KR101843172B1 - Perfume composition for expressing the fragrance of nelumbo nucifera plantation in haman - Google Patents

Abstract

The present invention relates to a perfume composition recreating the spatial flavor of the hanam lotus flower community. The perfume composition reproduces the spatial flavor of the hanan lotus flower community by extracting the optimum content based on the intrinsic fragrance component of the hanan lotus flower community, The present invention relates to a perfume composition having palatability.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a perfume composition recreating a space of a hanam lotus flower community,

The present invention relates to a fragrance composition recreating the spatial flavor of the hanthan lotus flower community. It is based on the intrinsic fragrance component of the hanthan lotus flower community, ≪ / RTI >

The desire to spend the time of healing in the nature leaving the everyday space to the modern people living busy life is getting bigger, but there are many modern people who do not even have enough time to leave the forest and leave for the forest. The present inventors have conceived the present invention to provide a method of easily healing time within a short time by providing a space-recreating perfume composition that appears to be in a real forest.

The present inventors have selected a hanam lotus flower community as a region having a Korean beauty and healing sensation, and perfume composition which gives an image of space and a distinctive feeling by inventing a fragrance composition recreating the spatial fragrance of this region.

The Hamanan Lotus Flower Community is the only place in the country where you can see the Ara Hongryn. The Nelumbo nucifera Gaertner is a flower that has germinated over 700 years from Yan, who was excavated from Sungsan Mountain in Haman, Gyeongsangnam-do. It is also called Haman Lotus. It is believed that ara-hwilin retains its shape before being divided into various lotus flowers and will be useful for studying lotus system.

Ara Hongryn is a long, petal-purple flower with a long petal that can be seen in the feuds of the Goryeo Dynasty. Each time the petal is rolled up, its color gradually becomes thinner, and later it is characterized by a dark red color remaining only at the end of the petal. The pure white color of the petal roots gradually fills the petals, and the long, elegant shape of the long petals is proud of its unrivaled shape.

On the other hand, there are various methods for reproducing the spatial incense. For example, a solvent extraction method in which a plant in the space is collected by a commonly used method to make a fragrance ingredient into an absolute form, and a steam distillation method in which a fragrance ingredient is made into an essential oil. However, the above methods require high heat in the extraction process, or the process is complicated and takes a lot of time, which may be different from the original flavor. In addition, it does not meet the object of the present invention because it reproduces the fragrance of the plant rather than reproducing the perfume of the space itself.

In the present invention, the dynamic headspace method used for analyzing the spatial fragrance component does not require a solvent and does not require a pretreatment step, so that the fragrance component in the actual space can be directly analyzed.

The dynamic headspace method is a method of circulating air through a resin for a predetermined period of time by using a collection device equipped with a resin capable of adsorbing fragrance to an air pump, analyzing components adsorbed on the resin, The fragrance ingredients contained in a trace amount can be measured.

In addition to various fragrance and flavor components such as terpene, phenol, ketone, and ester, the analyzed aroma components include volatile organic chemical components generally present in the air and allergen components that can cause an allergic reaction. Ingredients such as limonene, hexyl cinnamic acid, linalool, benzyl alcohol, geraniol and the like are fragrance ingredients and can induce allergy. When these ingredients are incorporated into the perfume composition as they are, they may cause problems such as allergic reaction.

The present inventors analyzed the spatial flavor components of the Haman lotus flower community harvested through the dynamic head space method, and then, based on the other flavor components except for the general atmospheric component and the allogenic component, the flavor composition of the Haman lotus flower community .

Further, the inventors of the present invention have perfected the fragrance composition having excellent taste and purity by reproducing the spatial flavor of the hanam lotus flower community by adjusting the content of the fragrance ingredient and using a suitable solvent.

Accordingly, a problem to be solved by the present invention is to provide a fragrance composition recreating the spatial flavor of the hanam lotus flower community.

Another object to be solved by the present invention is to provide a fragrance composition that reproduces the spatial flavor of the hanam lotus flower community that does not cause an allergic reaction by excluding the allergen components from the components collected by the dynamic headspace method.

Another object to be solved by the present invention is to provide a fragrance composition that reproduces the spatial flavor of the hanam lotus flower community and has a high degree of preference by selecting a suitable solvent and adjusting the content of the fragrance ingredient.

