KR100989724B1 - Manufacturing method nano particle chaga mushroom - Google Patents
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- KR100989724B1 KR100989724B1 KR1020070135156A KR20070135156A KR100989724B1 KR 100989724 B1 KR100989724 B1 KR 100989724B1 KR 1020070135156 A KR1020070135156 A KR 1020070135156A KR 20070135156 A KR20070135156 A KR 20070135156A KR 100989724 B1 KR100989724 B1 KR 100989724B1
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Abstract
본 발명에 의한 나노화된 차가버섯을 함유한 염모제 조성물은 레시친과 유사세라마이드(Questamide H)와 초산토코페롤과 프로필렌글리콜과 차가버섯 2차 추출액과, 글리세린과, 페노닙(PHENONIP)과 정제수로 조성되고,The hair dye composition containing nanoorganized chaga mushroom according to the present invention is composed of lecithin and pseudoceramide (Questamide H), tocopherol acetate, propylene glycol and chaga mushroom secondary extract, glycerin, phenonib (PHENONIP) and purified water,
상기 나노화된 차가버섯을 함유한 염모제 조성물을 제조하기 위해, 차가버섯을 건조기에 넣어서 건조시키는 건조단계와, 상기 건조된 차가버섯을 분쇄하여 분말로 만드는 분말 제조 단계와, 상기 분말을 정제수와 에탄올의 혼합 용매에 침적시키는 1차 침적 단계와, 상기 1차 침적 단계에서 침적되지 않은 상등액을 300메쉬 스크린과 1마이크로미터의 통공이 형성된 스크린으로 각각 여과시켜 1차 추출액을 걸러내는 1차 여과 단계와, 상기 1차 여과 단계를 거친 1차 추출액을 용매인 정제수와 에탄올의 혼합 용매에 침적시키는 2차 침적 단계와, 상기 2차 침적 단계에서 침전되지 않은 상등액을 1마이크로미터의 통공이 형성된 스크린으로 걸러서 2차 추출액을 얻는 2차 여과 단계가 이루어지고, In order to prepare the hair dye composition containing the nano- Chaga mushroom, the drying step of putting the chaga mushroom in a dryer and drying, a powder manufacturing step of pulverizing the dried chaga mushroom powder, and the powder of purified water and ethanol A primary filtration step of dipping in a mixed solvent and a supernatant not deposited in the first deposition step by filtering a 300 mesh screen and a screen having a hole of 1 micrometer, respectively, to filter the primary extract; The second immersion step of immersing the first extract after the first filtration step in a mixed solvent of purified water and ethanol as a solvent, and the supernatant not precipitated in the second immersion step by filtering the screen with a hole of 1 micrometer A second filtration step is made to get the tea extract,
상기 2차 추출액과 정제수, 레시친, 유사세라마이드, 초산토코페롤, 프로필렌글리콜, 글리세린, 페노닙, 정제수를 혼합하여 균질화한 후, 고압균질기에서 800바에서 3회 통과시켜 나노 입자로 만들어진 나노화된 차가버섯을 함유한 염모제 조성물을 조성한 것으로서, 이것을 이용하여 조제된 염모제에 관한 것이다.After homogenizing by mixing the secondary extract with purified water, lecithin , pseudoceramide , tocopherol acetate, propylene glycol, glycerin, phenonib , purified water, and then passed through three times at 800 bar in a high-pressure homogenizer nano-made chaga mushroom made of nanoparticles It is related with the hair dye prepared using the hair dye composition containing this, and using this.
차가버섯, 나노입자 Chaga, Nanoparticles
Description
본 발명은 나노화된 차가버섯을 함유한 염모제 조성물 및 그의 제조방법 그리고 상기 차가버섯 나노입자 조성물이 함유된 염모제에 관한 것으로서, 더욱 상세하게는 차가버섯 추출물을 나노입자로 제조하여 염모제의 원료로 사용되도록 하여 두피와 모발에 차가버섯 추출물이 흡수되도록 한 것이다.The present invention relates to a hair dye composition containing nanoparticles of chaga and a method for preparing the same, and a hair dye containing the chaga nanoparticle composition, and more particularly, to prepare chaga extract as nanoparticles to be used as a raw material of hair dye. Chaga mushroom extract will be absorbed into the scalp and hair.
