KR20150056184A - Perfume composition for expressing the fragrance of Lilium cernuum - Google Patents

Abstract

According to the present invention, a composition includes: benzaldehyde, acetophenone, nonanal, decanal, and eugenol analyzed as the fragrance ingredients of nodding lilies (Lilium cernuum) as well as hydroxycitronellal to implement the unique fragrance of the nodding lilies while having having excellent palatability.

Description

Description of the Related Art [0002] Perfume compositions for expressing fragrance of Lilium cernuum

The present invention relates to a perfume composition having excellent palatability while reproducing the intrinsic fragrance of Lilium cernuum .

Lilium cernuum ( Lilium cernuum) is a perennial bulb that grows north of the north, and is not often found in the vicinity because it is designated as an endangered wild plant due to its low population. The growth environment grows in a place where the sunny or semi-soft water is good. Its height is 70㎝. Leaves are alternate phyllotaxis, 10-15㎝ long, narrow in width, 1-5mm, thin line like pine leaves. Flowers are deep reddish purple, purple spots inside, 2.5 ~ 4.2㎝ in length, and 0.8㎝ in width, with one to four ends running on the end of the main stem and branches. The pistil is out longer than the surgery. The fruit is ripe, flat and brown in September-October. It is used for ornamental purposes, and the stem of the scales is used for food. The shallow and delicate scent of Korean lilies can stimulate the nostalgia of Koreans.

There are many ways to reproduce the fragrance of this lilies. For example, there is a solvent extraction method in which the flavor component of Solanari is converted into an Absolute form by using a solvent and a steam distillation method in which a flavor component is converted into essential oil by a conventional method. However, since the above methods require high heat in the extraction process, the process is complicated and takes a lot of time, so there may be a lot of difference from the original flavor of Solaris. In the case of Solaris, It is difficult to supply enough raw materials.

In recent years, Head Space and Solid Phase Micro Extraction (SPME) methods have been developed to overcome these disadvantages. Of these, the SPME method is disclosed in the paper (SUPELCO international, Vol.13, No.4, p.9-10), which is incorporated herein by reference in its entirety. Unlike the conventional extraction method, the SPME method does not use a solvent and does not require a pretreatment, and can analyze the fragrance ingredient quickly and easily. On the other hand, volatile fragrance components are easy to analyze, but fragrance components with low volatility or high molecular weight have a disadvantage that analysis by this method is not easy.

On the other hand, GC (Gas Chromatography) is widely used for analysis of all fragrance components since it is a useful instrumental analysis for the qualitative and quantitative analysis of volatile substances. However, since the threshold value of the fragrance component is very low, fragrance components that strongly exhibit fragrance even at a low concentration are present, while volatile components that can not express fragrance even at a high concentration due to a very high threshold value exist. Therefore, it can not be said that volatile components, which are mainly found quantitatively through GC, are not necessarily the main flavor components of a specific substance. To solve these problems, a method of GC-O (Gas Chromatography Olfactometry, Guth H, Grosch W (1993) Lebensm Wiss U Technol, 196, 22-28) has been developed and used. CG-O is a method of analyzing a fragrance component through the peak of a chromatogram and identifying the fragrant component which does not appear as a peak but takes on a direct perfume.

Korean Patent Laid-Open Publication No. 2013-0055331

Accordingly, the present inventors analyzed the main components of the scent of Korean lilies using the SPME method, which is effective for analyzing the fragrance of living natural products. However, as a result of the sensory evaluation, the present inventors found that the main component of the analyzed fragrance alone can not reproduce the fragrance of Solanari.

Accordingly, the inventors of the present invention have found that when the hydroxycitronellal is used together with the main ingredients of the fragrance at a certain ratio, the fragrance of the Solari can be reproduced and exhibits excellent palatability, .

Accordingly, an object of the present invention is to provide a perfume composition which can reproduce the intrinsic fragrance of Solanari and has excellent palatability.

Another object of the present invention is to provide a composition for external application for skin containing the above-mentioned perfume composition.

