KR100947638B1 - Composition comprising lava seawater salt - Google Patents

Abstract

The present invention relates to a composition containing lava sea salt and lava sea salt containing at least one selected from green tea, black tea, aloe, grape, banana and apple extract as an active ingredient, the composition of the present invention is to enhance the moisturizing power of the skin, It can be usefully used as a cosmetic composition for protecting and improving skin having an elasticity promoting and anti-inflammatory effect, a bathing agent, a soap composition, and an oral composition having a caries prevention effect.

Lava salt, Moisturizing, Elasticity, Anti-inflammatory, Cosmetic, Bath, Soap, Oral

Description

Composition containing lava seawater salt

1 is a diagram showing the cytotoxic effect of the composition containing lava sea salt.

The present invention relates to a composition for oral cavity having lava sea salt as an active ingredient, a cosmetic, bathing agent, soap composition and caries prevention effect for skin protection and improvement.

Skin is the most important organ in our body that most closely contacts the outside environment. Skin can be divided into three categories: epidermis, dermis and hypodermis. As the skin ages, phenomena such as wrinkles, dry skin, and sagging skin appear due to ultraviolet rays, pollution, and stress.

The skin is a complex organ composed of cells of various functions and corresponding physical properties. The dermal layer combines elastic solid materials (fibres) with viscous liquid materials to maintain inherent skin elasticity. . Thus, the skin reacts to mechanical tension due to its unique properties, which is called viscoelasticity. The skin has such viscoelasticity because collagen fibers and elastin fibers form a unique three-dimensional structure in the substrate of proteoglycans. In general, as the age of the skin decreases due to ultraviolet rays, pollution, stress, changes in atrophy appear, the number of skin cells or the thickness of the skin is reduced. In this process, the elastic fibers of the skin are deformed and the elasticity of the skin is reduced or the skin is stretched.

Human living bodies are mostly composed of water, which plays an important role in maintaining life. The moisture in normal skin is 70% in the body and 20% in the stratum corneum to support the elasticity and flexibility of the skin. If the moisture in the stratum corneum is less than 10%, the skin is known to dry out and cause skin problems. Moisture balance in the skin is controlled by the epidermis. The stratum corneum of the epidermis is the accumulation of dead cells, but plays a very important role in maintaining skin moisture. The amount of water in the stratum corneum produced by regular keratinization is always 10-20%. This is due to the sebum film, which is a mixture of sweat and sebum, which protects the skin from the outside and prevents water from evaporating from the stratum corneum. Natural Moisturizing Factor (NMF) and dermis lipids hold and retain moisture. Sebaceous membrane, NMF and dermis are working together to keep skin moisturized. NMF is a hydrophilic hygroscopic substance produced by keratinization process and plays an important role in moisturizing the skin. It is made of amino acids and holds moisture in the horny layer. In addition, 2-pyrrolidine-5-carboxylic acid (PCA) is particularly important in NMF. It forms a layer with a matrix filled between each cell and maintains moisture inside (Seuk Won Won and 2 others, Understanding and Treatment of Skin Aging, Journal of Skin Barriers, 4 , pp71-80, 2002).

When the skin is exposed to irritating substances, the stratum corneum is damaged, thus increasing transepidermal water loss, which is an indicator of stratum corneum damage, which may be a primary inflammatory response. Inflammatory reactions that can be caused by the use of cosmetics include irritation such as itching, stinging and burning, erythema and edema, and irritant contact with contact dermatitis. Dermatitis, allergic contact dermatitis, sensory stimulation, and phototoxic dermatitis can be roughly classified, but these symptoms are difficult to distinguish clearly and most often occur in combination with each other. Above all, in order for the inflammatory reaction to occur, foreign substances penetrate the skin, and they can be said to be activated by activating the immune system through interaction with epidermis or dermal cells.

Lava sea salt is a salt obtained from lava seawater. Lava seawater is a unique water resource that has been aged for a long time after seawater has been naturally filtered through basalt and sanisil layers and has been aged for a long time. Because of its cleanliness, lava seawater has been actively used as a breeding ground for flounder farms. Since 5-6 years ago, it has been used as a sauna water in terms of health and beauty.

Lava seawater contains not only essential minerals such as sodium, magnesium, calcium and potassium, but also general useful minerals (iron, manganese, zinc, molybdenum, etc.) than deep seawater and deep water than general seawater and deep water. Characteristically, lava seawater contains a large amount of useful components, so the industrial utilization value is very high. Among them, the action of stabilizing insulin secretion is now used to treat diabetes, vanadium, which improves hyperlipidemia, promotes blood circulation, enhances immunity, germanium, which has anticancer activity, inhibits oxidation of fat, synergistic effect of maintaining heart and liver, radical Selenium, which is effective in scavenging, anti-cancer, infertility, aging, and cholesterol levels, is a unique feature of lava seawater that has never been reported in deep sea water. In addition, these minerals are in an ionized state, which is easily digested and absorbed by humans and other animals. In addition, lava seawater is a clean groundwater resource in which E. coli, nitrate nitrogen, phosphate, phenol, etc. are not detected, and lava obtained from lava seawater because no harmful components such as arsenic, mercury, cadmium, or lead are detected Sea salt is not an obstacle to industrial application.

