KR101235549B1 - 하나 이상의 무색 디술피드/티올 전구체를 포함하는 염료 조성물 및 상기 조성물을 이용하는 염색 방법 - Google Patents

하나 이상의 무색 디술피드/티올 전구체를 포함하는 염료 조성물 및 상기 조성물을 이용하는 염색 방법 Download PDF

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Publication number
KR101235549B1
KR101235549B1 KR1020107006385A KR20107006385A KR101235549B1 KR 101235549 B1 KR101235549 B1 KR 101235549B1 KR 1020107006385 A KR1020107006385 A KR 1020107006385A KR 20107006385 A KR20107006385 A KR 20107006385A KR 101235549 B1 KR101235549 B1 KR 101235549B1
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South Korea
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group
formula
alkyl
precursor
hydrogen atom
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Expired - Fee Related
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KR1020107006385A
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English (en)
Korean (ko)
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KR20100043292A (ko
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앙드류 그리브
니꼴라 도브레쎄
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로레알
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B62/00—Reactive dyes, i.e. dyes which form covalent bonds with the substrates or which polymerise with themselves
    • C09B62/44—Reactive dyes, i.e. dyes which form covalent bonds with the substrates or which polymerise with themselves with the reactive group not directly attached to a heterocyclic ring
    • C09B62/78—Reactive dyes, i.e. dyes which form covalent bonds with the substrates or which polymerise with themselves with the reactive group not directly attached to a heterocyclic ring with other reactive groups
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A61K8/411—Aromatic amines, i.e. where the amino group is directly linked to the aromatic nucleus
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • A61K8/4933—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having sulfur as an exocyclic substituent, e.g. pyridinethione
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/10—Preparations for permanently dyeing the hair

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020107006385A 2007-09-24 2008-09-23 하나 이상의 무색 디술피드/티올 전구체를 포함하는 염료 조성물 및 상기 조성물을 이용하는 염색 방법 Expired - Fee Related KR101235549B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
FR0757808A FR2921258A1 (fr) 2007-09-24 2007-09-24 Composition tinctoriale comprenant au moins un precurseur incolore disulfures/thiol, proced de coloration a partir de la composition
FR0757808 2007-09-24
US96074207P 2007-10-11 2007-10-11
US60/960,742 2007-10-11
PCT/EP2008/062710 WO2009040354A1 (en) 2007-09-24 2008-09-23 Dye composition comprising at least one colorless disulfide/thiol precursor, and dyeing process using the composition

Publications (2)

Publication Number Publication Date
KR20100043292A KR20100043292A (ko) 2010-04-28
KR101235549B1 true KR101235549B1 (ko) 2013-02-21

Family

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Family Applications (1)

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KR1020107006385A Expired - Fee Related KR101235549B1 (ko) 2007-09-24 2008-09-23 하나 이상의 무색 디술피드/티올 전구체를 포함하는 염료 조성물 및 상기 조성물을 이용하는 염색 방법

Country Status (10)