In order to achieve the above object, the present invention provides a perfume composition recreating the fragrance component of a Korean ladle and a scent of a Korean ladle containing hydroxycitronellal as an active ingredient.

The present invention also provides a composition for external application for skin, which comprises a perfume composition recreating the fragrance of the above-mentioned Solanaceae.

The perfume composition according to the present invention can be applied to a variety of perfume compositions such as Benzaldehyde, Acetophenone, Nonanal, Decanal and Eugenol to reproduce the Solari flavor analyzed by SPME By containing hydroxycitronelal as a main component of the Solarius flavor, it is possible to reproduce the scent of Solarius and to improve the palatability of the scent.

The present invention provides a fragrance composition containing a fragrance component of a Korean lilium and a hydroxycitronellal as essential components to reproduce the fragrance of Korean lilium

Hereinafter, the present invention will be described more specifically.

The fragrance composition of the present invention contains a main component and a secondary component as a scent component of Solarius, and the main components thereof are benzaldehyde, acetophenone, noranal, decanal and eugenol. Cis-Linalool oxide, Acetic acid, Nonanoic acid and Phenylacetaldehyde are used as the above-mentioned secondary components.

In addition, the perfume composition of the present invention is characterized in that, to reproduce the intrinsic fragrance of Solanari to enhance similarity of fragrance with Solanari and to exhibit excellent palatability, hydroxycitronelal as an essential ingredient use.

The perfume composition of the present invention comprises 30 to 42% by weight of benzinddehyde, 15 to 26% by weight of acetophenone, 7 to 14% by weight of nornalde, 6 to 12% by weight of decanal, %, And 4 to 9% by weight of eugenol. The total content of the main components may be 75 to 95% by weight, preferably 80 to 90% by weight based on the total weight of the composition.

The perfume composition of the present invention contains the above-mentioned secondary components in an amount of 2 to 5 wt% of cis-linalool oxide, 1.2 to 3 wt% of acetic acid, 1 to 2.5 wt% of nonanoic acid, Acetaldehyde in an amount of 0.2 to 1.8% by weight.

The perfume composition of the present invention contains the hydroxycitronellal in an amount of 1.2 to 5% by weight.

In the present invention, benzaldehyde, acetophenone, nonanal, decanal, eugenol, and hydroxycitronelal, which are main ingredients for reproducing Solanace scent, have a low similarity of flavor with Solarius And the palatability of the fragrance is lowered. However, other secondary components such as cis-linalool oxide, acetic acid, nonanoic acid, phenylacetaldehyde and the like are preferably used within the above-mentioned range. However, as long as they do not affect the reproduction of the Solari flavor, May also be included in an amount outside the range.

The composition according to the present invention, which is mixed in the above-described range, may be formulated into a skin external-use base such as perfume, cosmetics, etc., and the blending amount may be appropriately selected and blended according to the conventional art have.

Such external devices include, but are not limited to, ointments, lotions, soluble images, suspensions, emulsions, creams, gels, sprays, papermaking, Can be incorporated into any given base.

In the present invention, the SPME method is used as a method of analyzing the fragrance component of Solanari. The SPME method is useful for analyzing the fragrance component of Solanaceae because the fractions adsorbed on the fiber can be rapidly desorbed and injected into the GS-MS column without special pretreatment, and the analysis time can be greatly shortened.

In the present invention, based on the fragrance component of Solanari analyzed by the SPME method, a combined fragrance is prepared, and the similarity with the scent of Solari and the taste of the fragrance are performed through the olfactory sensory test. The sensory evaluation was carried out by a professional irrigation and general public. The similarity with the scent of Solari and the preference of the scent were evaluated through questionnaires.

Hereinafter, the present invention will be described in more detail by way of examples, but the present invention is not limited thereto, and other applications, modifications and the like of the present invention will be apparent to those skilled in the art.