Another object of the present invention is to provide a cosmetic composition comprising the perfume composition.

Another object of the present invention is to provide a perfume composition comprising the perfume composition.

Another object to be solved by the present invention is to provide a composition for external application for skin comprising the perfume composition.

In order to solve the above-mentioned problems, the present invention provides a perfume composition recreating the spatial flavor of the Hama lotus flower community containing the fragrance component of the Hama lotus flower community as an active ingredient.

The above-mentioned fragrance components are allergy components other than the allergen component of the space-oriented component of the Haman lotus flower community, and more specifically, alpha-pinene, beta-pinene, dimethyl hydroquinone and aniline aldehyde anisic aldehyde).

The present invention provides a fragrance composition that reproduces the spatial indices of the hanam lotus flower community improved by using isopropyl myristate as a solvent to improve the reproducibility of fragrance and to have a soft feeling.

In one embodiment of the invention, the perfume composition of the present invention comprises 0.5 to 30.0% by weight of alpha-pinene, 0.5 to 30.0% by weight of beta-pinene, 0.1 to 10.0% by weight of dimethylhydroquinone, and 0.1 to 20.0% And it is possible to reproduce the spatial orientation of the hanam lotus flower community. Outside this range, the fragrance similarity is lowered. Preferably 0.5 to 10.0 wt.% Of alpha-pinene, 0.5 to 10.0 wt.% Of beta-pinene, 0.1 to 5.0 wt.% Of dimethylhydroquinone and 0.1 to 7.0 wt.% Of aniline aldehyde, have.

In one embodiment of the present invention, the perfume composition of the present invention may contain 10.0 to 98.0% by weight of isopropyl myristate based on the total weight of the composition. Preferably 60.0 to 98.0% by weight of isopropyl myristate.

In addition, the perfume composition mixed in the above-mentioned range is not limited thereto, and can be applied to general household products, cosmetic composition, perfume composition, composition for external application for skin and composition for oral cavity.

The perfume composition of the present invention can be used as a cosmetic composition for skin, lotion, essence, lotion, gel, nutritional cream, massage cream, hand cream, foot cream, foundation, makeup base, hair cream, hair tonic, hair conditioner, A bath liquid, a liquid cleanser, a soap or a shampoo.

The perfume composition of the present invention may be provided as a perfume composition, such as a perfume, a perfume, a deodorant, a diffuser or an aroma candle.

The perfume composition of the present invention can be provided as an external composition for skin such as ointment, lotion, soluble image, suspension, emulsion, cream, gel, spray, papermaking,

The perfume composition of the present invention may be provided as an oral composition such as a wax solution, a toothpaste, a dental floss, an oral spray, a mouthwash, a mouthwash for oral hygiene, and the like.

At this time, the compositions may further include colorants, fungicides, preservatives, antioxidants, moisturizers, thickeners, etc., which are generally acceptable for improving the physical properties. It is also possible to substitute some of the fragrance ingredients and the additional ingredients for oral use when they are provided in an oral composition.

The term "space aroma" as used in the present invention means a scent extracted from a specific area, and simply refers to a scent of the space other than a specific plant scent. In the present invention, a specific area means a hanam lotus flower community.

The term "spatially-oriented component" means a component identified as a result of analyzing the components captured in the space. In the present invention, the spatial orientation of the Hamaan lotus flower community is collected through a dynamic headspace method and analyzed by gas chromatography This means the spatial fragrance component of the hanam lotus flower community space.

In the present invention, the analyzed spatial perfumed components are divided into fragrance components and other components, and spatial fragrance is reproduced using only fragrance components.

Other components include general atmospheric components and allergen components. In the present invention, the term "general atmospheric component" refers to volatile organic chemical components present in the atmosphere as well as specific regions analyzed for spatial incoherence. Specific "general atmospheric components" include benzaldehyde, acetophenone, octanoic acid, nonanoic acid, and decanoic acid. "Allergen ingredients" are known to have the potential to cause allergic reactions when they enter the body, and include limonene, α-isomethyl ionone, and benzyl alcohol.

The "fragrance component" is a component excluding the "general atmospheric component" and "allergen component" among the spatial fragrance components of the specific region analyzed. In the present invention, the fragrance components of the Hama lotus flower community are alpha-pinene, beta- And an alicyclic aldehyde.