차가버섯(chaga mushroom)은 살아 있는 자작나무에 기생하면서 숙주(宿主)의 영양분을 섭취하여 자라는 버섯으로서, 자작나무 속에서 5∼10년 동안 성장한 후, 목피를 뚫고 돌출되어 나와서, 10∼20년을 더 자라게 된다.A chaga mushroom is a mushroom that grows on the living birch and feeds on the nutrients of the host. It grows in the birch for 5 to 10 years, then protrudes through the bark, 10 to 20 years. Will grow more.
이러한 차가버섯은 사람에게 유익한 40∼50 종의 성분들(트리체페놀산, 호로마도겐, 다당류, 폴리당, 페놀알데히드, 등)로 이루어져 있는 데, 그 중에서 베타글루칸(β glucan)은 SOD(super oxide dismutase, 생리활성효소)의 역할을 하는 것으로서, 환경 오염으로 말미암아 인체가 생산하지 못하는 SOD의 양을 보충해 주는 역할을 하게 된다.Chaga is composed of 40 to 50 kinds of ingredients (trichephenolic acid, hormones, polysaccharides, polysaccharides, phenolaldehydes, etc.) beneficial to humans, among which beta glucan (β glucan) is SOD ( It plays a role of super oxide dismutase, which supplements the amount of SOD that the human body cannot produce due to environmental pollution.
상기 SOD는 인체에 나쁜 영향을 미치는 활성산소를 분해하는 항산화 기능을 하는 것으로서, 상기 활성산소는 세포를 공격하여 제 기능을 상실하고, 돌연변이가 되어 병원균으로부터 노출되어 질병이 발생하도록 하는 인체의 독이다.The SOD has an antioxidant function that decomposes free radicals that adversely affect the human body. The free radicals attack the cells, lose their function, become mutations, and are exposed to pathogens to cause disease. .
또한, 상기 차가버섯은 멜라닌 색소를 다량 함유하고 있는 데, 상기 멜라닌 색소는 SOD와 같은 항산화 물질이며, 유전자 보호 작용과 질병 억제 작용을 하는 물질인 것이 과학적으로 공지된 상태다.In addition, the chaga mushroom contains a large amount of melanin pigment, the melanin pigment is an antioxidant substance such as SOD, it is a state known scientifically to be a substance that has a gene protection action and disease suppression action.
그러나 지금까지, 상기 멜라닌 색소, 베타글루칸 등 인체에 유익한 성분을 많이 함유하고 있는 차가버섯을 염모제로 응용하지 못하고 있는 데, 그 이유는 차가버섯의 추출물이 염모제와 용이하게 혼합되며 머리카락 및 피부에 용이하게 흡수되도록, 나노 입자로 형성시켜야 하는 데, 아직까지 개발된 바가 없어서 약제나 건강식품으로서 복용될 뿐이었다.However, until now, the chaga mushroom containing a lot of beneficial ingredients such as melanin, beta glucan, etc. has not been applied as a hair dye, because the extract of chaga is easily mixed with the hair dye and is easy to hair and skin. It needs to be formed into nanoparticles so that it can be absorbed quickly.
또한 일반적인 화학 염모제는 모발의 멜라닌 색소를 탈색한 후, 새로운 컬러가 착색되도록 하는 것으로서, 머리카락을 손상시킬 뿐만 아니라, 수분을 제거하여 윤기 있고 아름다운 머리카락을 유지할 수 없고, 산화로 인하여 악취를 유발하며, 두피를 자극하여 피부병을 유발시키는 문제점이 있었다.In addition, a general chemical hair dye is used to decolor the melanin pigment in the hair, and then to color the new color, not only to damage the hair, but also to remove moisture, to maintain a glossy and beautiful hair, and to cause odor due to oxidation, There was a problem of causing skin diseases by stimulating the scalp.
이에 본 발명에서는 상기 차가버섯의 추출물을 염모제에 적용할 수 있도록 나노 입자로 제조함으로써, 염모제에 적용될 경우, 멜라닌 색소가 모발의 단백질인 케라틴과 자연스럽게 결합하여 염모 효과를 얻을 수 있도록 하여, 모발에 트리트먼트 및 보습 효과로 모발에 윤기를 부여하고 항산화 기능에 의해 산화로 인한 악취를 제거하며, 두피에서 발생한 산화로 인한 피부 질환을 항산화 기능에 의해 치료 가능하도록 하며, 함유되어 있는 베타글루칸에 의해 모근을 튼튼하게 함으로써 모공 관리에 효과가 있는 나노화된 차가버섯을 함유한 염모제 조성물 및 그의 제조방법을 제공하는 것을 목적으로 한다.In the present invention, by extracting the chaga extract in the nanoparticles to be applied to the hair dye, when applied to the hair dye, melanin pigments are naturally combined with keratin, a protein of the hair to obtain a hair dye effect, hair treatment It moisturizes and moisturizes hair, removes odors caused by oxidation by antioxidant function, treats skin diseases caused by oxidation on scalp by antioxidant function, and contains hair root by beta glucan. It is an object of the present invention to provide a hair dye composition containing nanoorganized chaga that is effective in pore management by making it durable.
