KR101192455B1 - 귀금속 촉매의 반응계외 환원 및 건식 부동화 - Google Patents

귀금속 촉매의 반응계외 환원 및 건식 부동화 Download PDF

Info

Publication number
KR101192455B1
KR101192455B1 KR1020077009839A KR20077009839A KR101192455B1 KR 101192455 B1 KR101192455 B1 KR 101192455B1 KR 1020077009839 A KR1020077009839 A KR 1020077009839A KR 20077009839 A KR20077009839 A KR 20077009839A KR 101192455 B1 KR101192455 B1 KR 101192455B1
Authority
KR
South Korea
Prior art keywords
catalyst
reduction
dry
oil
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
KR1020077009839A
Other languages
English (en)
Korean (ko)
Other versions
KR20070063572A (ko
Inventor
스테펜 제이 맥카티
진 더블유 비크만
위리암 쥐 보르가르드
실바인 한처
Original Assignee
엑손모빌 리서치 앤드 엔지니어링 컴퍼니
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 엑손모빌 리서치 앤드 엔지니어링 컴퍼니 filed Critical 엑손모빌 리서치 앤드 엔지니어링 컴퍼니
Publication of KR20070063572A publication Critical patent/KR20070063572A/ko
Application granted granted Critical
Publication of KR101192455B1 publication Critical patent/KR101192455B1/ko
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/0308—Mesoporous materials not having base exchange properties, e.g. Si-MCM-41
    • B01J29/0316—Mesoporous materials not having base exchange properties, e.g. Si-MCM-41 containing iron group metals, noble metals or copper
    • B01J29/0325—Noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42—Platinum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/041—Mesoporous materials having base exchange properties, e.g. Si/Al-MCM-41
    • B01J29/042—Mesoporous materials having base exchange properties, e.g. Si/Al-MCM-41 containing iron group metals, noble metals or copper
    • B01J29/043—Noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/064—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof containing iron group metals, noble metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/12—Oxidising
    • B01J37/14—Oxidising with gases containing free oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B01J37/18—Reducing with gases containing free hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B01J35/394—Metal dispersion value, e.g. percentage or fraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020077009839A 2004-10-01 2005-09-27 귀금속 촉매의 반응계외 환원 및 건식 부동화 Expired - Lifetime KR101192455B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US61501604P 2004-10-01 2004-10-01
US60/615,016 2004-10-01
US11/228,366 2005-09-16
US11/228,366 US7407909B2 (en) 2004-10-01 2005-09-16 Ex-situ reduction and dry passivation of noble metal catalysts
PCT/US2005/034752 WO2006039316A2 (en) 2004-10-01 2005-09-27 Ex-situ reduction and dry passivation of noble metal catalysts

Publications (2)

Publication Number Publication Date
KR20070063572A KR20070063572A (ko) 2007-06-19
KR101192455B1 true KR101192455B1 (ko) 2012-10-17

Family

ID=36126285

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020077009839A Expired - Lifetime KR101192455B1 (ko) 2004-10-01 2005-09-27 귀금속 촉매의 반응계외 환원 및 건식 부동화

Country Status (7)

