KR101587786B1 - 알킬화 촉매 재생을 최소화시키는 방법 - Google Patents

알킬화 촉매 재생을 최소화시키는 방법 Download PDF

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KR101587786B1
KR101587786B1 KR1020147005866A KR20147005866A KR101587786B1 KR 101587786 B1 KR101587786 B1 KR 101587786B1 KR 1020147005866 A KR1020147005866 A KR 1020147005866A KR 20147005866 A KR20147005866 A KR 20147005866A KR 101587786 B1 KR101587786 B1 KR 101587786B1
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alkylation
catalyst
alkylation catalyst
zeolite
aromatic hydrocarbon
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KR20140051389A (ko
Inventor
제임스 버틀러
신 시아오
짐 메릴
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피나 테크놀러지, 인코포레이티드
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/54—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
    • C07C2/64—Addition to a carbon atom of a six-membered aromatic ring
    • C07C2/66—Catalytic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
    • B01J29/7057—Zeolite Beta
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02—Monocyclic hydrocarbons
    • C07C15/067—C8H10 hydrocarbons
    • C07C15/073—Ethylbenzene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C6/00—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions
    • C07C6/08—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond
    • C07C6/12—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring
    • C07C6/126—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring of more than one hydrocarbon
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups C07C2529/08 - C07C2529/65
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020147005866A 2006-09-05 2007-08-27 알킬화 촉매 재생을 최소화시키는 방법 Expired - Fee Related KR101587786B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US11/515,679 2006-09-05
US11/515,679 US20080058566A1 (en) 2006-09-05 2006-09-05 Processes for reduction of alkylation catalyst deactivation utilizing low silica to alumina ratio catalyst
PCT/US2007/076872 WO2008030722A2 (en) 2006-09-05 2007-08-27 Processes for the reduction of alkylation catalyst deactivation utilizing low silica to alumina ratio catalyst

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
KR1020097006770A Division KR101542785B1 (ko) 2006-09-05 2007-08-27 저 실리카 대 알루미나 비의 촉매를 사용하여 알킬화 촉매 불활성화를 감소시키기 위한 방법

Publications (2)

Publication Number Publication Date
KR20140051389A KR20140051389A (ko) 2014-04-30
KR101587786B1 true KR101587786B1 (ko) 2016-01-25

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ID=39152703

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KR1020147005866A Expired - Fee Related KR101587786B1 (ko) 2006-09-05 2007-08-27 알킬화 촉매 재생을 최소화시키는 방법
KR1020147005870A Expired - Fee Related KR101586629B1 (ko) 2006-09-05 2007-08-27 알킬 방향족 화합물 제조방법
KR1020097006770A Expired - Fee Related KR101542785B1 (ko) 2006-09-05 2007-08-27 저 실리카 대 알루미나 비의 촉매를 사용하여 알킬화 촉매 불활성화를 감소시키기 위한 방법

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KR1020147005870A Expired - Fee Related KR101586629B1 (ko) 2006-09-05 2007-08-27 알킬 방향족 화합물 제조방법
KR1020097006770A Expired - Fee Related KR101542785B1 (ko) 2006-09-05 2007-08-27 저 실리카 대 알루미나 비의 촉매를 사용하여 알킬화 촉매 불활성화를 감소시키기 위한 방법

Country Status (8)

Country Link
US (5) US20080058566A1 (enExample)
EP (1) EP2064168A4 (enExample)
JP (1) JP5486306B2 (enExample)
KR (3) KR101587786B1 (enExample)
CN (2) CN101511753A (enExample)
CA (1) CA2661021C (enExample)
MX (2) MX2009002350A (enExample)
WO (1) WO2008030722A2 (enExample)