The perfume composition of the present invention has an effect of enhancing the reproducibility of the fragrance and enhancing the reproducibility of spatial orientation of the hanam lotus flower community by selecting a solvent which improves to have a soft feeling.

In addition, the perfume composition of the present invention has the effect of preventing the allergic reaction and maintaining spatial perfusion by removing allergen components from the spatially-oriented components collected by the dynamic headspace method.

Further, the perfume composition of the present invention has an effect of further improving the preference degree by adjusting the content of the perfume ingredient.

Hereinafter, the present invention will be described in more detail with reference to Examples. It is to be understood, however, that the scope of the present invention is not limited by these examples.

EXPERIMENTAL EXAMPLE 1 Analysis of Spice Odor Scent Components

In the present invention, a dynamic headspace method was used to analyze the spatially-oriented components of the Haman Lotus Collection.

Mini - pump and TENAX filling tube were used for collecting the space - oriented components. The collection tool was installed in the space where the fragrance characteristic of the specific area was best, and the space fragrance was collected in the TENAX filling tube at a flow rate of 1 L / min for more than 3 hours. Gas chromatography was used to identify the spatial fragrance components in the collected air, and the conditions were as shown in Table 1 below.

GC Model Agilent 6890N Inlet Temp. 250 Split mode Splitless Cryo-focus Initial -90 Ramp1 90 / min to 180 DEG C Final 180 Column TC-WAX: 60 m-0.25 mm-0.25 m Oven temp. program Initial 40 (0 min) Ramp1 3 / min to 230 ° C Final 30 min Carrier gas flow Helium-1.0 ml / min MSD Model Agilent 5973N Transfer line 280 Quad 150 Ion source 230

As a result, the spatial fragrance components of the hanan lotus flower community were analyzed as shown in Table 2 below.

Ingredients Content (% by weight) Alpha-pinene < / RTI > 1.423 Beta-pinene < / RTI > 1.478 Dimethyl hydroquinone 0.424 Anisic aldehyde 0.702 Other 95.973 total 100,000

In Table 2, the guitar includes volatile organic chemical components (that is, general atmospheric components) that are generally floating in the air and components that are likely to act as allergens (that is, allergen components). Only the fragrance ingredients were used except for the ingredients. The main fragrance components of the hanthanum flower community area except for the other ingredients are alpha - pinene, beta - pinene, dimethylhydroquinone, and anhydro aldehyde.

Table 3 shows the compositional names of the main general air and allergen components and the respective contents (% by weight with respect to total space-oriented components).

Ingredients Content (% by weight) Classification Toluene 5.591 General atmospheric composition Nonanal 8.532 General atmospheric composition Benzaldehyde < / RTI > 10.409 General atmospheric composition Acetophenone 9.125 General atmospheric composition Benzoic acid 28.097 General atmospheric composition Limonene 0.404 Allogenic component Linalool 0.062 Allogenic component Benzyl alcohol 0.376 Allogenic component

Experimental Example 2. Preparation and Sensory Evaluation of Examples According to the Results of Analysis

Based on the results of the analysis of Experimental Example 1, Examples 1 and 2 having the compositions shown in Table 4 were prepared except for the other ingredients such as allergen and the similarity between the flavor and the natural flavor of the lotus flower community was verified through sensory evaluation.

Dipropylene glycol (DPG) and isopropyl myristate were used as solvents in the preparation of the examples. Dipropylene glycol is used as a flavoring agent, a solvent and a viscosity reducing agent, and isopropyl myristate has good skin absorbency and is mainly used as a cosmetic or dermatological solvent. In addition, both of these solvents are generally used as a solvent (solvent) for dissolving various constituents in the production of a perfume composition.

Ingredients Content (% by weight) Example 1 Example 2 Alpha-pinen 1.5 1.5 Beta-pinen 1.5 1.5 Dimethylhydroquinone 0.5 0.5 No formaldehyde 0.7 0.7 Dipropylene glycol 95.8 - Isopropyl myristate - 95.8 total 100.0 100.0

Sensory evaluation was carried out on perfume experts composed of irritants. The fragrance suitability of the items was evaluated as -10 (very weak - unsuitable), -5 (slightly weak - fit), 0 (very fit) High-fit), and +10 (high-to-poor) scores. In other words, the closer the score is to zero, the better the local space is.