[Referential Example 1] Flavor analysis of Solarie using SPME method

A fragrant component was adsorbed on Polyacrylate Fiber (Polyacrylate Fiber) coated with 85 ㎛ of polyacrylate for 2 hours. Collected for 3 hours in Gyeongsangbuk - do province.

After collecting the fragrance components (Sample A), the fiber was sealed, transferred to the inlet of the GC-MS, desorbed for 2 minutes, and subjected to GC-MS analysis. GC-MS analysis conditions are as follows.

Analysis condition

. Analytical instrument: HP 5890 II GC

. Detector: HP 5972 MSD

. Column: DB-1 (60m X 0.25mm X 0.25um) (Agilent)

. Carrier gas: He

. Injection Temperature: 250 ° C

. Detector Temperature: 280 ° C

. Oven Temperature: 70 ° C to 220 ° C (3 ° C / min)

. Ionization Voltage: 70eV

. Removal time: 2 minutes

As a result, the fragrance components of Solanari analyzed by the SPME method are shown in Table 1 below.

Perfume name content(%) Ben saddheid 32.14 Acetophenone 19.48 No day 9.74 Decanal 7.79 Eugenol 5.72 cis-linalool oxide 4.47 Acetic acid 2.79 Nonanoic acid 2.23 Phenylacetaldehyde 1.12 Etc 11.17 Total content 100.0

As shown in Table 1, it can be seen that Solarius contains benzaldehyde, acetophenone, nonanal, decanal and eugenol as main flavor components.

[Test Example 1] Comparative sensory evaluation between the combined fragrance of the analyzed fragrance components and the fragrance of the scorpion

Based on the analyzed results, a combination perfume (Sample B) having the composition shown in the following Table 2 was prepared, and the similarity of the fragrance to the natural black lily was verified through sensory evaluation.

Perfume name content(%) Ben saddheid 32.14 Acetophenone 19.48 No day 9.74 Decanal 7.79 Eugenol 5.72 cis-linalool oxide 4.47 Acetic acid 2.79 Nonanoic acid 2.23 Phenylacetaldehyde 1.12 DPG (solvent) 11.17 Total content 100.0

The sensory evaluation was carried out on 20 normal male and female twenty people aged 20 to 45 years. The sample A of the Solari flowerpot of Reference Example 1 and the sample B of the combined perfume reproduced by the SPME method were respectively handled, (Question 1) and sample palatability (Question 2) of Sample A and Sample B were investigated. The results are shown in Table 4.

survey
(1) Question 1: How similar are samples A and B?
1) It is not at all similar.
2) Not very similar.
3) Just so.
4) Somewhat similar.
5) Very similar.
(2) Question 2: How much do you like the smell of Sample B?
1) Not at all good.
2) Not very good.
3) Just so.
4) Somewhat good.
5) Very good.

Rating agent Question 1 (similarity) Question 2 (palatability) One 3 2 2 2 2 3 2 2 4 4 3 5 3 3 6 3 3 7 2 2 8 3 2 9 2 2 10 One One 11 2 3 12 2 2 13 3 2 14 2 2 15 3 2 16 3 3 17 2 3 18 4 4 19 3 2 20 3 One Average 2.6 2.3

As shown in Table 4, Sample B, which is a combination fragrance, showed a large difference from the floral aroma of the Solari flowerpot, and the palatability was also low.

[Test Example 2] Analysis of fragrance by professional evaluation team and comparison of fragrance with Solari

As shown in Test Example 1, the fragrance composition prepared with the components analyzed by the SPME method had no similarity to saliva.

Thus, a professional evaluation team composed of a steamer performed a sensory evaluation on each of the fragrance components of Solanari. As a result, among the fragrance ingredients of Solanari, benzaldehyde to produce a sweet floral scent, acetophenone to produce a warm floral scent, a flower to produce a floral fruity scent Day after day, five ingredients of eugenol, which produces a decaline and spicy fragrance that produces a fresh citrusy flavor, are found to be the main ingredients of the true flavor of Solanari.