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US20080192226A1 (en) * 2004-06-07 2008-08-14 Nikon Corporation Stage Unit, Exposure Apparatus, and Exposure Method
US7645913B2 (en) 2007-01-19 2010-01-12 Exxonmobil Chemical Patents Inc. Liquid phase alkylation with multiple catalysts
US8134036B2 (en) * 2008-03-13 2012-03-13 Fina Technology Inc Process for liquid phase alkylation
US8865958B2 (en) * 2008-09-30 2014-10-21 Fina Technology, Inc. Process for ethylbenzene production
US8697208B2 (en) * 2009-07-24 2014-04-15 Fina Technology, Inc. Polystyrene nanocomposites for blow molding applications
US8455383B2 (en) 2009-09-28 2013-06-04 Fina Technology, Inc. Process for catalyst regeneration and extended use
JP5757996B2 (ja) * 2010-05-20 2015-08-05 エクソンモービル ケミカル パテンツ インコーポレイテッド 改善されたアルキル化プロセス
US20120296142A1 (en) * 2011-05-22 2012-11-22 Fina Technology, Inc. Addition of basic nitrogen to alkylation reactions
US8785706B2 (en) * 2011-05-22 2014-07-22 Fina Technology, Inc. Addition of a base to enhance product yield in alkylation reactions
CN105709815B (zh) * 2014-12-02 2018-06-19 中国石油化工股份有限公司 一种甲苯与乙烯选择性烷基化催化剂及其制备方法
CN108698952B (zh) * 2016-02-17 2021-04-27 巴杰许可有限责任公司 制备乙苯的方法
BR112019006899A2 (pt) * 2016-10-06 2019-07-02 Exxonmobil Chemical Patents Inc processo para metilar hidrocarbonetos aromáticos
KR20210088742A (ko) * 2016-10-06 2021-07-14 엑손모빌 케미칼 패턴츠 인코포레이티드 벤젠 및/또는 톨루엔의 메틸화에 의한 파라크실렌의 제조 방법
US10246387B2 (en) 2016-10-06 2019-04-02 Exxonmobil Chemical Patents Inc. Process for selectivating catalyst for producing paraxylene by methylation of benzene and/or toluene
US11673849B2 (en) 2016-12-21 2023-06-13 Exxonmobil Chemical Patents Inc. Process for selectivating catalyst for producing paraxylene by methylation of benzene and/or toluene

Citations (1)

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WO2003074452A1 (en) * 2002-02-28 2003-09-12 Stone & Webster, Inc. Production of alkyl aromatic compounds

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US4358362A (en) * 1981-01-15 1982-11-09 Mobil Oil Corporation Method for enhancing catalytic activity
US4642226A (en) 1984-04-16 1987-02-10 Mobil Oil Corporation Process for the preparation of zeolite Beta using dibenzyldimethylammonium ions and the product produced
US5081323A (en) * 1987-12-17 1992-01-14 Chevron Research And Technology Company Liquid phase alkylation or transalkylation process using zeolite beta
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Also Published As

Publication number Publication date
MX2009002350A (es) 2009-03-23
US20130225888A1 (en) 2013-08-29
MX374947B (es) 2025-03-06
CN102153435A (zh) 2011-08-17
KR101542785B1 (ko) 2015-08-07
US8680354B2 (en) 2014-03-25
CN101511753A (zh) 2009-08-19
CA2661021C (en) 2015-11-24
US20080058566A1 (en) 2008-03-06
US20140128651A1 (en) 2014-05-08
US9556083B2 (en) 2017-01-31
KR20140051390A (ko) 2014-04-30
JP5486306B2 (ja) 2014-05-07
JP2010502636A (ja) 2010-01-28
EP2064168A4 (en) 2010-12-15
CA2661021A1 (en) 2008-03-13
KR20090059139A (ko) 2009-06-10
KR20140051389A (ko) 2014-04-30
US20140005454A1 (en) 2014-01-02
US8552238B2 (en) 2013-10-08
US9556084B2 (en) 2017-01-31
US20110301396A1 (en) 2011-12-08
WO2008030722A3 (en) 2008-04-24
EP2064168A2 (en) 2009-06-03
WO2008030722A2 (en) 2008-03-13
KR101586629B1 (ko) 2016-01-19

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