Recently, the interest in half body baths has increased, and the domestic market for bathing agents has been greatly expanded recently. The effect of half-bath was known by Dutch name at the beginning of the 18th century. The half-bath is soaked in warm water at 37-39 ℃ just above body temperature for 20-30 minutes under the chest. Do not put your shoulders or arms under water. This may cause you to feel a bit chilly at first, but it will gradually warm up from the center of your body, causing you to sweat. The source of all illnesses is the cold and cold state of body temperature, which increases the body temperature of the upper body and lowers the body temperature of the lower body. The half body bath removes this cold, which causes blood circulation disorder by warming the lower body. It's a bath. In addition to the flow of blood flow and acupuncture points through acupuncture and meridian heat stimulation to help the circulation of the people these days, many people enjoy half-bath. Therefore, a lot of commodities for bathing agents, including half-baths.

Recently, the most widely used substances for skin protection are expensive placenta extract, sturgeon egg (caviar), retinol, vitamin C, etc. To prevent it from being absorbed into the interior. Therefore, even if you apply a good ingredient is not effective because it is difficult to absorb into the skin. This is because the main function of the skin is secretion, not absorption. Therefore, the best method of skin protection is to discharge the waste and maintain the self-cleaning function of the human body by promoting the secretion, which is a unique function of the skin, by using a bath that has excellent blood circulation, heat action, and sweating action without any skin irritation. It is to be.

In this regard, 26 patents have been searched as of 2004. Among them, the patent application of the bathing agent related to herbal medicine is disclosed in Korean bathing agent disclosed in Korean Patent Publication No. 2004-83033 and its manufacturing method, Korean Patent Publication No. 2004-0081248 There is a method for producing a functional herbal bath containing turmeric extract disclosed in the above, a functional bath composition comprising a natural plant extract component disclosed in Korean Patent Laid-Open Publication No. 2004-0035950, and a method for producing the same. These baths have been described as having effects of preventing skin aging, skin moisturizing effect, fatigue recovery, skin beauty, and blood circulation. However, all of them have a problem that the skin irritation is insufficient even though they are used in contact with the skin. In other words, herbal baths can expect various pharmacological effects depending on the type of herbal medicines used as raw materials. On the other hand, the active ingredients with these pharmacological effects can act as a strong irritant to the skin. Unless otherwise, there should be no skin irritation. Therefore, while having various pharmacological effects, there is a need for a bath without any skin irritation.

Looking at the effects of salt on the oral cavity, in general, when salt is used in the oral cavity, it is known to be effective in preventing or treating periodontal diseases such as oral diseases, especially gingivitis and alveolar pylori, by converging action on the gums. Many oral compositions containing salt have been proposed for the purpose of preventing and treating diseases.

Looking at the domestic patents related to salt, bamboo salt, which is widely known as a therapeutic agent in traditional Korean folk remedies, has already been commercialized and used widely with patent applications. Patents related to bamboo salt include Korean Patent Application Nos. 92-12630, 92-25416, 93-16729, 93-23960, 2001-0011005, etc. There is no teaching or disclosure about the use of the cosmetics, baths, soaps and oral compositions used.

Green tea has the longest history among beverages around the world, and is widely used in 160 countries as the three major beverages along with coffee and cocoa. These green teas contain polyphenols, including flavanols, flavanidiols, flavonoids and phenol acids, which account for about 30% of the dry weight of green tea. Occupies. In addition, the tea polyphenols are anti-allergic (Yeo et al.,. Antioxidative effect of tea extracts from green tea, oolong tea and black tea, J. Korean Soc. Food Sci. Nutr., 24, pp.229-304, 1995 (An et al., Inhibitory effect of flavan-3-ols isolated from oolong tea on xanthine oxidase., Korean J Food Sci . Technol ., 28 (6) , pp. 1084-1088, 1996), gout It is reported that prevention, antibacterial and oxidation are excellent.

Aloe vera glycoprotein (Glycoprotein) to the (Aloe vera, Aloe barbadensis Miller) is a jelrijil has hypoglycemic activity in polysaccharides with immunity enhancing effect and wound healing effect of the human body (Polysaccharids) and the body to be removed, and aloe peel using only jelrijil It contains a large amount of active ingredients (Duk-kyun Ahn, Korean Herbal Painting, pp280, Kyohaksa, 2000: Changmin Kim, Primary Color Herbal Painting, pp306, Academy Books, 2001).

Vitis vinifera L.) is a deciduous tree that contains glucose, fructose, small amounts of xylose, tartaric acid, acetic acid, citric acid and malic acid. Grape peel contains cyanidin, peonidin, delpinidin, petunidin, malvidin and oenin, and the fat content of seeds is 9.58 %, Catechol, gallocatechol, vitamins B1 and B2, nicotinic acid, vitamin C, and the like. It is known to cure blood, muscle, bone, and iso-pyeon, and to treat weakness of blood, pain caused by rheumatism, swelling, low back pain, and stomach pain. Shin Min, Teaching Ambassador, Yeonglimsa, pp298-303, 1998).

The green leaves of black tea are composed of 75-80% moisture and 20-25% solids. The green leaves are fermented and heat treated to produce black tea. This is because it prevents the chlorophyll from being destroyed, removes moisture from the tea leaves and makes the surface of the black tea impermeable, thereby minimizing the escape of the tea leaf components and prolonging the storage. Tea is uniquely composed of caffeine and polyphenol (catechin), a tannin-based substance, and contains various amino acids to make tea unique. Caffeine is an awakening and diuretic effect, which is almost excreted with catechins. The astringent catechin is oxidized to give a reddish brown color, and occupies the most of the components of black tea, and has a large number of hydroxyl groups (-OH) in chemical structure, so that it can be easily combined with various substances. Because of this property, it has antioxidant activity to remove heavy metals or free radicals in the body. In general, catechins are expected to be effective in inhibiting carcinogenesis, mutagenesis, antioxidant, blood cholesterol, hypertension, detoxification, bad breath and odor removal. Vitamin C, a potent antioxidant, works synergistically with tocopherols and catechins, which are contained in tea leaves.