Country Link
US (1) US7407909B2 (https=)
EP (1) EP1814664A4 (https=)
JP (1) JP5134958B2 (https=)
KR (1) KR101192455B1 (https=)
CA (1) CA2581187C (https=)
RU (1) RU2376060C2 (https=)
WO (1) WO2006039316A2 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2850882B1 (fr) * 2003-02-11 2005-03-18 Eurecat Sa Passivation de catalyseur d'hydroconversion sulfure
KR101274995B1 (ko) * 2006-08-31 2013-06-14 재단법인 포항산업과학연구원 고활성 다이옥신 분해용 슬러리형 Ｐｄ／Ｃ 촉매, 그제조방법 및 이를 이용한 다이옥신 분해 방법
WO2015050635A1 (en) 2013-10-03 2015-04-09 Exxonmobil Chemical Patents Inc. Hydrocarbon raffinate stream processing
EP3137212A1 (en) * 2014-04-30 2017-03-08 ExxonMobil Chemical Patents Inc. Method of improving metal-impregnated catalyst performance
AU2018311668A1 (en) 2017-08-03 2020-01-16 Exxonmobil Research And Engineering Company Activation of noble metal catalysts on siliceous supports with water-containing gas stream
US11433386B2 (en) 2019-01-25 2022-09-06 Exxonmobil Chemical Patents Inc. Activation of low metal content catalyst
WO2020154134A1 (en) * 2019-01-25 2020-07-30 Exxonmobil Chemical Patents Inc. Activation of low metal content catalyst
CN114522682B (zh) * 2020-11-23 2024-04-26 中国科学院大连化学物理研究所 一种炭载双金属单原子催化剂及其制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11104499A (ja) 1997-08-11 1999-04-20 Eurecat Europ De Retraitement De Catalyseurs 保護層の堆積による触媒の保護方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2850719A1 (de) * 1978-11-23 1980-07-10 Winsel August Prof Dipl Phys D Verfahren zur herstellung eines gegen die oxidation durch luftsauerstoff geschuetzten nickel-katalysators
US4372841A (en) * 1979-12-31 1983-02-08 Exxon Research And Engineering Co. Process for reducing coke formation in heavy feed catalytic cracking
GB2118453B (en) * 1982-03-12 1985-06-26 British Gas Corp Passivated nickel-alumina catalysts
NL9420024A (nl) * 1993-05-04 1996-05-01 Cri International Werkwijze voor het behandelen van spontaan ontbrandbare katalysatoren.
WO1994026846A1 (en) * 1993-05-10 1994-11-24 Akzo Nobel N.V. Hydrogenation of aromatics in hydrocarbonaceous feedstocks
US5451312A (en) * 1993-10-26 1995-09-19 Mobil Oil Corporation Catalyst and process for producing low-aromatics distillates
EP0736079B1 (en) * 1993-12-20 2000-05-10 Mobil Oil Corporation Hydrogenation process
FR2725381B1 (fr) * 1994-10-07 1996-12-13 Eurecat Europ Retrait Catalys Procede de pretraitement hors site d'un catalyseur de traitement d'hydrocarbures
FR2749779B1 (fr) * 1996-06-12 1998-09-11 Eurecat Europ Retrait Catalys Procede de presulfuration de catalyseurs d'hydrotraitement
DE19909175A1 (de) * 1999-03-03 2000-09-07 Kataleuna Gmbh Catalysts Verfahren zur Passivierung pyrophorer Katalysatoren
US6930219B2 (en) * 1999-09-07 2005-08-16 Abb Lummus Global Inc. Mesoporous material with active metals
JP4394787B2 (ja) * 1999-12-16 2010-01-06 独立行政法人産業技術総合研究所 芳香族炭化水素の水素化触媒組成物
ATE537898T1 (de) * 2000-04-11 2012-01-15 Albemarle Netherlands Bv Verfahren zur sulfidierung eines additiv- enthaltenden katalysators
US7094333B2 (en) * 2001-09-04 2006-08-22 The Regents Of The University Of Michigan Selective sorbents for purification of hydrocarbons
JP2003284961A (ja) * 2002-03-27 2003-10-07 National Institute Of Advanced Industrial & Technology 炭化水素の水素化処理触媒組成物の製造方法
EP3195931A1 (en) * 2002-10-18 2017-07-26 BASF Corporation Nickel catalyst for hydrogenation reactions
FR2850882B1 (fr) * 2003-02-11 2005-03-18 Eurecat Sa Passivation de catalyseur d'hydroconversion sulfure
FR2854335B1 (fr) * 2003-04-30 2009-03-20 Eurecat Sa Traitement hors site de catalyseurs d'hydrogenation
US20060073961A1 (en) * 2004-09-08 2006-04-06 Mccarthy Stephen J Noble metal-containing catalyst having a specific average pore diameter

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11104499A (ja) 1997-08-11 1999-04-20 Eurecat Europ De Retraitement De Catalyseurs 保護層の堆積による触媒の保護方法