[Example 1] Preparation of new combination fragrance according to changes in contents of main ingredients

From Test Example 2, it was confirmed that benzaldehyde, acetophenone, nonanal, decanal, and eugenol were the main components of the original scent of Solarius. Therefore, the present inventors made the new combination fragrances of the following # 1 to # 4 in order to produce the fragrance with good taste while showing the fragrance of the lupine containing these five ingredients.

Combination fragrances # 1 to # 4 were prepared by varying the content of the five fragrances to 60 to 90% by weight while maintaining the ratio of the five fractions. The specific composition is shown in Table 5 below.

Combination number #One #2 # 3 #4 Perfume name (content:% by weight) 60% 70% 80% 90% Ben saddheid 25.8 30.0 34.4 38.6 Acetophenone 15.6 18.2 20.8 23.4 No day 7.8 9.1 10.4 11.7 Decanal 6.2 7.3 8.3 9.4 Eugenol 4.6 5.4 6.1 6.9 Linalool oxide 16.9 12.6 8.4 4.2 Acetic acid 10.5 7.9 5.3 2.6 Nonanoic acid 8.4 6.3 4.2 2.1 Phenylacetaldehyde 4.2 3.2 2.1 1.1 Total content 100.0 100.0 100.0 100.0

[Test Example 3] The sensory evaluation of the flavors prepared in Example 1

The similarity and palatability of the freshly combined fragrance to the scent of Solari were evaluated by the same method as in Test Example 1 above. On the other hand, after performing the comparative sensory evaluation on the two combined flavorings, a resting time of 5 minutes was given to prevent the post sensory paralysis phenomenon. The sensory evaluation results of the perfume similarity and palatability of the new combination fragrance and Solarius are shown in Table 6 below.

evaluation
agent Question 1 (similarity) Question 2 (palatability) Combination Spice Number Combination Spice Number #One #2 # 3 #4 #One #2 # 3 #4 One 1.0 2.0 3.0 4.0 1.0 2.0 2.0 3.0 2 2.0 2.0 3.0 3.0 2.0 3.0 3.0 4.0 3 1.0 2.0 3.0 4.0 3.0 3.0 3.0 4.0 4 1.0 3.0 3.0 3.0 2.0 2.0 3.0 3.0 5 3.0 3.0 3.0 3.0 2.0 3.0 3.0 4.0 6 3.0 3.0 3.0 3.0 2.0 2.0 2.0 3.0 7 2.0 3.0 3.0 4.0 3.0 3.0 3.0 4.0 8 2.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 9 2.0 3.0 3.0 4.0 2.0 3.0 3.0 3.0 10 2.0 2.0 3.0 3.0 1.0 2.0 2.0 3.0 11 2.0 2.0 3.0 4.0 2.0 3.0 3.0 4.0 12 1.0 3.0 3.0 3.0 2.0 2.0 4.0 3.0 13 2.0 2.0 3.0 4.0 2.0 3.0 3.0 4.0 14 2.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 15 1.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 16 2.0 2.0 2.0 4.0 2.0 2.0 4.0 3.0 17 1.0 2.0 2.0 3.0 3.0 3.0 3.0 4.0 18 1.0 1.0 1.0 2.0 1.0 2.0 2.0 3.0 19 3.0 3.0 3.0 3.0 2.0 3.0 3.0 4.0 20 1.0 3.0 3.0 3.0 2.0 2.0 2.0 4.0 Average 1.75 2.5 2.8 3.3 2.15 2.6 2.85 3.45

As shown in Table 6, Sample # 4 having the total content of the five major components of 90% by weight was shown to have the highest similarity and palatability among the four combined flavors, but both of the similarity and palatability were not satisfied appear.