Banana is an evergreen perennial herbaceous perennial plant, 3 ~ 10m high, leaves are long oval, pale yellow flowers in early summer, fruits are crescent long oval, ripe, yellowish, and tropical This is origin. Bananas are low-calorie foods with 87 calories per 100 grams of calories, with little fat, very low sodium, rich in potassium and vitamins B6 and C. Therefore, bananas are known to be good for high blood pressure, stress relief, and gastrointestinal disease, and are said to lower the risk of cerebral hemorrhage or heart disease. Starch and protein are comparable to potatoes, and pectin, one of carotene and dietary fiber. When bananas are fully cooked, the sugars produced are fructose and glucose, so digestion and absorption are good for patients, children, and those who exercise. Bananas help to regulate heart rate and balance body ions, and pectin, which is effective for constipation, helps the intestines function.

Apples are rich in vitamins and minerals, especially 110 mg of calcium, which releases salt from the body. It also has a lot of fiber, so it has a formal effect, and it creates a jelly-shaped shield on the wall of the intestine to prevent the absorption of toxic substances and to prevent abnormal fermentation in the intestine. The organic acids of apples stimulate the secretion of gastric juice to help digestion, increase iron absorption, and relieve stress from stress. Apples are a tonic product belonging to the Rosaceae family, which contains abundant citric acid and tartaric acid, which removes fatigue substances from the body.In addition, apple's pectin is good for hypertension, arteriosclerosis, and obesity. It is effective in diabetics by controlling and preventing blood sugar fluctuations. Pectin in apple sauce and ground apples is good for recovery during diarrhea. It also contains a lot of potassium, which helps balance blood pressure.

The present inventors found lava saltwater obtained from Jeju lava seawater and continued the research. As a result, the composition containing it has excellent skin moisturizing, elasticity and anti-inflammatory effects, and thus has excellent effects on skin protection and improvement. It has been found to be effective in inhibiting tooth decay compared to general natural salts. Also, it contains green tea, black tea, aloe, grape, banana, and apple extracts in lava sea salt, which is provided in plant extracts in addition to mineral components of lava sea salt. Phenolic substances such as phenylalkanoids, flavonoids, anthocyanins, flavonols, flavonoids and flavones, terpenoids such as saponins, diterpenoids, monoterpenoids, and steroids, citric acid, malic acid and grape acid Vaginal acids, fatty acids, sugars and alkanoids, peptides, purines and purimidines The lava year by reinforcement-containing compounds, such as providing a composition having a critical effect of the whiskers, thereby completing the present invention.

The present invention provides a composition containing lava sea salt and lava sea salt containing one or more selected from green tea, black tea, aloe, grape, banana and apple extract as an active ingredient.

The present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt and lava sea salt containing one or more selected from green tea, black tea, aloe, grape, banana and apple extract as an active ingredient.

One preferred aspect of the present invention provides a cosmetic, bathing agent, soap and oral composition containing lava sea salt.

One preferred embodiment of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt and green tea extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt and black tea extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt and aloe extract.

One preferred aspect of the present invention provides a cosmetic, bathing agent, soap and oral composition containing lava sea salt and grape extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt and banana extract.

One preferred aspect of the present invention provides a cosmetic, bathing agent, soap and oral composition containing lava sea salt and apple extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt, green tea and black tea extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt, aloe and grape extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt, banana and apple extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt, green tea, aloe and apple extract.

One preferred aspect of the present invention provides a cosmetic, bath, soap and oral composition containing lava sea salt, black tea, grapes and banana extract.

The lava sea salt as defined in the present invention is excavated from 100 to 200 m underground, preferably 150 m underground in the eastern part of Jeju Island, Gujwa-eup, Gujwa-eup, 30-150 m underground, preferably 44.35 m, 86.35 m Alternatively, the lava salt water taken at 126.35m is sterilized using a sterile filter, and then obtained by using a method such as heat evaporation, vacuum evaporation, sun drying or ventilation drying.

The extract of the present invention is a cosmetic extracted with a solvent selected from polar solvents such as lower alcohols having 1 to 4 carbon atoms, such as water, methanol, ethanol and a non-polar solvent such as acetone, ethyl acetate, chloroform, dichloromethane or a mixed solvent thereof And bath compositions, soaps, and oral compositions.

Hereinafter, the present invention will be described in more detail.

The lava sea salt of the present invention and a specific manufacturing process for producing lava sea salt containing one or more selected from green tea, black tea, aloe, grape, banana and apple extract is as follows.