상기 목적을 달성하기 위해 본 발명에서는 차가버섯 나노입자 추출액을 조제한 후, 상기 추출액 및 레시친과 유사세라마이드와 초산토코페롤과 프로필렌글리콜과 글리세린과 페노닙(PHENONIP)과 상기 구성물질에 100 중량%가 되도록 채워지는 정제수를 균질화한 후, 고압균질기에서 800바에서 3회 통과시켜 차가버섯 나노 입자가 제조되도록 하여 염모제에 적용되도록 한다.In order to achieve the above object, in the present invention, chaga mushroom nanoparticle extract is prepared, and then the extract and lecithin and pseudoceramide, tocopherol acetate, propylene glycol, glycerin, phenonib (PHENONIP) and the composition are filled to 100% by weight. After homogenizing the purified water, three times at 800 bar in a high pressure homogenizer so that chaga nanoparticles are produced to be applied to the hair dye.
본 발명에 의한 나노화된 차가버섯을 함유한 염모제 조성물 및 그의 제조방법은 차가버섯 나노 입자가 모발에 침투되어 멜라닌 색소가 모발의 단백질인 케라틴과 자연스럽게 결합하여 염모 효과를 얻을 수 있도록 함으로써, 모발에 트리트먼트 및 보습 효과로 모발에 윤기를 부여하고 항산화 기능에 의해 산화로 인한 악취를 제거하고, 두피에서 발생한 산화로 인한 피부 질환을 항산화 기능에 의해 치료 가능하도록 하며, 함유되어 있는 베타글루칸에 의해 모근을 튼튼하게 함으로써 모공 관리에 효과가 있다.The hair dye composition containing the nanonized chaga mushroom according to the present invention and a method for preparing the chaga mushroom nanoparticles penetrate the hair so that the melanin pigment naturally binds to keratin, which is a protein of the hair, thereby obtaining a hair dye effect. It moisturizes and moisturizes the hair, removes odors caused by oxidation by the antioxidant function, treats skin diseases caused by oxidation on the scalp by the antioxidant function, and restores the hair root by the contained beta glucan. By making it strong, it is effective in pore management.
이하, 상기 목적을 달성하기 위한 나노화된 차가버섯을 함유한 염모제 조성물 및 그의 제조방법을 살펴보면 다음과 같다.Hereinafter, looking at the hair dye composition containing the nanonized chaga mushroom and its preparation method for achieving the above object.
차가버섯은 멜라닌 색소, 베타글루칸 등 인체에 유익한 성분을 많이 함유하고 있는 것으로서, 본 발명에서는 상기 차가버섯의 추출물을 나노입자로 조제하여 염모제에 용이하게 첨가시킬 수 있도록 한 것과 상기 나노입자가 첨가된 염모제를 조제하여 차가버섯의 추출물이 피부에 영향을 미치도록 한 것을 특징으로 한다.Chaga contains a lot of beneficial ingredients such as melanin, beta glucan, etc. In the present invention, the extract of chaga is prepared as nanoparticles so that it can be easily added to the hair dye and the nanoparticles are added. By preparing a hair dye, chaga extract is characterized in that it affects the skin.
이를 위한 나노화된 차가버섯을 함유한 염모제 조성물을 살펴보면, 레시친 1∼5 중량%와 유사세라마이드(Questamide H, 0.1∼3.00 중량%와 초산토코페롤 0.1∼0.50 중량%와 프로필렌글리콜 10∼30.00 중량%와 차가버섯 2차 추출액 1∼30.00 중량%와, 글리세린 1∼10.0 중량%와, 페노닙(PHENONIP) 0.1∼0.5 중량%와 상기 조성물과의 합이 100 중량%가 되도록 첨가된 정제수로 조성된다.Looking at the hair dye composition containing nano- Chaga mushroom for this purpose, 1 to 5% by weight of lecithin and pseudoceramide ( Questamide H, 0.1 to 3.00% by weight , 0.1 to 0.50% by weight of tocopherol acetate and 10 to 30.00% by weight of propylene glycol) 1 to 30.00% by weight of the mushroom secondary extract, 1 to 10.0% by weight of glycerin, 0.1 to 0.5% by weight of PHENONIP, and purified water added to add 100% by weight of the composition.