[Example 2] Preparation of flavor improving fragrance by analysis of a professional evaluation unit

In order to improve the similarity and palatability of the fragrance of sample # 4 in which the flavor of Solari was most similar in Table 6, benzaldehyde, acetophenone, nonanal, decanal and eugenol were dissolved in 90 % ≪ / RTI > by weight of the composition, and the hydroxycitronelal is used to make a perfume unique to the reproduction of the perfume of the perfume. At this time, the hydroxycitronelal was added in an amount of 0.9 wt%, 1.5 wt%, 2.1 wt%, 2.7 wt%, 3.3 wt% and 3.9 wt%, 4.5 wt%. The content of hydroxy citronellal was determined based on the judgment of the specialist group. The composition of these recombinant perfumes is shown in Table 7 below.

Combination number
Perfume name (content:% by weight) # # I # All # La #Me # Bar # Company Ben saddheid 38.6 38.6 38.6 38.6 38.6 38.6 38.6 Acetophenone 23.4 23.4 23.4 23.4 23.4 23.4 23.4 No day 11.7 11.7 11.7 11.7 11.7 11.7 11.7 Decanal 9.4 9.4 9.4 9.4 9.4 9.4 9.4 Eugenol 6.9 6.9 6.9 6.9 6.9 6.9 6.9 Linalool oxide 3.8 3.5 3.3 3.1 2.8 2.6 2.6 Acetic acid 2.4 2.3 2.1 1.9 1.8 1.6 1.4 Nonanoic acid 1.9 1.8 1.7 1.6 1.5 1.4 1.3 Phenylacetaldehyde 1.0 0.9 0.8 0.7 0.6 0.5 0.4 Hydroxycitronellal 0.9 1.5 2.1 2.7 3.3 3.9 4.5 Total content 100.0 100.0 100.0 100.0 100.0 100.0 100.0

[Test Example 4] Sensory evaluation of the combined flavorings prepared in Example 2

The flavor similarity and taste peculiarity of the combination of # and #, #, #, #, #, and # combined flavors to the cucumber and melon flavor combined in Example 2 were measured in the same manner as in Test Example 1 And the sensory evaluation was carried out. After performing a comparative sensory evaluation on the two combined flavorings, a resting time of 5 minutes was given to prevent posterior sensory paralysis. The results are shown in Table 8 below, in terms of the fragrance similarity and flavor preference with the new combination fragrance and the lily of the valley.

Rating agent Question 1 (similarity) Question 2 (palatability) Combination Spice Number Combination Spice Number #end #I #All #la #hemp #bar #four #end #I #All #la #hemp #bar #four One 3.0 4.0 4.0 4.0 3.0 3.0 3.0 2.0 3.0 3.0 4.0 5.0 4.0 2.0 2 2.0 4.0 4.0 5.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 4.0 4.0 3.0 3 3.0 3.0 3.0 4.0 4.0 4.0 3.0 3.0 4.0 4.0 4.0 5.0 4.0 2.0 4 3.0 3.0 3.0 4.0 4.0 3.0 3.0 3.0 3.0 3.0 4.0 4.0 3.0 3.0 5 4.0 4.0 4.0 5.0 4.0 4.0 4.0 3.0 3.0 3.0 4.0 4.0 3.0 3.0 6 3.0 3.0 3.0 4.0 3.0 3.0 3.0 4.0 4.0 4.0 3.0 3.0 4.0 3.0 7 3.0 3.0 4.0 3.0 5.0 4.0 4.0 3.0 3.0 4.0 3.0 4.0 5.0 3.0 8 3.0 4.0 4.0 4.0 4.0 3.0 3.0 3.0 4.0 3.0 4.0 4.0 3.0 3.0 9 2.0 2.0 3.0 3.0 4.0 4.0 3.0 2.0 3.0 3.0 3.0 4.0 4.0 2.0 10 3.0 3.0 3.0 4.0 4.0 4.0 3.0 3.0 4.0 3.0 4.0 5.0 4.0 3.0 11 2.0 4.0 4.0 4.0 4.0 5.0 4.0 2.0 3.0 4.0 3.0 4.0 3.0 3.0 12 3.0 3.0 4.0 4.0 5.0 4.0 3.0 4.0 3.0 4.0 4.0 5.0 4.0 2.0 13 2.0 4.0 4.0 4.0 5.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 3.0 2.0 14 3.0 3.0 3.0 5.0 5.0 4.0 3.0 3.0 3.0 4.0 5.0 5.0 4.0 4.0 15 4.0 3.0 3.0 3.0 4.0 4.0 3.0 3.0 4.0 3.0 4.0 4.0 3.0 3.0 16 3.0 4.0 4.0 4.0 4.0 5.0 3.0 3.0 3.0 3.0 3.0 4.0 4.0 4.0 17 2.0 3.0 3.0 4.0 5.0 4.0 2.0 2.0 3.0 4.0 5.0 4.0 3.0 4.0 18 4.0 3.0 4.0 4.0 4.0 5.0 3.0 3.0 4.0 3.0 4.0 4.0 3.0 3.0 19 3.0 3.0 3.0 3.0 4.0 4.0 3.0 3.0 4.0 4.0 4.0 4.0 3.0 3.0 20 2.0 3.0 4.0 4.0 5.0 4.0 3.0 3.0 3.0 3.0 3.0 4.0 3.0 3.0 Average 2.85 3.3 3.55 3.95 4.15 3.85 3.1 2.9 3.35 3.4 3.7 4.15 3.55 2.9

