KR101384935B1 - 산화 알킬렌의 제조 방법 - Google Patents

산화 알킬렌의 제조 방법 Download PDF

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Publication number
KR101384935B1
KR101384935B1 KR1020087023588A KR20087023588A KR101384935B1 KR 101384935 B1 KR101384935 B1 KR 101384935B1 KR 1020087023588 A KR1020087023588 A KR 1020087023588A KR 20087023588 A KR20087023588 A KR 20087023588A KR 101384935 B1 KR101384935 B1 KR 101384935B1
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South Korea
Prior art keywords
reaction
microreaction
carried out
microreaction system
ethylene
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Expired - Fee Related
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KR1020087023588A
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English (en)
Korean (ko)
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KR20080104345A (ko
Inventor
베른하르트 구트쉐
베른트 파브리
슈테판 프란첸
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코그니스 아이피 매니지먼트 게엠베하
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/14—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with organic peracids, or salts, anhydrides or esters thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00801—Means to assemble
    • B01J2219/0081—Plurality of modules
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00824—Ceramic
    • B01J2219/00828—Silicon wafers or plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00831—Glass
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00833—Plastic
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/00862—Dimensions of the reaction cavity itself
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00867—Microreactors placed in series, on the same or on different supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00869—Microreactors placed in parallel, on the same or on different supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020087023588A 2006-04-01 2007-03-23 산화 알킬렌의 제조 방법 Expired - Fee Related KR101384935B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102006015268A DE102006015268A1 (de) 2006-04-01 2006-04-01 Verfahren zur Herstellung von Alkylenoxiden
DE102006015268.9 2006-04-01
PCT/EP2007/002576 WO2007112866A1 (de) 2006-04-01 2007-03-23 Verfahren zur herstellung von alkylenoxiden

Publications (2)

Publication Number Publication Date
KR20080104345A KR20080104345A (ko) 2008-12-02
KR101384935B1 true KR101384935B1 (ko) 2014-04-11

Family

ID=38330712

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020087023588A Expired - Fee Related KR101384935B1 (ko) 2006-04-01 2007-03-23 산화 알킬렌의 제조 방법

Country Status (9)

Country Link
US (1) US7943790B2 (https=)
EP (1) EP2001858B1 (https=)
JP (1) JP2009532397A (https=)
KR (1) KR101384935B1 (https=)
CN (1) CN101415696B (https=)
DE (2) DE202006020415U1 (https=)
ES (1) ES2599847T3 (https=)
PL (1) PL2001858T3 (https=)
WO (1) WO2007112866A1 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007039874B9 (de) * 2007-08-20 2010-12-09 Zylum Beteiligungsgesellschaft Mbh & Co. Patente Ii Kg Verfahren zur Herstellung von Epoxiden durch Oxidation von Olefinen in der homogenen Gasphase
US8933254B2 (en) 2008-07-14 2015-01-13 Basf Se Process for making ethylene oxide
CN102099345A (zh) * 2008-07-14 2011-06-15 万罗赛斯公司 使用微通道工艺技术制造环氧乙烷的方法
US8524927B2 (en) 2009-07-13 2013-09-03 Velocys, Inc. Process for making ethylene oxide using microchannel process technology
JP5742390B2 (ja) * 2011-03-31 2015-07-01 株式会社Ihi 窒化ガリウム結晶の成長方法
CN107216296B (zh) * 2016-03-22 2020-07-17 中国石油化工股份有限公司 在微通道反应器内制备环氧丙烷的方法
CN112979587B (zh) * 2019-12-12 2022-12-02 中国科学院大连化学物理研究所 一种微通道反应器合成环氧丙烷的方法
EP4368649A1 (en) 2022-11-14 2024-05-15 Cliq Swisstech (The Netherlands) B.V. Continuous processs for the manufacture of urea urethanes

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060036106A1 (en) * 2004-08-12 2006-02-16 Terry Mazanec Process for converting ethylene to ethylene oxide using microchannel process technology

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19741645A1 (de) 1997-09-22 1999-03-25 Bayer Ag Verfahren und Vorrichtung zur Oxidation organischer Verbindungen in flüssiger Phase unter Verwendung peroxidischer Oxidationsmittel
DE10020632A1 (de) 2000-04-27 2001-10-31 Merck Patent Gmbh Verfahren zur Expodierung von Olefinen
DE10042746A1 (de) * 2000-08-31 2002-03-28 Degussa Verfahren und Vorrichtung zum Durchführen von Reaktionen in einem Reaktor mit spaltförmigen Reaktionsräumen
DE10257239B3 (de) 2002-12-04 2004-07-01 INSTITUT FüR ANGEWANDTE CHEMIE BERLIN-ADLERSHOF E.V. Verfahren zur Photooxigenerierung von Olefinen in Mikrostrukturreaktoren
JP2004285001A (ja) 2003-03-24 2004-10-14 Sumitomo Chem Co Ltd 含酸素化合物の製造方法
DE10317451A1 (de) * 2003-04-16 2004-11-18 Degussa Ag Reaktor für heterogen katalysierte Reaktionen
DE102004050506A1 (de) * 2004-10-15 2006-04-20 Degussa Ag Verfahren zur Herstellung von Olefinoxiden und Peroxiden, Reaktor und dessen Verwendung

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060036106A1 (en) * 2004-08-12 2006-02-16 Terry Mazanec Process for converting ethylene to ethylene oxide using microchannel process technology
WO2006020709A1 (en) 2004-08-12 2006-02-23 Velocys Inc. Process for converting ethylene to ethylene oxide using microchannel process technology

Also Published As

Publication number Publication date
WO2007112866A1 (de) 2007-10-11
DE202006020415U1 (de) 2008-07-03
CN101415696B (zh) 2012-08-22
EP2001858B1 (de) 2016-07-27
US7943790B2 (en) 2011-05-17
PL2001858T3 (pl) 2017-03-31
ES2599847T3 (es) 2017-02-03
DE102006015268A1 (de) 2007-10-25
KR20080104345A (ko) 2008-12-02
EP2001858A1 (de) 2008-12-17
JP2009532397A (ja) 2009-09-10
CN101415696A (zh) 2009-04-22
US20090253944A1 (en) 2009-10-08

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