Excavated 150m underground in Handong-ri, Gujwa-eup, Bukjeju-gun, Jeju-do, and sterilized Jeju lava seawater taken from 44.35m, 86.35m, or 126.35m underground (by average sea level) using a sterile filter, followed by heating evaporation, vacuum evaporation, and sun drying. Or a step of obtaining dry powder of lava sea salt using a drying method such as ventilation drying, preferably a ventilation drying method; Green tea, aloe, black tea, banana or apple, 2 to 20 times by weight, preferably 1 to 10 times the volume of water and C1 to C4 lower alcohols, such as methanol, ethanol, butanol, etc., preferably ethanol or these Mixed solvent having a mixing ratio of 1 to 50% by weight, preferably 10 to 30% by weight of hot water extraction, cold extraction, reflux cooling extraction for about 1 to 5 weeks at room temperature, preferably 1 to 3 weeks. Alternatively, by using an extraction method such as ultrasonic extraction, the supernatant is recovered by vacuum filtration, and then the above process is repeated 2 to 5 times, preferably twice, to collect the supernatant, and concentrated under reduced pressure to extract the plant extract. 2 steps of obtaining a liquid; 3 steps of dissolving the lava sea salt dry powder obtained in step 1 in a ratio of 5 to 30% by weight relative to the weight in the plant extract liquid obtained in step 2, and then drying to obtain a lava sea salt dry powder containing a plant extract It is possible to obtain a lava sea salt containing lava sea salt or a plant extract of the present invention by a series of processes including.

The present invention provides a cosmetic composition containing lava sea salt and lava sea salt containing at least one selected from green tea, black tea, aloe, grapes, bananas and apple extracts obtained by the production method as an active ingredient.

The composition of the present invention may be included alone or mixed with other functional ingredients in an amount of 0.00001 to 50.00% by weight, preferably 0.1 to 5% by weight based on the cosmetic composition.

Cosmetics of the present invention comprises a composition selected from the group consisting of water-soluble vitamins, oil-soluble vitamins, polymer peptides, polymer polysaccharides, sphingolipids and seaweed extract.

The water-soluble vitamins may be any compound that can be incorporated into cosmetics, but preferably vitamin B1, vitamin B2, vitamin B6, pyridoxine, pyridoxine, vitamin B12, pantothenic acid, nicotinic acid, nicotinic acid amide, folic acid, vitamin C, vitamin H, and the like. Their salts (thiamine hydrochloride, sodium ascorbate salt, etc.) and derivatives (ascorbic acid-2-sodium phosphate salt, ascorbic acid-2-magnesium phosphate salt, etc.) may also be used in the water-soluble vitamins that can be used in the present invention. Included. The water-soluble vitamins can be obtained by conventional methods such as microbial transformation, purification from microorganism culture, enzyme or chemical synthesis.

The oil-soluble vitamin may be any compound that can be incorporated into cosmetics, but preferably vitamin A, carotene, vitamin D2, vitamin D3, vitamin E (d1-alpha tocopherol, d-alpha tocopherol, d-alpha tocopherol), and the like. And derivatives thereof (ascorbic palmitate, ascorbic stearate, ascorbic acid dipalmitate, dl-alpha tocopherol acetate, dl-alpha tocopherolvitamin E, DL-pantothenyl alcohol, D-pantothenyl alcohol, pantothenyl ethyl) Ethers, etc.) are also included in the oil-soluble vitamins used in the present invention. Oil-soluble vitamins can be obtained by conventional methods such as microbial transformation, purification of microorganism culture, enzyme or chemical synthesis.

The polymer peptide may be any compound as long as it can be incorporated into cosmetics. Preferably, collagen, hydrolyzed collagen, gelatin, elastin, hydrolyzed elastin, keratin, and the like can be given. Polymeric peptides can be purified and obtained by conventional methods such as purification from microbial cultures, enzymatic methods or chemical synthesis methods, or can be purified and used from natural products such as dermis and pig silk such as pigs and cattle.

The polymer polysaccharide may be any compound as long as it can be blended into cosmetics. Preferably, hydroxyethyl cellulose, xanthan gum, sodium hyaluronate, chondroitin sulfate or a salt thereof (sodium salt, etc.) may be mentioned. For example, chondroitin sulfate or its salt can be normally purified from a mammal or fish.

The sphingolipid may be any compound as long as it can be blended into cosmetics. Preferably, ceramide, phytosphingosine, sphingosaccharide lipid, etc. may be mentioned. Sphingo lipids can usually be purified from mammals, fish, shellfish, yeasts or plants by conventional methods or obtained by chemical synthesis.

The seaweed extract may be any compound as long as it can be blended into cosmetics. Preferably, the seaweed extract may include brown algae extract, red algae extract, green algae extract, and the like. Also, calginine, arginic acid, sodium arginate, Potassium arginate and the like are also included in the seaweed extract used in the present invention. Seaweed extract can be obtained by purification from seaweed by conventional methods.

In addition to the said essential component, you may mix | blend the cosmetics of this invention with the other components normally mix | blended with cosmetics as needed.

Other components that may be added include fats and oils, moisturizers, emollients, surfactants, organic and inorganic pigments, organic powders, ultraviolet absorbers, preservatives, fungicides, antioxidants, plant extracts, pH adjusters, alcohols, pigments, flavorings, Blood circulation accelerators, cold depressants, delimiters, purified water and the like.

Examples of the fat or oil component include ester fats, hydrocarbon fats, silicone fats, fluorine fats, animal fats, and vegetable fats and oils.