상기 각 조성물의 중량%는 최적의 조건으로서 필요에 따라 가변이 가능함은 물론이다.The weight percent of each composition may be varied as necessary as the optimum conditions, of course.
상기 레시친, 유사세라마이드는 피부의 인지질과 유사한 기능을 가진 것으로 피부 컨디셔닝 효과가 있도록 하는 것이며, 상기 초산토코페롤은 항산화 물질로서 원료가 산패되는 것을 방지하고, 상기 프로필렌글리콜은 보습제의 기능을 하는 것이며, 페논닙은 방부제이고, 정제수는 상기 각 성분이 고르게 혼합되어 섞이도록 하는 용매의 역할을 하게 된다.The lecithin and pseudoceramide have a function similar to the phospholipid of the skin to have a skin conditioning effect, the tocopherol acetate is an antioxidant to prevent the raw material from being rancid, and the propylene glycol functions as a moisturizer. Nonnib is a preservative, and purified water serves as a solvent to mix and mix the components evenly.
상기 나노화된 차가버섯을 함유한 염모제 조성물은 나노화된 차가버섯 추출물이 모발과 두피에 흡입 가능하게 되고, 산패 방지 및 방부 효과와 더불어 보습효과와 피부컨디셔닝 효과를 구비함으로써, 염모제에 용이하게 적용할 수 있다.The hair dye composition containing the nanonized chaga mushroom can be easily applied to the hair dye by having the nanonized chaga extract extract is inhalable to the hair and scalp, and has a moisturizing effect and skin conditioning effect as well as antiseptic and antiseptic effects. have.
상기 나노화된 차가버섯을 함유한 염모제 조성물의 제조방법을 살펴보면 다음과 같다.Looking at the manufacturing method of the hair dye composition containing the nano- Chaga mushroom as follows.
차가버섯 5kg을 건조기에 넣어서 50℃ 이상에서 24시간 동안 건조시키는 건조단계와, 상기 건조된 차가버섯을 분쇄하여 분말로 만드는 분말 제조 단계와, 상기 분말을 정제수(精製水) 15kg과 에탄올 15kg의 혼합 용매에 침적시키는 1차 침적 단계가 이루어진다.5 kg of chaga mushroom in a drier and drying for 24 hours at 50 ℃ or more, a powder manufacturing step of pulverizing the dried chaga mushroom powder, and mixing the powder of 15 kg of purified water and 15 kg of ethanol A first deposition step is made which deposits in a solvent.
상기 1차 침적 단계에서 침적되지 않은 상등액을 300 메쉬의 스크린(screen)과 1마이크로의 통공이 형성된 스크린으로 각각 여과시키는 1차 여과 단계와, 상기 1차 여과 단계에서 얻어진 1차 추출액을 용매인 정제수 10kg과 에탄올 10kg의 혼합 용매에 침적시키는 2차 침적 단계와, 상기 2차 침적 단계에서 침적되지 않은 상등액을 1㎛의 통공이 형성된 스크린으로 여과시켜 2차 추출액을 얻는 2차 여과 단계가 이루어진다. 따라서, 상기 차가버섯 2차 추출액의 제조가 완료된다. 즉, 차가버섯 2차 추출액은 상기 차가버섯 분말을 1차 침적 단계와 1차 여과 단계를 거친 후, 다시 2차 침적 단계와 2차 여과 단계를 거쳐서 만들어낸 추출액을 지칭한다.