The diffusiveness and intensity were compared to assess reproducibility with local spatial orientation. The diffusiveness refers to the ability of the fragrance to spread around, and the intensity refers to the intensity of the fragrance. Since it is a basic sensory evaluation item of the fragrance composition, it is an item suitable for evaluating the reproducibility specific to the spatial fragrance.

The sensory evaluation results of Examples 1 and 2 for the above items are shown in Table 5 below.

Evaluation items Local space Example 1 Example 2 Diffusiveness 0 -5.0 -3.0 Intensity 0 -3.0 -2.0

As a result of the sensory evaluation of the above Examples 1 and 2, it was confirmed that both of the examples were less than ± 5.0 points and were similar to the fragrance type in the local space. The composition of Example 1 was slightly less diffusive (-5.0), less intense (-3.0), and more diffusive (-3.0) and less intense (-2.0 ) Were evaluated as similar to the local space.

Therefore, based on the sensory evaluation results, in order to further improve the reproducibility with respect to the local flavor, the content of the total components including a suitable solvent was adjusted to find an optimal combination flavor.

Experimental Example 3. Preparation and Sensory Evaluation of Examples according to Content Changes

As can be seen from the results in Table 5, since the reproducibility of the perfume composition prepared using isopropyl myristate as a solvent was excellent, the perfume composition was prepared using the solvent in the following Examples.

The new combination fragrances of Examples 3 to 8 were prepared by varying the content of the fragrance ingredients. The specific composition is shown in Table 6 below.

Ingredients Example 2 Example 3 Example 4 Example 5 Example 6 Example 7 Example 8 Alpha-pinen 1.5 1.0 0.5 4.5 6.0 15 30 Beta-pinen 1.5 1.0 0.5 4.5 6.0 15 30 Dimethylhydroquinone 0.5 0.3 1.0 1.5 0.1 5 10 No formaldehyde 0.7 0.4 1.5 2.0 0.1 7.5 20 Isopropyl myristate 95.8 97.3 97.3 87.5 87.8 57.5 10 total 100.0 100.0 100.0 100.0 100.0 100.0 100.0

For the fragrance evaluation of Examples 2 to 8, evaluation was made by the five-point rating method as Strength, Closeness, Diffusiveness and Hedonics as shown in Table 7 below. The evaluation was carried out on perfume experts composed of a perfume maker. The evaluation results are shown in Table 8 below. If each item is more than 2.5 points, it is judged that there is excellence in the item.

Evaluation items score Strength: Is the strength of the fragrance appropriate?
1 2 3 4 5
(Complaint) (fitness) (satisfaction) Reproducibility: Has the spatial orientation been expressed well? Diffusivity: The spread of fragrance is good Preference: Does it feel like a pleasant scent

Subject burglar Reproducibility preference Diffusibility Average Example 2 4.00 4.00 3.75 4.25 4.00 Example 3 4.50 4.25 4.50 4.50 4.44 Example 4 3.75 3.75 3.75 4.00 3.81 Example 5 3.50 4.00 3.50 3.75 3.69 Example 6 3.25 3.50 3.00 3.00 3.19 Example 7 3.25 3.00 2.75 3.00 3.00 Example 8 3.00 2.75 2.75 3.25 2.94

As a result of the sensory evaluation, all of Examples 2 to 8 were found to have a score of 2.5 or more, and that the items had excellence. In particular, the perfume composition of Example 3 was found to be excellent in strength, reproducibility, preference and diffusibility of fragrance.

Claims (7)

The composition according to the present invention may further comprise 0.5 to 30.0% by weight of alpha-pinene, 0.5 to 30.0% by weight of beta-pinene, 0.1 to 10.0% by weight of dimethyl hydroquinone and an anisic aldehyde ( Nelumbo Nucifera ) containing 0.1 to 20.0% by weight of aldehyde.
delete The method according to claim 1,
Wherein the composition comprises isopropyl myristate as a solvent. ≪ RTI ID = 0.0 > 21. < / RTI >
The method of claim 3,
Wherein the isopropyl myristate is contained in an amount of 10.0 to 98.0% by weight based on the total weight of the composition.
A cosmetic composition comprising the perfume composition according to any one of claims 1, 3 or 4.
A perfume composition comprising the perfume composition of any one of claims 1, 3 or 4.
A composition for external application for skin comprising the perfume composition according to any one of claims 1, 3 and 4.