As ester fats and oils, glyceryl tri2-ethylhexanoate, cetyl 2-ethylhexanoate, isopropyl myristate, butyl mystinate, isopropyl palmitate, ethyl stearate, octyl palmitate, isocetyl isostearate, and stearic acid Butyl, ethyl linoleate, isopropyl linoleate, ethyl oleate, isocetyl acid isocetyl, isostyl acid isostearyl, isostaryl palmitate, octylate acid octyldodecyl, isostearic acid isetyl, diethyl sebacate, adipine Acid isopropyl, isoalkyl neopentane, tri (capryl, capric acid) glyceryl, trimethyl ethyl trimethylol propane, triisostearic acid trimethylol propane, tetra 2-ethylhexanoic penta erythritol Cetyl caprylate, lauric acid decyl, hexyl laurate, decyl myristin, myristin acid myristyl, myritic acid cetyl, stearyl stearate, decyl oleate, rininooleic acid , Isostearyl laurate, isotridecyl myristin, isocetyl palmitate, octyl stearate, isocetyl stearate, isodecate oleate, octylate decyl oleate, octyl dodecyl linoleate, isopropyl isopropyl acid, 2 -Cetostearyl ethylhexanoate, stearyl 2-ethylhexanoate, hexyl isostearate, ethylene glycol dioctanoate, ethylene glycol dioleate, propylene glycol dicapric acid, propylene glycol dicacapate, capric acid Propylene glycol, dicapric acid neopentyl glycol, dioctanoate neopentyl glycol, tricaprylic acid glyceryl, triundecyl glyceryl, triisopalmitinate glyceryl, triisostearate glyceryl, neopentane dodecyl Isostearyl octanoate, octyl isononate, hexyl decyl neodecanoate, octyl dodecyl neodecanoate, isocetyl isostearate, isostearyl isostearate, Sothete octylate, polyglycerol oleate, polyglycerine isostearate, triisocetyl citrate, triisoalkyl citrate, triisoctyl citrate, lauryl lactate, myritic lactate, octyl lactate, octyl lactate, tricitric acid Ethyl, acetyl triethyl citrate, acetyl tributyl citrate, trioctyl citrate, diisostearyl malic acid, 2-ethylhexyl hydroxystearate, di2-ethylhexyl succinate, diisobutyl adipicate, diisopropyl sebacinate, Dioctyl sebacate, cholesteryl stearate, cholesteryl isostearate, cholesteryl hydroxystearate, cholesteryl oleate, dihydrocholesteryl oleate, physteryl isostearate, phytic oleate, 12-Steloylhydroxystearate isocetyl, 12-Steloylhydroxystearate stearyl, 12-steal One hydroxy stearic acid and the like esters such as cetearyl source.

Hydrocarbon-based fats and oils, such as squalene, a liquid paraffin, alpha-olefin oligomer, isoparaffin, ceresin, paraffin, a liquid isoparaffin, polybutene, microcrystal wax, and a vaseline, etc. are mentioned as a hydrocarbon-type fats and oils.

Examples of the silicone-based oils and fats include polymethylsilicone, methylphenylsilicone, methylcyclopolysiloxane, octamethylpolysiloxane, decamethylpolysiloxane, dodecamethylcyclosiloxane, dimethylsiloxane, methylcetyloxysiloxane copolymer, dimethylsiloxane and methylsteoxysiloxane copolymer, and alkyl. Modified silicone oil, amino modified silicone oil and the like.

Perfluoro polyether etc. are mentioned as fluorine-based fats and oils.

Animal or vegetable oils include avocado oil, almond oil, olive oil, sesame oil, rice bran oil, soybean oil, soybean oil, corn oil, rapeseed oil, almond oil, palm kernel oil, palm oil, castor oil, sunflower oil, grape seed oil. , Cottonseed oil, Palm oil, Cucumber nut oil, Wheat germ oil, Rice germ oil, Shea butter, Walnut colostrum oil, Marker demia nut oil, Meadow home oil, Egg yolk oil, Uji, Horse oil, Mink oil, Orange rape oil, Jojoba oil And animal or plant fats and oils such as candeler wax, carnava wax, liquid lanolin and hardened castor oil.

Examples of the moisturizing agent include a water-soluble low molecular moisturizer, a fat-soluble molecular moisturizer, a water-soluble polymer, and a fat-soluble polymer.

Water-soluble low molecular humectants include serine, glutamine, sorbitol, mannitol, pyrrolidone-sodium carboxylate, glycerin, propylene glycol, 1,3-butylene glycol, ethylene glycol, polyethylene glycol B (polymerization degree n = 2 or more), polypropylene Glycol (polymerization degree n = 2 or more), polyglycerol B (polymerization degree n = 2 or more), lactic acid, lactic acid salt, etc. are mentioned.

Examples of the fat-soluble low molecular humectants include cholesterol and cholesterol esters.

Examples of the water-soluble polymer include carboxyvinyl polymer, polyasparaginate, tragacanth, xanthan gum, methyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethyl cellulose, water soluble chitin, chitosan, and dextrin. Can be.

Examples of the fat-soluble polymers include polyvinylpyrrolidone-eicosene copolymers, polyvinylpyrrolidone-hexadecene copolymers, nitrocellulose, dextrin fatty acid esters, polymer silicones, and the like.

Examples of the emollient include long-chain acyl glutamic acid cholesteryl esters, hydroxy stearic acid cholesterol, 12-hydroxystearic acid, stearic acid, rosin acid, lanolin fatty acid cholesteryl esters, and the like.

As surfactant, nonionic surfactant, anionic surfactant, cationic surfactant, amphoteric surfactant, etc. are mentioned.

Nonionic surfactants include self-emulsifying glycerin monostearate, propylene glycol fatty acid esters, glycerin fatty acid esters, polyglycerol fatty acid esters, sorbitan fatty acid esters, POE (polyoxyethylene), sorbitan fatty acid esters, POE sorbitan fatty acid esters, POE glycerin fatty acid ester, POE alkyl ether, POE fatty acid ester, POE hardened castor oil, POE castor oil, POEPOP (polyoxyethylene polyoxypropylene) copolymer, POEPOP alkyl ether, polyether modified silicone, lauric acid alkanolamide, Alkylamine oxide, hydrogenated soybean phospholipid, etc. are mentioned.

