin capable of adsorbing a perfume to an air pump, The fragrance ingredients contained in a trace amount can be measured.

In addition to various fragrance and flavor components such as terpene, phenol, ketone, and ester, the analyzed aroma components include volatile organic chemical components generally present in the air and allergen components that can cause an allergic reaction. Ingredients such as limonene, hexyl cinnamic acid, linanol, benzyl alcohol, geraniol and the like are fragrance ingredients and can cause allergies. When these ingredients are incorporated directly into the perfume composition, they may cause problems such as allergic reaction.

Accordingly, the inventors analyzed the spatial flavor components of the Solanthus sinensis community harvested through the dynamic headspace method, and then, based on the remaining flavor components except for the general atmospheric and allergen components, the perfume composition .

Further, the inventors of the present invention have perfected the fragrance composition having a high degree of preference while reproducing the spatial flavor of the Solanaceae lotus flower community by adjusting the content of the fragrance ingredient and using a solvent suitable therefor.

Accordingly, a problem to be solved by the present invention is to provide a perfume composition which reproduces the spatial flavor of Solanthus sinensis community.

Another object of the present invention is to provide a fragrance composition that reproduces the spatial flavor of Solanthus sinensis community without inducing an allergic reaction by excluding the allergen component from the components collected by the dynamic headspace method.

Another object to be solved by the present invention is to provide a fragrance composition which reproduces the spatial flavor of Lotus Polygonaceae community by selecting a suitable solvent and adjusting the content of the fragrance ingredient, and has an excellent taste.

Another object of the present invention is to provide a cosmetic composition comprising the perfume composition.

Another object of the present invention is to provide a perfume composition comprising the perfume composition.

Another object to be solved by the present invention is to provide a composition for external application for skin comprising the perfume composition.

In order to solve the above problems, the present invention provides a perfume composition recreating the spatial flavor of Solanaceae lotus flower community containing the fragrance component of Solanaceae lotus flower community as an active ingredient.

The above-mentioned fragrance component includes allergen components of the space-oriented component of the Lotus Solanaceae community, and more specifically includes dimethyl hydroquinone, myrcene, eucalyptol and anisic aldehyde. do.

The present invention provides a fragrance composition that reproduces the spatial flavor of the Solanthus multiflorum community improved by using isopropyl myristate as a solvent to improve the reproducibility of fragrance and to have a soft feeling.

In one embodiment of the present invention, the perfume composition of the present invention comprises 45.0 to 98.5% by weight of dimethyl hydroquinone, 0.1 to 30.0% by weight of myrcene, 0.1 to 15.0% by weight of eucalyptol and 0.5 to 25.0% by weight of anisic aldehyde can be reproduced in the spatial orientation of the Solanaceae lotus flower community.

In one embodiment of the invention, the perfume composition of the present invention may comprise from 20.0 to 97.0% by weight of isopropyl myristate based on the total weight of the composition. Outside this range, the fragrance similarity is lowered.

In addition, the perfume composition mixed in the above-mentioned range is not limited to this, and can be applied to general daily necessities, cosmetic compositions, perfume compositions, and external composition for skin.

The perfume composition of the present invention can be used as a cosmetic composition for skin, lotion, essence, lotion, gel, nutritional cream, massage cream, hand cream, foot cream, foundation, makeup base, hair cream, hair tonic, hair conditioner, A bath liquid, a liquid cleanser, a soap or a shampoo.

The perfume composition of the present invention may be provided as a perfume composition, such as a perfume, a perfume, a deodorant, a diffuser or an aroma candle.

The perfume composition of the present invention can be provided as an external composition for skin such as ointment, lotion, soluble image, suspension, emulsion, cream, gel, spray, papermaking,

At this time, the compositions may further include colorants, fungicides, preservatives, antioxidants, moisturizers, thickeners, etc., which are generally acceptable for improving the physical properties.

The term "space aroma" as used in the present invention means a scent extracted from a specific area, and simply refers to a scent of the space other than a specific plant scent. In the present invention, a specific region means a Lotus flower community of Solanum.

The term "spatially-oriented component" refers to a component identified as a result of analyzing the components captured in the space. In the present invention, the spatial orientation of the Solanthus grandiflorum community is collected through a dynamic headspace method and analyzed by gas chromatography Which is a part of the space of the Lotus.