그리고, 정제수, 레시친 1∼5 중량%, 유사세라마이드 0.1∼3.00 중량%, 초산토코페롤 0.1∼0.50 중량%를 프로필렌글리콜 10∼30.00 중량%에 용해하여 균질화하는 1차 균질화 단계와, 상기 차가버섯 2차 추출액 1∼30.00 중량%와, 글리세린 1∼10.0 중량%, 페노닙 0.1∼0.5 중량%, 정제수를 혼합하여 균질화하는 2차 균질화 단계와 상기 1차, 2차 균질화 단계를 거친 용액을 혼합하여 균질화한 후, 고압균질기에서 800바에서 3회 통과시켜 용액 상태의 차가버섯 나노 입자가 제조되도록 하는데, 상기 1차, 2차 균질화 단계의 정제수 합은 상기 조성물과의 합계가 100 중량%가 되도록 양이 조정되어 첨가된다.The first filtration step of filtering the supernatant not deposited in the first immersion step into a screen of 300 mesh screen and a screen having a hole of 1 micro, respectively, and the first extract obtained in the first filtration step is purified water as a solvent. A secondary immersion step of immersing in a mixed solvent of 10 kg and 10 kg of ethanol, and a secondary filtration step of obtaining a secondary extract by filtering the supernatant not deposited in the second immersion step through a screen having a 1 μm aperture. Thus, the preparation of the chaga secondary extract is completed. That is, the chaga mushroom secondary extract refers to the extract produced through the secondary filtration step and the secondary filtration step after the primary filtration step and the primary filtration step.
In addition, a first homogenization step of homogenizing by dissolving purified water, 1 to 5% by weight of lecithin, 0.1 to 3.00% by weight of pseudoceramide, and 0.1 to 0.50% by weight of tocopherol acetate in 10 to 30.00% by weight of propylene glycol, and secondary chaga mushroom 1 to 30.00% by weight of the extract, 1 to 10.0% by weight of glycerin, 0.1 to 0.5% by weight of fenonib, and homogenized by mixing the second homogenization step and homogenizing the solution after the first and second homogenization step Afterwards, the mixture is passed three times at 800 bar in a high pressure homogenizer to prepare chaga mushroom nanoparticles in a solution state. Adjusted and added.
삭제delete
상기 각 조성물의 중량%는 최적의 조건으로서 필요에 따라 가변이 가능함은 물론이다.The weight percent of each composition may be varied as necessary as the optimum conditions, of course.
상기에서 정제수와 에탄올의 혼합 용매에 차가버섯의 분말을 침적시키는 이유는 정제수와 에탄올에 각각 녹는 물질을 모두 용해시키기 위해서이며, 1차 여과 단계를 거친 후, 2차 침적 단계 및 2차 여과 단계를 거치는 이유는 1차 여과 단계 후 1차 추출물에 용해된 물질이 석출되어 알맹이로 형성되기 때문에, 이를 다시 혼합 용매에 침적시켜 용해시킨 후, 2차 여과를 거쳐 완전한 액상으로 조제하기 위해서이다.The reason for immersing the powder of chaga in the mixed solvent of purified water and ethanol is to dissolve all the soluble substances in purified water and ethanol, respectively, after the first filtration step, the second immersion step and the second filtration step The reason for the passage is that the material dissolved in the first extract after the first filtration step is precipitated and formed into kernels, so that it is immersed in a mixed solvent to dissolve and then dissolved in a mixed solvent to prepare a complete liquid phase through secondary filtration.
상기 고압균질기는 가압에 의해 미세한 간극 사이로 균질화된 용액을 밀어내는 기계로서 800바의 압력으로 상기 간극을 3번 통과시키게 되면 미세한 나노입자가 형성된다.The high pressure homogenizer is a machine that pushes the homogenized solution between the fine gaps by pressurization and passes the gap three times at a pressure of 800 bar to form fine nanoparticles.
1차 균질화 단계와 2차 균질화 단계로 공정을 나누어서 작업한 후, 다시 1, 2차 균질화 단계를 거친 용액을 혼합하는 이유는, 보다 용이하게 혼합되어 각 성분이 고르게 분포되어 균질화되도록 하기 위해서이다.After dividing the process into a first homogenization step and a second homogenization step, the first and second homogenization steps are mixed again so that the solution is more easily mixed so that each component is evenly distributed and homogenized.
이하 나노화된 차가버섯을 함유한 염모제 조성물을 이용한 염모제의 실시예를 살펴보면 다음과 같다.Hereinafter, an example of a hair dye using a hair dye composition containing nanoorganized chaga is as follows.
하기와 같은 조성의 염모제를 일반적인 제조방법으로 조제하였다.A hair dye having the following composition was prepared by a general manufacturing method.