Anionic surfactants include fatty acid soaps, alpha-acyl sulfonates, alkyl sulfonates, alkyl allyl sulfonates, alkyl naphthalene sulfonates, alkyl sulfates, POE alkyl ether sulfates, alkylamide sulfates, alkyl phosphates, POE alkylphosphates, and alkylamides. Phosphates, alkyloylalkyltaurine salts, N-acylamino acid salts, POE alkyl ether carboxylate salts, alkyl sulfosuccinate salts, sodium alkyl sulfo acetates, acylated hydrolyzed collagen peptide salts, perfluoroalkyl phosphate esters, and the like. have.

As cationic surfactant, alkyltrimethylammonium chloride, stearyl trimethyl ammonium chloride, stearyl trimethyl ammonium bromide, cetostearyl trimethyl ammonium chloride, distearyl dimethyl ammonium chloride, stearyl dimethyl benzyl ammonium bromide, behenyl trimethyl ammonium chloride, chloride Benzalkonium, diethylaminoethyl stearate, dimethylaminopropyl stearate, lanolin derivatives, quaternary ammonium salts, and the like.

Examples of amphoteric surfactants include the carboxybetaine type, the amide betain type, the sulfobetain type, the hydroxysulfobetain type, the amide sulfobetain type, the phosphobetaine type, the aminocarboxylate type, the imidazoline derivative type, and the amideamine type. An amphoteric surfactant etc. are mentioned.

Organic and inorganic pigments include silicic acid, silicic anhydride, magnesium silicate, talc, sericite, mica, kaolin, bengala, clay, bentonite, titanium film mica, bismuth oxychloride, zirconium oxide, magnesium oxide, zinc oxide, titanium oxide, aluminum oxide Inorganic pigments such as calcium sulfate, barium sulfate, magnesium sulfate, calcium carbonate, magnesium carbonate, iron oxide, ultramarine blue, chromium oxide, chromium hydroxide, calamine and composites thereof; Polyamide, polyester, polypropylene, polystyrene, polyurethane, vinyl resin, urea resin, phenol resin, fluorine resin, silicon resin, acrylic resin, melamine resin, epoxy resin, polycarbonate resin, divinylbenzene, styrene copolymer, Organic pigments such as silk powder, cellulose, CI pigment yellow, CI pigment orange, and composite pigments of these inorganic pigments and organic pigments;

As organic powder, Metal soaps, such as a calcium stearate; Alkyl phosphate metal salts such as sodium cetylinate, zinc lauryl acid and calcium laurate; Acylamino acid polyvalent metal salts such as N-lauroyl-beta-alanine calcium, N-lauroyl-beta-alanine zinc, and N-lauroylglycine calcium; Amide sulfonic acid polyvalent metal salts, such as N-lauroyl-taurine calcium and N-palmitoyl-taurine calcium; N-epsilon-lauroyl-L-lysine, N-epsilon-palmitolyzine, N-alpha-paratoylol nitin, N-alpha-lauroyl arginine, N-alpha-cured fatty acid acyl arginine -Acyl basic amino acid; N-acyl polypeptides, such as N-lauroyl glycyl glycine; Alpha-amino fatty acids such as alpha-aminocaprylic acid and alpha-aminolauric acid; Polyethylene, polypropylene, nylon, polymethyl methacrylate, polystyrene, divinylbenzene-styrene copolymer, ethylene tetrafluoride and the like.

Examples of the ultraviolet absorber include paraaminobenzoic acid, ethyl paraaminobenzoate, amyl paraaminobenzoic acid, octyl paraaminobenzoate, ethylene glycol salicylate, phenyl salicylate, octyl salicylate, benzyl salicylate, butylphenyl salicylate, homomentyl salicylic acid and benzyl cinnamic acid. , Paramethoxy cinnamic acid-2-ethoxyethyl, paramethoxy cinnamic acid octyl, diparamethoxy cinnamic acid mono-2-ethylhexaneglyceryl, paramethoxy cinnamic acid isopropyl, diisopropyl diisopropyl cinnamic acid ester mixture, wuro Canonic acid, ethyl urokanoate, hydroxymethoxybenzophenone, hydroxymethoxybenzophenonesulfonic acid and salts thereof, dihydroxymethoxybenzophenone, dihydroxymethoxybenzophenone sodium sulfonate, dihydroxybenzophenone , Tetrahydroxybenzophenone, 4- tert -butyl-4'-methoxydibenzoylmethane, 2,4,6-trianilino- p- (carbo-2'-ethylhexyl-1'-oxy) -1 , 3,5-triazine, 2- (2-hi And the like can be mentioned hydroxy-5-methylphenyl) benzotriazole.

As fungicides, hinokithiol, trichloric acid, trichlorohydroxydiphenyl ether, chlorhexidine gluconate, phenoxyethanol, resorcin, isopropylmethylphenol, azulene, salicylic acid, ginxitlionone, benzalkonium chloride, photosensitive Sodium No. 301, sodium mononitroguicol, undecylenic acid, and the like.

Examples of the antioxidant include butylhydroxyanisole, propyl gallic acid, and erythorbic acid.

Examples of the pH adjuster include citric acid, sodium citrate, malic acid, sodium malate, fmaric acid, sodium pmarate, succinic acid, sodium succinate, sodium hydroxide, sodium dihydrogen phosphate, and the like.

