KR101729869B1 - 알데하이드화합물의 정제방법 - Google Patents

알데하이드화합물의 정제방법 Download PDF

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KR101729869B1
KR101729869B1 KR1020157008055A KR20157008055A KR101729869B1 KR 101729869 B1 KR101729869 B1 KR 101729869B1 KR 1020157008055 A KR1020157008055 A KR 1020157008055A KR 20157008055 A KR20157008055 A KR 20157008055A KR 101729869 B1 KR101729869 B1 KR 101729869B1
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compound
group
aldehyde
general formula
formula
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KR20150047611A (ko
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나오유키 카키누마
마사유키 후루야
미치하루 사카타
코이치 토쿠나가
시게토시 쿠마
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미쓰이 가가쿠 가부시키가이샤
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J25/00—Catalysts of the Raney type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/16—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of a saturated carbon skeleton containing rings other than six-membered aromatic rings
    • C07C211/19—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of a saturated carbon skeleton containing rings other than six-membered aromatic rings containing condensed ring systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/45—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C255/47—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of rings being part of condensed ring systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C265/00—Derivatives of isocyanic acid
    • C07C265/14—Derivatives of isocyanic acid containing at least two isocyanate groups bound to the same carbon skeleton
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/821—Ruthenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/822—Rhodium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/842—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/845—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185—Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/36—Systems containing two condensed rings the rings having more than two atoms in common
    • C07C2602/42—Systems containing two condensed rings the rings having more than two atoms in common the bicyclo ring system containing seven carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
KR1020157008055A 2012-11-09 2013-11-08 알데하이드화합물의 정제방법 Active KR101729869B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2012247464 2012-11-09
JPJP-P-2012-247464 2012-11-09
PCT/JP2013/080315 WO2014073663A1 (ja) 2012-11-09 2013-11-08 アルデヒド化合物の精製方法

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KR20150047611A KR20150047611A (ko) 2015-05-04
KR101729869B1 true KR101729869B1 (ko) 2017-04-24

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KR1020157008055A Active KR101729869B1 (ko) 2012-11-09 2013-11-08 알데하이드화합물의 정제방법

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US (3) US9809533B2 (https=)
EP (1) EP2918577B1 (https=)
JP (1) JP5583879B1 (https=)
KR (1) KR101729869B1 (https=)
CN (1) CN104768924B (https=)
IN (1) IN2015DN02806A (https=)
WO (1) WO2014073663A1 (https=)

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CN114181077B (zh) * 2021-12-20 2024-02-27 风火轮(上海)生物科技有限公司 一种合成氨甲环酸的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
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US3143570A (en) 1960-07-01 1964-08-04 Eastman Kodak Co Method for preparing alicyclic diamines
DE3119819A1 (de) * 1981-05-19 1982-12-16 Hoechst Ag, 6000 Frankfurt "verfahren zur herstellung von formylcyannorbornan"
JPS6072844A (ja) 1983-09-29 1985-04-24 Mitsubishi Petrochem Co Ltd 極性官能基含有ホルミルノルボルナンの製造方法
US4649214A (en) * 1984-11-30 1987-03-10 Henkel Corporation 5(6)-hydroxymethyl-norbornane-2-carboxylic acid esters and polyurethanes prepared therefrom
JP2764081B2 (ja) * 1990-01-23 1998-06-11 三井化学株式会社 脂環式―脂肪族ジイソシアナートの製造方法
US5360938A (en) * 1991-08-21 1994-11-01 Union Carbide Chemicals & Plastics Technology Corporation Asymmetric syntheses
DE4220267A1 (de) 1992-06-20 1993-12-23 Hoechst Ag 3,4-Dimethyl-2,5,6-tris(p-sulfonatophenyl)-1-phosphanor-bornadien, Verfahren zu seiner Herstellung und Verfahren zur Hydroformylierung von olefinisch ungesättigten Verbindungen
US5307024A (en) 1992-07-27 1994-04-26 Tektronix, Inc. Linearized level-shifting amplifier
JPH0649554A (ja) * 1992-08-04 1994-02-22 N E Chemcat Corp ロジウムの回収方法
JPH0717909A (ja) * 1993-06-29 1995-01-20 Daicel Chem Ind Ltd メタクリル酸メチルの製造方法
US5767321A (en) * 1995-12-06 1998-06-16 Union Carbide Chemicals & Plastics Technology Corporation Metal-ligand complex catalyzed processes
US6252121B1 (en) 1999-07-27 2001-06-26 Union Carbide Chemicals & Plastics Technology Corporation Metal-ligand complex catalyzed processes
JP2001261660A (ja) * 2000-03-21 2001-09-26 Mitsui Chemicals Inc 着色の少ないイソシアヌレート環含有ポリイソシアナートの製造方法
DE10352258B4 (de) * 2003-11-08 2013-06-13 Oxea Gmbh Verfahren zur Herstellung von TCD-Diamin
DE10357718A1 (de) * 2003-12-09 2005-07-21 Basf Ag Verfahren zur Herstellung von Tricyclodecandialdehyd
JP4890107B2 (ja) * 2006-06-05 2012-03-07 株式会社クラレ ２−ヒドロキシ−４−メチルテトラヒドロピランの製造方法
US9227925B2 (en) * 2011-05-09 2016-01-05 Mitsui Chemicals, Inc. Process for producing aldehyde compounds

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Publication number Publication date
EP2918577B1 (en) 2018-07-25
JP5583879B1 (ja) 2014-09-03
KR20150047611A (ko) 2015-05-04
WO2014073663A1 (ja) 2014-05-15
US20180093944A1 (en) 2018-04-05
US10399930B2 (en) 2019-09-03
IN2015DN02806A (https=) 2015-09-11
JPWO2014073663A1 (ja) 2016-09-08
CN104768924A (zh) 2015-07-08
US20150291513A1 (en) 2015-10-15
US20180093945A1 (en) 2018-04-05
US10399929B2 (en) 2019-09-03
EP2918577A1 (en) 2015-09-16
US9809533B2 (en) 2017-11-07
CN104768924B (zh) 2017-03-01
EP2918577A4 (en) 2016-06-29

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