Country Link
US (1) US8034125B2 (https=)
EP (1) EP2205681B1 (https=)
JP (3) JP2010540419A (https=)
KR (1) KR101235549B1 (https=)
CN (2) CN103251513A (https=)
AT (1) ATE522582T1 (https=)
BR (1) BRPI0816004B1 (https=)
ES (1) ES2368878T3 (https=)
FR (1) FR2921258A1 (https=)
WO (1) WO2009040354A1 (https=)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE518916T1 (de) 2006-03-24 2011-08-15 Oreal Färbezusammensetzung mit einem thiol/disulfid- leuchtfarbstoff mit einem heterozyklus und einer internen kationischen ladung sowie verfahren zur aufhellung von keratinmaterial mit diesem farbstoff
EP2024444B1 (fr) 2006-03-24 2011-07-06 L'Oréal Composition de teinture comprenant un colorant fluorescent naphtylimide thiol/disulfure, procede d'eclaircissement des matieres keratiniques a partir de ce colorant
FR2898903B1 (fr) 2006-03-24 2012-08-31 Oreal Composition de teinture comprenant un colorant disulfure fluorescent, procede d'eclaircissement des matieres keratiniques a partir de ce colorant
FR2921377B1 (fr) 2007-09-21 2009-10-30 Oreal Compose styryl a motif hydroxy(cyclo)alkylamino thiol/disulfure, procede d'eclaircissement des matieres keratiniques a partir de ce colorant
FR2921376B1 (fr) 2007-09-21 2009-10-30 Oreal Compose styryl tetrahydroquinolinium thiol/disulfure, procede d'eclaircissement des matieres keratiniques a partir de ce colorant
FR2921381B1 (fr) 2007-09-21 2009-10-30 Oreal Colorant hemicyanine styryle thiol/disulfure, composition tinctoriale comprenant ce colorant, procede d'eclaircissement des matieres keratiniques a partir de ce colorant
FR2921373B1 (fr) 2007-09-21 2009-10-30 Oreal Colorant derive d'indole styryle a linker alkylene, composition tinctoriale comprenant ce colorant, procede d'eclaircissement des matieres keratiniques a partir de ce colorant
FR2968954B1 (fr) 2010-12-15 2012-12-21 Oreal Procede de coloration de fibres keratiniques mettant en oeuvre un colorant direct a fonction disulfure/thiol/thiol protege et de la vapeur d'eau
WO2012112689A1 (en) * 2011-02-15 2012-08-23 The University Of North Carolina At Chapel Hill Nanoparticle, liposomes, polymers, agents and proteins modified with reversible linkers
FR2971935B1 (fr) 2011-02-25 2013-02-15 Oreal Composition pour colorer les fibres keratiniques comprenant un colorant direct a fonction disulfure/thiol, un polymere epaississant, un tensioactif non ionique, un agent alcalin, et un agent reducteur
FR2971938B1 (fr) 2011-02-25 2013-08-02 Oreal Composition pour colorer les fibres keratiniques comprenant un colorant direct a fonction disulfure/thiol, un alcool gras faiblement ou non ethoxyle, un tensioactif cationique, un agent alcalin, et un agent reducteur
FR2971936B1 (fr) 2011-02-25 2013-02-15 Oreal Composition pour colorer les fibres keratiniques comprenant un colorant direct a fonction disulfure/thiol, un tensioactif non ionique, un tensioactif amphotere, un alcool gras ethoxyle, un agent alcalin, et un agent reducteur
FR2971939B1 (fr) 2011-02-25 2013-02-15 Oreal Composition pour colorer les fibres keratiniques comprenant un colorant direct a fonction disulfure/thiol, un corps gras, un agent alcalin, et un agent reducteur
MX345094B (es) 2011-02-25 2017-01-17 Oreal Composicion para teñir fibras queratinicas que comprende un tinte directo que tiene un grupo funcional disulfuro/tiol, un polimero espesante, un alcohol graso etoxilado y/o un tensioactivo no ionico, un agente alcalino y un agente reductor.
FR2971937B1 (fr) 2011-02-25 2013-02-15 Oreal Composition pour colorer les fibres keratiniques comprenant un colorant direct a fonction disulfure/thiol, un polymere epaississant non cellulosique, un agent alcalin, et un agent reducteur
FR2990944A1 (fr) 2012-05-23 2013-11-29 Oreal Procede de coloration des fibres keratiniques comprenant un colorant /pigment, un compose photoactif, et une source lumineuse
RU2680068C2 (ru) 2013-09-02 2019-02-14 Л'Ореаль Способ окрашивания кератиновых волокон с применением катионных стириловых дисульфидных красителей и композиция, содержащая указанные красители
CN105492078A (zh) * 2013-09-03 2016-04-13 荷兰联合利华有限公司 评价头发颜色变化的方法
FR3043551B1 (fr) 2015-11-12 2017-11-24 Oreal Colorant direct cationique a chaine aliphatique et a fonction disulfure/thiol/thiol protege pour colorer les fibres keratiniques
FR3066108B1 (fr) 2017-05-10 2020-10-30 Oreal Colorant direct fluorescent a chaine aliphatique et a fonction disulfure/thiol/thiol protege pour colorer les matieres keratiniques
FR3067599B1 (fr) 2017-06-16 2020-09-04 Oreal Procede de coloration des matieres keratiniques mettant en oeuvre au moins un colorant bleu, violet ou vert et au moins un colorant fluorescent disulfure, thiol ou thiol protege
FR3067598B1 (fr) 2017-06-16 2020-09-11 Oreal Procede de coloration des fibres keratiniques mettant en œuvre au moins un colorant fluorescent disulfure, thiol ou thiol protege et au moins un activateur comprenant un reducteur et moins deux agents alcalins differents
FR3067597B1 (fr) 2017-06-16 2020-09-04 Oreal Procede de coloration des fibres keratiniques mettant en œuvre au moins un colorant direct et au moins un colorant fluorescent disulfure, thiol ou thiol protege
CN114015003A (zh) * 2021-11-17 2022-02-08 长春工业大学 一种基于香草醛含亚胺结构可降解聚氨酯弹性体及其制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003030847A1 (de) 2001-10-04 2003-04-17 Henkel Kommanditgesellschaft Auf Aktien Mittel zum färben von keratinhaltigen fasern
US20070130702A1 (en) 1998-12-23 2007-06-14 L'oreal S.A. Dyeing process using a specific compound containing active methylene and a compound chosen from a specific aldehyde, a specific ketone, a quinone and a diiminoisoindoline or 3-aminoisoindolone derivative