나노화된 차가버섯을 함유한 염모제 조성물 5.0 중량%,5.0 wt% hair dye composition containing nanoorganized chaga,
P-페닐렌디아민 0.8 중량%, 0.8 wt% of P-phenylenediamine,
P-아미노-O크레졸 0.5 중량%, 0.5 wt% of P-amino-Ocresol,
모노에탄올아민 5 중량%, 5% by weight monoethanolamine,
올레일알콜 2 중량%, 2% by weight of oleyl alcohol,
스테아릴알콜 5중량%, 5% by weight of stearyl alcohol,
세탄올 5 중량%, Cethanol 5% by weight,
호호바유5 중량%, 5% by weight of jojoba oil,
폴리옥시에칠렌세틸에텔(12E.O) 4중량%, 4% by weight of polyoxyethylene cetyl ether (12E.O),
염화세틸트리메칠암모늄29 2.5 중량%, Cetyltrimethylammonium chloride29 2.5% by weight,
치오글리콘산암모늄 0.5 중량%, 0.5 wt% ammonium thioglyconate,
정제수 64.7 중량%Purified water 64.7 wt%
상기 각 조성물의 중량%는 최적의 조건으로서 필요에 따라 가변이 가능함은 물론이며, 상기 실시예는 하나의 예시로서 제시된 것이다.The weight percent of each composition may be varied as necessary as the optimum conditions, and the above examples are presented as an example.
상기 나노화된 차가버섯을 함유한 염모제 조성물이 함유된 염모제를 임상 실험한 결과, 차가버섯 나노입자가 모발에 침투되어 모발에 트리트먼트 및 보습 효과로 모발에 윤기를 부여하고 항산화 기능에 의해 산화로 인한 악취를 제거하며, 두피에서 발생한 산화로 인한 피부 질환을 항산화 기능에 의해 치료 가능하도록 하며, 함유되어 있는 베타글루칸에 의해 모근을 튼튼하게 함으로써 모공 관리에 효과가 있는 것을 확인할 수 있었다.The nano the difference result of clinical trials, the hair dyes of the hair dye composition containing a mushroom-containing, the difference is with mushrooms nanoparticles penetrates the hair giving a gloss to the hair as a treatment and moisturizing effect to the hair, and due to oxidation by the antioxidant properties Elimination of odor, skin disease caused by oxidation caused in the scalp can be cured by the antioxidant function, and by strengthening the hair root by the contained beta glucan was confirmed that it is effective in pore management.
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| KR101489126B1 (en) | 2014-06-30 | 2015-02-04 | 김용배 | Mushroom extract using fulvic and extracting method thereof |
| KR20190030280A (en) | 2017-09-14 | 2019-03-22 | 농업회사법인 주식회사 수신오도 | Bamboo vessel-matured puerh tea including Chaga mushroom and manufacturing method thereof |
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| KR101121713B1 (en) * | 2010-11-16 | 2012-03-21 | 서현숙 | The broccoli soap to produce with the conc. solution of beanstalk's ash and pottery core |
| KR101494602B1 (en) * | 2012-08-10 | 2015-02-23 | 주식회사 셀루스 | A composite having the function of sun-blocking and manufaturing method thereof |
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| JPH0348612A (en) * | 1989-07-18 | 1991-03-01 | Nikka Chem Co Ltd | Hair dyeing composition |
| KR20010057260A (en) * | 1999-12-21 | 2001-07-04 | 김기운 | A composition for neutral hair-dyeing agent having allergy suppression and hair damage prevention effect |
| KR20040102558A (en) * | 2003-05-28 | 2004-12-08 | 유앤아이화장품(주) | Cosmetic composition including an extract from inonotus obliquus having skin age resisting effect and the preparation the same |
| KR20070063207A (en) * | 2005-12-14 | 2007-06-19 | 이창구 | Hair improving material |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH0348612A (en) * | 1989-07-18 | 1991-03-01 | Nikka Chem Co Ltd | Hair dyeing composition |
| KR20010057260A (en) * | 1999-12-21 | 2001-07-04 | 김기운 | A composition for neutral hair-dyeing agent having allergy suppression and hair damage prevention effect |
| KR20040102558A (en) * | 2003-05-28 | 2004-12-08 | 유앤아이화장품(주) | Cosmetic composition including an extract from inonotus obliquus having skin age resisting effect and the preparation the same |
| KR20070063207A (en) * | 2005-12-14 | 2007-06-19 | 이창구 | Hair improving material |
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| KR101489126B1 (en) | 2014-06-30 | 2015-02-04 | 김용배 | Mushroom extract using fulvic and extracting method thereof |
| KR20190030280A (en) | 2017-09-14 | 2019-03-22 | 농업회사법인 주식회사 수신오도 | Bamboo vessel-matured puerh tea including Chaga mushroom and manufacturing method thereof |
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