As shown in Table 8, when the content of hydroxycitronelal is from 1.5 to 3.9% by weight in the main flavor component of Benaluddehyde, Acetophenone, Noonnal, Decanal and Eugenol, , And it was confirmed that the palatability was high (average 2.7 or more). In particular, when the content of hydroxycitronelal was in the range of 2.7 to 3.9% by weight, it was found that the perfume similarity and flavor preference with Solari were excellent (average 3.3 or more).

On the other hand, when the hydroxycitronelal is contained in an amount of less than 1.5 wt% or more than 3.9 wt%, the similarity and palatability of the fragrance are lowered.

[Example 3] Preparation of combination fragrance

Combination fragrances of #A, #, #, and #CAR were prepared according to the composition of Table 9 below. The combination fragrances of # ah, # ja, # tea, and # ka were prepared by mixing the contents of the main ingredients benzaldehyde, acetophenone, nonanal, decanal, and eugenol in # 2, #, # Bars, respectively, but having a composition in which the content of the secondary components cis-linalool oxide, acetic acid, nonanoic acid and phenylacetaldehyde are changed differently.

Combination number
Perfume name (content:% by weight) # Ah # Now # Car # Car Ben saddheid 38.6 38.6 38.6 38.6 Acetophenone 23.4 23.4 23.4 23.4 No day 11.7 11.7 11.7 11.7 Decanal 9.4 9.4 9.4 9.4 Eugenol 6.9 6.9 6.9 6.9 Linalool oxide 0 2.8 2.8 2.8 Acetic acid 1.8 0 1.8 1.8 Nonanoic acid 1.5 1.5 0 1.5 Phenylacetaldehyde 0.6 0.6 0.6 0 Hydroxycitronellal 3.3 3.3 3.3 3.3 DPG 2.8 1.8 1.5 0.6 Total content 100.0 100.0 100.0 100.0

[Test Example 5] Sensory evaluation of the combined flavorings prepared in Example 2

For the combination fragrances of #A, #B, #C, and #C combined in Example 3, sensory similarity with the cicadas and taste of the scent was evaluated by the same method as in Test Example 1 above. On the other hand, after performing the comparative sensory evaluation on the two combined flavorings, a resting time of 5 minutes was given to prevent the posterior sensory paralysis phenomenon. The sensory evaluation results on the fragrance similarity and the taste palatability of the new combination fragrance and the Korean lemon scent are shown in Table 10 below.