In the present invention, the analyzed spatial perfumed components are divided into fragrance components and other components, and spatial fragrance is reproduced using only fragrance components.

Other components include general atmospheric components and allergen components. In the present invention, the term "general atmospheric component" refers to volatile organic chemical components present in the atmosphere as well as specific regions analyzed for spatial incoherence. Specific "general atmospheric components" include toluene, xylene, benzoic acid, and phenol. "Allergen ingredients" are known to have the potential to cause allergic reactions when they enter the body, including limonene, linalool, and benzyl alcohol.

In the present invention, the fragrance component of the Solanthum lotus flower community is selected from the group consisting of dimethyl hydroquinone, myrcene (methylhydroquinone, myrcene, eucalyptol, and anisic aldehyde.

The perfume composition of the present invention has an effect of enhancing the reproducibility of the fragrance and improving the reproducibility of the spatial composition of the Solanthus grandiflorum community by selecting a solvent which improves to have a soft feeling.

In addition, the perfume composition of the present invention has the effect of preventing the allergic reaction and maintaining spatial perfusion by removing allergen components from the spatially-oriented components collected by the dynamic headspace method.

Further, the perfume composition of the present invention has an effect of further improving the preference degree by adjusting the content of the perfume ingredient.

Hereinafter, the present invention will be described in more detail with reference to Examples. It is to be understood, however, that the scope of the present invention is not limited by these examples.

Experimental Example  One. Space incense  Analysis of fragrance components

In the present invention, a dynamic headspace method was used to analyze the spatially-oriented components of the Solanthus sinensis community.

Mini - pump and TENAX filling tube were used for collecting the space - oriented components. The collection tool was installed in the space where the fragrance characteristic of the specific area was best, and the space fragrance was collected in the TENAX filling tube at a flow rate of 1 L / min for more than 3 hours. Gas Chromatography was used to identify the air aroma components in the collected air, and the conditions were as shown in Table 1 below.

GC Model Agilent 6890N Inlet Temp. 250 ℃ Split mode Splitless Cryo-focus Initial -90 ° C Ramp1 90 ° C / min to 180 ° C Final 180 DEG C Column TC-WAX: 60 m-0.25 mm-0.25 m Oven temp. program Initial 40 [deg.] C (0 min) Ramp1 3 ° C / min to 230 ° C Final 30 min Carrier gas flow Helium-1.0 ml / min MSD Model Agilent 5973N Transfer line 280 ℃ Quad 150 ℃ Ion source 230 ℃

As a result of analysis, the spatial flavor components of the Solanthus sinensis community were analyzed as shown in Table 2 below.

Ingredients Content (% by weight) Dimethyl hydroquinone (Dimethyl hydroquinone) 80.878 Myrcene 0.419 Eucalyptol 0.305 Anisic aldehyde 0.473 Other 17.925 total 100

In Table 2, the guitar includes volatile organic chemical components (that is, general atmospheric components) that are generally floating in the air and components that are likely to act as allergens (that is, allergen components). Only the fragrance ingredients were used except for the ingredients. The major fragrance components of the Solanthus sinensis community space except for the other ingredients are dimethylhydroquinone, myrcene, eucalyptol and aniline aldehyde.

Table 3 shows the compositional names of the main general air and allergen components and the respective contents (% by weight with respect to total space-oriented components).

Ingredients Content (% by weight) Classification Benzaldehyde 0.872 General atmospheric composition Phenol 0.631 General atmospheric composition Octanoic acid 0.439 General atmospheric composition Nonanoic acid 2.329 General atmospheric composition 2-Ethylhexyl benzoate 0.485 General atmospheric composition Decanoic acid 0.849 General atmospheric composition Benzoic acid 2.280 General atmospheric composition Limonene 1.026 Allogenic component

Experimental Example  2. Example 1  Lotus Flower Space-oriented Comparative sensory evaluation

Based on the analysis results of Experimental Example 1, Example 1 having the composition shown in the following Table 4 was prepared except for the other ingredients such as allergen, and the similarity between the flavor and the flavor of the natural lotus flower lotus community was verified through sensory evaluation.