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE544768A (https=) 1955-01-28
NL105936C (https=) 1956-07-17
DE1544506A1 (de) 1965-01-02 1970-04-16 Hoechst Ag Verfahren zur Herstellung von basischen Azofarbstoffen
JPS548626A (en) 1977-06-23 1979-01-23 Hodogaya Chem Co Ltd Basic dye pyrido(1.2-a)indolium
DK140584A (da) * 1983-03-08 1984-09-09 Bristol Myers Co Fremgangsmaade til fremstilling af carbapenemderivater
US4880922A (en) * 1985-11-22 1989-11-14 Bristol-Myers Company Carbapenems with quaternized heterothioalkylthio substitution at position 2
US5034014A (en) * 1990-06-18 1991-07-23 Clairol, Inc. Hair dye composition and method
DE19842071A1 (de) * 1998-09-15 2000-03-16 Henkel Kgaa Verfahren zum Färben von keratinhaltigen Fasern unter Verwendung von stabilen Diazoniumsalzen
BR0007437A (pt) * 1999-01-08 2001-11-20 Procter & Gamble Composições tópicas que compreendem tióisfuncionais protegidos
US6114350A (en) * 1999-04-19 2000-09-05 Nen Life Science Products, Inc. Cyanine dyes and synthesis methods thereof
DE19936911A1 (de) * 1999-08-05 2001-02-08 Henkel Kgaa Mittel zum Färben von keratinhaltigen Fasern
DE19951134A1 (de) * 1999-10-23 2001-04-26 Henkel Kgaa Mittel zum Färben von keratinhaltigen Fasern
EP1133975B1 (en) 2000-03-17 2008-02-13 Kao Corporation Use of a compound for dyeing hair
JP2003246940A (ja) * 2002-02-27 2003-09-05 Fuji Photo Film Co Ltd シアニン色素の製造方法
EP2168634B1 (en) * 2002-09-13 2012-12-19 Kao Corporation Hair dye composition comprising methine dye
WO2005097051A2 (en) 2004-04-08 2005-10-20 Ciba Specialty Chemicals Holding Inc. Disulfide dyes, composition comprising them and method of dyeing hair
US7488354B2 (en) * 2004-10-14 2009-02-10 L'oreal S.A. Dyeing composition comprising at least one disulphide dye and method of dyeing human keratin fibers using this dye
FR2876576B1 (fr) 2004-10-14 2006-12-08 Oreal Composition de teinture comprenant un colorant disulfure particulier et procede de coloration des fibres keratiniques humaines a partir de ce colorant
US7247713B2 (en) 2004-12-15 2007-07-24 L'oreal, S.A. Symmetrical diazo compounds containing 2-pyridinium groups and cationic or non-cationic linker, compositions comprising them, method of coloring, and device
FR2879195B1 (fr) 2004-12-15 2007-03-02 Oreal Composes diazoiques symetriques a groupements 2-pyridinium et bras de liaison cationique ou non, compositions les comprenant, procede de coloration et dispositif
DE102005026545A1 (de) * 2005-06-08 2006-12-21 Henkel Kgaa Mehrkomponentenmittel zum Färben keratinischer Fasern
ES2328068T3 (es) * 2005-06-16 2009-11-06 Basf Se Colorantes del tipo esteril sulfuro.
EP2530261B1 (en) * 2005-09-23 2014-04-30 JP Scope, Inc. Valve apparatus for an internal combustion engine
CN100451003C (zh) * 2005-11-17 2009-01-14 复旦大学 含巯基的分子整流材料及其制备方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070130702A1 (en) 1998-12-23 2007-06-14 L'oreal S.A. Dyeing process using a specific compound containing active methylene and a compound chosen from a specific aldehyde, a specific ketone, a quinone and a diiminoisoindoline or 3-aminoisoindolone derivative
WO2003030847A1 (de) 2001-10-04 2003-04-17 Henkel Kommanditgesellschaft Auf Aktien Mittel zum färben von keratinhaltigen fasern

Also Published As

Publication number Publication date
WO2009040354A1 (en) 2009-04-02
JP2015193663A (ja) 2015-11-05
US8034125B2 (en) 2011-10-11
CN103251513A (zh) 2013-08-21
EP2205681B1 (en) 2011-08-31
ATE522582T1 (de) 2011-09-15
BRPI0816004A2 (pt) 2018-03-27
KR20100043292A (ko) 2010-04-28
JP2017203044A (ja) 2017-11-16
JP2010540419A (ja) 2010-12-24
JP6499037B2 (ja) 2019-04-10
FR2921258A1 (fr) 2009-03-27
BRPI0816004B1 (pt) 2018-08-28
ES2368878T3 (es) 2011-11-23
EP2205681A1 (en) 2010-07-14
CN101802107B (zh) 2014-08-27
US20110016642A1 (en) 2011-01-27
CN101802107A (zh) 2010-08-11

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