Examples of the alcohol include higher alcohols such as cetyl alcohol.

Moreover, the compounding component which may be added other than this is not limited to this, Moreover, Although all said components can be mix | blended within the range which does not impair the objective and effect of this invention, Preferably it is 0.01-5% weight percentage with respect to a total weight, More preferably 0.01-3% by weight.

The cosmetic of the present invention may take the form of a solution, an emulsion, a viscous mixture, or the like.

Ingredients included in the cosmetic composition of the present invention may include components commonly used in cosmetic compositions in addition to the compound as an active ingredient, for example, conventional auxiliary agents such as stabilizers, solubilizers, vitamins, pigments and flavorings. And carriers.

The cosmetic composition of the present invention may be prepared in any formulation commonly prepared in the art, and includes, for example, milky lotion, cream, lotion, pack, foundation, lotion, essence, hair cosmetic, and the like.

Specifically, the cosmetic composition of the present invention skin lotion, skin softener, skin toner, astringent, lotion, milk lotion, moisturizing lotion, nutrition lotion, massage cream, nutrition cream, moisturizing cream, hand cream, foundation, essence, nutrition essence, Formulations of packs, soaps, cleansing foams, cleansing lotions, cleansing creams, body lotions and body cleansers.

When the formulation of the present invention is a paste, cream or gel, animal carriers, vegetable fibers, waxes, paraffins, starches, tracantes, cellulose derivatives, polyethylene glycols, silicones, bentonites, silicas, talc or zinc oxide, etc. may be used as carrier components. Can be.

When the formulation of the present invention is a powder or a spray, lactose, talc, silica, aluminum hydroxide, calcium silicate or polyamide powder may be used, in particular in the case of a spray, additionally chlorofluorohydrocarbon, propane Propellant such as butane or dimethyl ether.

When the formulation of the present invention is a solution or emulsion, a solvent, solvating or emulsifying agent is used as the carrier component, such as water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, propylene glycol, 1 Fatty acid esters of, 3-butylglycol oil, glycerol aliphatic ester, polyethylene glycol or sorbitan.

When the dosage form of the present invention is a suspension, liquid carrier diluents such as water, ethanol or propylene glycol, suspending agents such as ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester, microcrystalline Cellulose, aluminum metahydroxy, bentonite, agar or tracant and the like can be used.

When the formulation of the present invention is a surfactant-containing cleansing, the carrier component is an aliphatic alcohol sulfate, an aliphatic alcohol ether sulfate, a sulfosuccinic acid monoester, an isethionate, an imidazolinium derivative, a methyltaurate, a sarcosinate, a fatty acid amide. Ether sulfates, alkylamidobetaines, aliphatic alcohols, fatty acid glycerides, fatty acid diethanolamides, vegetable oils, linolin derivatives or ethoxylated glycerol fatty acid esters and the like can be used.

The present invention provides a bath composition comprising lava sea salt and lava sea salt containing one or more selected from green tea, black tea, aloe, grape, banana and apple extract as active ingredients.

The bathing agent of the present invention can be used for half body bath, systemic bath, face wash and foot bath, the amount of use varies depending on the use, but roughly 50-200g per 100ℓ of water when used in skin irritation or active oxygen It is sufficient in terms of its ability to remove and antioxidant.

As the bathing agent defined in the present invention has no skin irritation at all, it can be widely and safely used for not only normal skin but also sensitive skin, so that it can be commercialized in cosmetics and quasi-drugs for the purpose of half body bath, whole body bath, face wash and foot bath.

The present invention provides a soap composition containing lava sea salt and lava sea salt containing at least one selected from green tea, black tea, aloe, grape, banana and apple extract as an active ingredient.

The soap composition of the present invention can be used in combination with a composition selected from the group consisting of a base, a moisturizing agent, an antioxidant, a light shielding agent, a cleaning agent, and purified water as it is exemplified below.

The composition according to the invention contains 0.01 to 10% by weight relative to the total weight, preferably 0.05 to 5% by weight, more preferably 0.1 to 2% by weight.

The base is a fat or oil which is a raw material of soap, and contains a hydrophobic hydrocarbon portion and a hydrophilic carboxyl group that is soluble in water. Typically, fats and oils are weak alkali salts of higher fatty acids, which are acid alkali neutralization reactions of higher fatty acids with 8 to 20 carbon atoms derived from animal and vegetable fats and oils such as tallow, lard, fish oil, palm oil, palm oil and palm kernel oil. The mixture of the obtained weak alkali salt is used, Preferably vegetable palm oil is used. Soaps vary in their properties depending on the fatty acids they contain. Saturated fatty acid soaps with less than 12 carbons are very hard and have good solubility stability. If above, the solubility decreases, but the washing power and the bubble power become strong. Since the base of the soap actually used is not a fatty acid of one element, but a mixture of several fatty acids, the soap is mixed according to the purpose and manufactured in consideration of firmness, solubility, foaming power, washing power, salting power, and preservation.

Moisturizers are intended to maintain moisture and supply various nutrients to the skin and hair after use, and moisturizers that can be used in this field are commonly available. Preferably glycerin, propylene glycol (PG), butylene glycol (BG), hexylene glycol (HG), urea, dexpanthenol, isopentyldiol and One or more mixtures selected from pyrrolidone carboxylic acid and salts thereof (sodium) are used.

As antioxidants, tocopherol acetate, butylated hydroxy anisole (BHA), ascorbyl palmitate, and eddronic acid are used.