Example Dipropylene glycol (DPG) was used as a solvent in the preparation. DPG has a use as a flavoring agent, a solvent and a viscosity reducing agent, and is mainly used as a solvent (solvent) for dissolving various constituents in the production of a perfume composition.

Ingredients Content (% by weight) Dimethylhydroquinone 81.0 Mirsen 0.4 Eucalyptol 0.3 No formaldehyde 0.5 DPG 17.8 total 100

Sensory evaluation was performed on perfume experts composed of irritants. Scoring of the fragrances for the items was scored in the range of -10 (very weak-nonconforming), O (very fit) and +10 (very many-inappropriate). In other words, the closer the score is to zero, the better the local space is.

In order to evaluate the reproducibility with the local space, the degree of sweetness, which is a typical incense type of lotus flower community, was compared. Sweetness is a soft and sweet scent possessed by a typical flower scent. Since the lotus scent also has a sweet scent characteristic of a flower, a sweet scent can be selected as a scent type representing the spatial scent of a lotus flower community .

The diffusiveness is an ability to spread around the perfume and is an item suitable for evaluating the reproducibility specific to the space flavor. The intensity refers to the intensity of the perfume, and is used as a basic sensory evaluation item of the perfume composition .

As a result of the sensory evaluation of Example 1, it was confirmed that the fragrance type was similar to the flavor type in the local space. However, as shown in Table 5 below, the flavor (-5) 5) were evaluated as slightly higher.

In addition, the terpene-based components such as myrcene and eucalyptol among the components of the combined perfume differ in their solubility in solvents depending on the kind and content thereof. In the case of Example 1 using DPG, the solubility problem causes unstable properties And it was judged that it inhibited the diffusibility of the fragrance in the fragrance.

Evaluation items Local space Example 1 Sweetness 0 +2.0 Diffusiveness 0 -5.0 Intensity 0 +5.0

Therefore, based on the results of the sensory evaluation, the content of the fragrance component was adjusted in the direction of enhancing the diffusing property of the fragrance and lowering the sweetness and strength to improve the reproducibility of the spatial fragrance, and to select a suitable solvent for the constituents of the combined fragrance.

Experimental Example  3. Example 2  Lotus Flower Space-oriented Comparative sensory evaluation

As a result of Experimental Example 2, isopropyl myristate was selected as a new solvent capable of improving the diffusing property of fragrance and lowering sweetness and strength.

Example 2 having the composition shown in the following Table 6 was prepared using isopropyl myristate as a solvent and the similarity between the flavor and the flavor of the natural polyunsaturated lotus flower community was verified by sensory evaluation.

Ingredients Content (% by weight) Dimethylhydroquinone 81.0 Mirsen 0.4 Eucalyptol 0.3 No formaldehyde 0.5 Isopropyl myristate 17.8 total 100

The sensory evaluation was carried out in the same manner as in Experimental Example 2, and the evaluation results are shown in Table 7 below.

Evaluation items Local space Example 1 Example 2 Sweetness 0 +2.0 +1.5 Diffusiveness 0 -5.0 -3.5 Intensity 0 +5.0 +4.5

The results of the sensory evaluation of Example 2 were compared with those of Example 1, and it was evaluated that in Example 1, the sweetness and strength of the fragrance were higher and the degree of diffusivity was somewhat lower than that of the local space, Was found to be improved in all of sweetness, diffusibility and strength as compared with Example 1.

Experimental Example  4. Depending on the content of constituents in the fragrance component Example  Manufacturing and sensory evaluation

As can be seen from the results of Table 7, since reproducibility of Example 2 prepared using isopropyl myristate as a solvent was improved as compared with Example 1, a perfume composition was prepared using the solvent as a solvent in the following Examples.

However, since the content ratio between not only the solvent but also the fragrance components is also a main component of the fragrance composition, the sensory evaluation of the combined fragrance is conducted as in the following Examples 3 to 7 in order to obtain the optimum fragrance ingredient content ratio.

The content of the fragrant component analyzed in Experimental Example 1 was adjusted, and the content of each fragrance component in the total weight of the fragrant component was taken as 100 by weight ratio. The specific composition is shown in Table 8 below. For reference, in Example 3, the ratio of the fractions analyzed in Experimental Example 1 was maintained.