Rating agent Question 1 (similarity) Question 2 (palatability) Combination Spice Number Combination Spice Number # Ah # Now # Car # Car # Ah # Now # Car # Car One 4.0 4.0 3.0 4.0 3.0 3.0 4.0 5.0 2 3.0 3.0 3.0 5.0 4.0 4.0 4.0 4.0 3 4.0 4.0 4.0 4.0 4.0 4.0 4.0 5.0 4 4.0 3.0 3.0 4.0 4.0 4.0 4.0 4.0 5 4.0 4.0 4.0 5.0 4.0 4.0 4.0 4.0 6 3.0 3.0 3.0 4.0 3.0 3.0 3.0 3.0 7 3.0 4.0 4.0 3.0 4.0 4.0 4.0 5.0 8 4.0 3.0 3.0 4.0 4.0 4.0 3.0 4.0 9 3.0 4.0 4.0 3.0 3.0 3.0 4.0 4.0 10 4.0 4.0 4.0 4.0 4.0 4.0 4.0 3.0 11 3.0 5.0 5.0 4.0 4.0 4.0 4.0 4.0 12 4.0 4.0 4.0 4.0 4.0 4.0 5.0 5.0 13 3.0 3.0 3.0 4.0 3.0 3.0 3.0 3.0 14 5.0 3.0 4.0 5.0 4.0 4.0 5.0 5.0 15 4.0 4.0 4.0 3.0 3.0 4.0 4.0 4.0 16 3.0 5.0 5.0 4.0 4.0 4.0 4.0 4.0 17 5.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0 18 4.0 5.0 5.0 4.0 4.0 4.0 3.0 4.0 19 4.0 4.0 4.0 3.0 4.0 4.0 4.0 4.0 20 3.0 3.0 4.0 4.0 3.0 4.0 4.0 5.0 Average 3.7 3.8 3.85 3.95 3.7 3.8 3.9 4.15

As shown in Table 10, even if the contents of cis-linalool oxide, acetic acid, nonanoic acid and phenylacetaldehyde were varied, the major components, benzindehydro, acetophenone, It can be confirmed that when the content of the eugenol and the hydroxycitronellal is within the range of the present invention, the flavor similarity and palatability are not greatly affected.

[Production Example 1]

A perfume composition having similarity to the scent of Korean lilies as described above was blended to prepare the perfume of Table 11 below.

Perfume containing fragrance compositions recreating the fragrance of lilies Renaissance fragrance reproduction combination fragrance
Alcohol
water
Pigment
Sunscreen 15 wt%
83 wt%
2 wt%
Suitable amount
Suitable amount

Claims (10)

A fragrance composition containing a scent component of Solanari and hydroxycitronellal as an active ingredient to reproduce the fragrance of Solanari. The method according to claim 1, characterized in that the major component of the flavor component of the Solarius is comprised of benzaldehyde, acetophenone, nonanal, decanal and eugenol ≪ / RTI > The composition of claim 2, wherein the composition is selected from the group consisting of cis-linalool oxide, acetic acid, nonanoic acid, and phenylacetaldehyde And further contains at least one kind of a perfume composition. The perfume composition according to claim 2, wherein the perfume composition comprises 30 to 42% by weight of benzaldehyde, 15 to 26% by weight of acetophenone, 7 to 14% by weight of nonanal, , Decanal in an amount of 6 to 12 wt%, eugenol in an amount of 4 to 9 wt%, and hydroxycitronellal in an amount of 1.2 to 5 wt% Perfume composition. The perfume composition according to claim 2, wherein the perfume composition contains 75 to 95% by weight of the main component and 1.2 to 5% by weight of hydroxycitronelal, based on the total weight of the composition. The perfume composition according to claim 3, wherein cis-linalool oxide is contained in an amount of 2 to 5% by weight based on the total weight of the composition. The perfume composition according to claim 3, wherein acetic acid is contained in an amount of 1.2 to 3% by weight based on the total weight of the composition. The perfume composition according to claim 3, wherein the nonanoic acid is contained in an amount of 1 to 2.5% by weight based on the total weight of the composition. The perfume composition according to claim 3, which comprises phenylacetaldehyde in an amount of 0.2 to 1.8% by weight based on the total weight of the composition. 10. A composition for external application for skin containing the perfume composition according to any one of claims 1 to 9.