Also Published As

Publication number Publication date
KR20070063572A (ko) 2007-06-19
CA2581187A1 (en) 2006-04-13
RU2376060C2 (ru) 2009-12-20
CA2581187C (en) 2012-08-07
EP1814664A4 (en) 2011-05-11
US7407909B2 (en) 2008-08-05
US20060073965A1 (en) 2006-04-06
JP5134958B2 (ja) 2013-01-30
WO2006039316A3 (en) 2006-09-08
JP2008514420A (ja) 2008-05-08
EP1814664A2 (en) 2007-08-08
WO2006039316A2 (en) 2006-04-13
RU2007114109A (ru) 2008-11-10

Similar Documents

Publication Publication Date Title
RU2146171C1 (ru) Каталитическая система для каталитических гидродесульфуризации, гидроденитрогенизации, реформинга, гидрирования-дегидрирования и изомеризации углеводородного сырья, способ ее получения, активации, регенерации и использования
CA2470393C (en) Arsenic removal catalyst and method for making same
JP6280705B2 (ja) 窒素含有化合物によるゼオライト触媒、特に、水素化分解触媒の不動態化方法
JP4927365B2 (ja) 水素化処理触媒の硫化方法
KR101192455B1 (ko) 귀금속 촉매의 반응계외 환원 및 건식 부동화
US8864980B2 (en) Hydrotreating process
CA3061358A1 (en) Methods for regenerating and rejuvenating catalysts
US7582587B2 (en) Passivation of sulphur hydroconversion catalyst
JPH08224484A (ja) 触媒及び水素処理方法
US4555495A (en) Reactivation of noble metal-containing zeolite catalyst materials
AU610628B2 (en) Process for dispersing or redispersing a group viii noble metal species on a porous inorganic support
EP0105631B1 (en) Very low crystallinity catalyst made from crystalline zeolite and process for catalytic dewaxing/pour point reduction of waxy hydrocarbon oils using said catalyst
JP5611750B2 (ja) 炭化水素処理用触媒の硫化方法
JP3486756B2 (ja) 炭化水素中の砒素を予備硫化された捕獲物質上への通過によって除去する方法
CN101031359B (zh) 贵金属催化剂的非原位还原和干燥钝化
NZ333762A (en) Process for presulphiding hydrocarbon conversion catalysts
US20020107139A1 (en) Encapsulated hydrogenation catalysts with controlled dispersion and activity
US9415385B2 (en) Activation of dual catalyst systems
DE102006025148A1 (de) Verfahren zur Herstellung eines geträgerten Metallkatalysators
JP4436757B2 (ja) チオフェン系化合物を含む炭化水素供給原料中の芳香族化合物の水素化方法
JP3324746B2 (ja) 硫黄化合物吸着剤
EP0969931A1 (en) Ex-situ presulphided hydrocarbon conversion catalysts
RU2758846C1 (ru) Способ получения зимних и арктических дизельных топлив из прямогонных дизельных фракций с содержанием серы до 5000 мг/кг и азота до 100 мг/кг
JP2002210362A (ja) 重質炭化水素油の水素化処理触媒、その製造方法及びそれを用いた重質炭化水素油の水素化処理方法
CN109718750B (zh) 用于加氢脱氮的载体、催化剂及其制备方法

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

FPAY Annual fee payment

Payment date: 20150930

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20160929

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

FPAY Annual fee payment

Payment date: 20170929

Year of fee payment: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

FPAY Annual fee payment

Payment date: 20180928

Year of fee payment: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

FPAY Annual fee payment

Payment date: 20190924

Year of fee payment: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

FPAY Annual fee payment

Payment date: 20201005

Year of fee payment: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

FPAY Annual fee payment

Payment date: 20210929

Year of fee payment: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

FPAY Annual fee payment

Payment date: 20221004

Year of fee payment: 11

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 11

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 12

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 13

PC1801 Expiration of term

St.27 status event code: N-4-6-H10-H14-oth-PC1801

Not in force date: 20250928

Ip right cessation event data comment text: Termination Category : EXPIRATION_OF_DURATION