Ingredients Example 3 Example 4 Example 5 Example 6 Example 7 Dimethylhydroquinone 98.5 85.0 72.5 52.6 48.3 Mirsen 0.5 5.0 8.0 15.8 23.6 Eucalyptol 0.4 2.0 4.5 10.5 12.3 No formaldehyde 0.6 8.0 15.0 21.1 15.8 Total (% by weight) 100.0 100.0 100.0 100.0 100.0

For the fragrance evaluation of Examples 3 to 7, evaluation was made by a five-point rating method as Strength, Closeness, Diffusiveness and Hedonics as shown in Table 9 below. The evaluation was carried out with perfume experts composed of a perfume maker. The evaluation results are shown in Table 10 below. If each item is more than 2.5 points, it is judged that there is excellence in the item.

Evaluation items score Strength: Is the strength of the fragrance appropriate?
1 2 3 4 5
(Complaint) (fitness) (satisfaction) Reproducibility: Has the spatial orientation been expressed well? Diffusivity: The spread of fragrance is good Preference: Does it feel like a pleasant scent

Subject burglar Reproducibility preference Diffusibility Average Example 3 2.50 2.50 2.50 3.25 2.69 Example 4 2.50 2.75 2.50 3.00 2.69 Example 5 3.25 3.00 3.00 3.50 3.19 Example 6 4.00 4.50 3.00 3.50 3.75 Example 7 4.00 4.25 3.00 3.25 3.63

As a result of the sensory evaluation, it was confirmed that Examples 3 to 7 were excellent in all of the items, and in particular, the taste component ratio of Example 6 was excellent in all items composed of fragrance intensity, reproducibility, The rating was found to be the best.

Experimental Example 5 . The solvent dilution to the fragrance component Example  Manufacturing and sensory evaluation

As can be seen from the results of Table 10, the fragrance composition prepared by the ratio of the fragrance components of Example 6 was the most excellent in all the evaluation items. Therefore, based on the fragrance ingredient ratio as in Example 6, Reproducibility was evaluated.

The effect of the relative proportions of solvents on the fragrance components of the same content ratio as in Example 6 was examined. Isopropyl myristate was used as a solvent.

Target component Example 8 Example 9 Example 10 Example 11 Fragrance component
(Example 6) 80.0 30.0 10.0 3.0 Isopropyl myristate 20.0 70.0 90.0 97.0 Total (% by weight) 100.0 100.0 100.0 100.0

Sensory evaluation was performed on perfume experts composed of irritants. Scoring of the fragrances for the items was scored in the range of -10 (very weak-nonconforming), O (very fit) and +10 (very many-inappropriate). In other words, the closer the score is to zero, the better the local space is.

The sensory evaluation items proceeded with intensity and diffusiveness that seemed to depend on the solvent ratio.

Evaluation items Local space Example 8 Example 9 Example 10 Example 11 Intensity 0 +3.5 +2.0 -0.5 -0.5 Diffusiveness 0 -3.5 -1.0 +1.0 +0.5

As a result of the sensory evaluation, it was confirmed that Examples 8 to 11 were excellent in strength and diffusibility and were suitable for spatial perfection, and the perfume composition of Example 11 showed the most excellent results.

Claims (8)

A perfume composition recreating the spatial flavor of Solanaceae lotus flower community comprising an aroma component of Nelumbo nucifera community as an active ingredient,
The fragrance component comprises 45.0 to 98.5% by weight of dimethyl hydroquinone, 0.1 to 30.0% by weight of myrcene, 0.1 to 15.0% by weight of eucalyptol, From 0.5 to 25.0% by weight of anisic aldehyde,
Wherein the composition comprises isopropyl myristate as a solvent. The fragrance composition recreates the spatial flavor of the Solanthus lotus flower community.
delete delete delete The method according to claim 1,
Wherein the isopropyl myristate is contained in an amount of 20.0 to 97.0% by weight based on the total weight of the composition.
A cosmetic composition comprising the perfume composition of any one of claims 1 to 5.
A perfume composition comprising the perfume composition of any one of claims 1 to 5.
A composition for external application for skin comprising the perfume composition of claim 1 or 5.