The light-shielding agent decolorizes and prevents the color change of the soap itself and keeps the soapy bird. Titanium oxide, dipropylene glycol salicylate, and methyl salicylate are used as the light-shielding agent.

The cleaning agent imparts a washing effect and foaming power of the soap to improve the feeling of use of the soap. As a detergent, cocamidopropyl betaine containing an alkyl group of C8 to C22, an amphoteric surfactant, coco-betaine, alkyl betaine, cocamide DEA, and cocamide MEA (cocamide MEA), glyceryl cocoate is used.

Purified water is used to dissolve the solid component in the vehicle, and 2 to 4 times the weight ratio of the solid component is added.

In addition, additives such as preservatives, pH adjusters, flavorings, dyes, hardness enhancers, etc. may be further added to those soap compositions containing the composition by those skilled in the art.

As a preservative, methyl paraben, propyl paraben, etc. are mentioned.

Examples of the pH regulator include citric acid, sodium citrate, malic acid, sodium malate, fmaric acid, sodium pmamate, succinic acid, sodium succinate, sodium hydroxide, sodium dihydrogen phosphate, and the like.

Examples of the hardness enhancer include polyethylene glycol (PEG) -4000.

In addition to the said component, you may mix | blend with the soap composition of this invention the other component normally mix | blended with a soap composition as needed.

In addition, the compounding component which may be added other than this is not limited to this, Moreover, Although all said components can be mix | blended within the range which does not impair the objective and effect of this invention, Preferably it is 0.01-5 weight% with respect to gross weight, More Preferably it is 0.01-3 weight% compounding.

In addition, the type of soap containing the soap composition of the present invention includes a cosmetic soap, powdered soap, medicated soap, water soap, cream soap, paper soap, bath soap, beauty soap and the like.

The present invention provides a composition for oral cavity containing lava sea salt and lava sea salt containing at least one selected from green tea, black tea, aloe, grape, banana and apple extract.

The composition of the present invention comprises 0.05 to 5% by weight, preferably 0.1 to 3% by weight relative to the total weight of the composition for oral cavity.

The composition for oral cavity of this invention is not specifically limited in the formulation, For example, it can have formulations, such as a toothpaste, a mouthwash, and a mouthwash.

In addition, the lava sea salt or lava sea salt containing the extract constituting the composition for oral cavity of the present invention can be arbitrarily selected and blended by those skilled in the art according to the formulation of the other ingredients, and according to the desired effect. .

For example, toothpaste is composed of abrasives, caking agents, moisturizers, active ingredients, foaming agents, sweeteners, and flavoring components. The abrasive components include dicalcium phosphate dihydrate and anhydrides, tricalcium phosphate, and carbonic acid. 20 to 90 weight percent of one or more selected from calcium, calcium pyrophosphate, aluminum hydroxide, silicic anhydride, aluminum silicate, insoluble sodium metaphosphate, magnesium triphosphate, magnesium carbonate, calcium sulfate, polymethyl acrylate, and other synthetic resins It is contained in the amount of%.

In the case of the pasty composition, gums such as tares, various cellulose derivatives, xanthan gum, and tragacanth gum, polyvinyl alcohol, sodium polyacrylate, and polyacrylic acid / maleic acid copolymer And at least one selected from organic binders such as synthetic polymer derivatives such as carboxyvinyl polymer and inorganic binders such as silica and laponite in an amount of 0.3 to 5% by weight.

In addition, in the preparation of paste-like and liquid oral compositions in toothpaste, sorbitol, glycerin, ethylene glycol, propylene glycol, polyethylene glycol, polypropylene glycol and the like are usually contained in an amount of 10 to 70% by weight as a moisturizing agent.

Oral composition of the present invention includes menthol (Mentol), anetol (Anetol), Eugenol (Eugenol), Limonene (Limonene), Ocimene (n-Dodecyl Alcohol), Citronone Citronenol, α-Terpineol, Methyl salycilate, Methyl Acetate, Citronelyl Acetate, Cineol, Linarol ( Linalool, ethylinalol, vanillin, thymol, spearmint oil, sage oil, rosemary oil, cinnamon oil, etc. It may be contained in an amount of less than or equal to% by weight, preferably in an amount of 0.5 to 5% by weight. In addition, sweeteners such as sodium saccharin, stevioside, asparatam, D-Xylose and the like may be contained in an amount of 1% by weight or less, preferably in an amount of 0.01 to 0.5% by weight. .

In addition, as an active ingredient, fluoride with alkali metal monofluoro phosphates such as trichloric acid, chlorohexidine, benzetonium chloride, benzalkonium chloride, cetylpyridium chloride, cationic fungicides, sodium monofluorophosphate and potassium monofluorophosphate, etc. Fluorides such as sodium and tin fluoride, trinexamic acid, epsilon amino caproic acid, aluminum chlorohydroxy allantoin, dihydrocholestanol, glytiric acid, glycerophosphate, sodium chloride, water-soluble inorganic phosphate compounds, ascorbic acid (Sodium), dl-tocopherol acetate, xylitol, pyridoxine hydrochloride, polyvinyl pyrrolidone and the like, or one or two or more kinds thereof can be selected and blended.

In addition, N-acyl sarcos such as sodium lauryl sulfate, sodium alkyl sulfates such as myristyl sulfate, sodium N-Lauroyl sarcosinate, and sodium N-myristyl sarcosinate Anionic surfactants such as sodium N-acyl sarcosinate; Sugar-derived fatty acid esters such as sugar fatty acid esters, maltose fatty acid esters, lactose fatty acid esters, polyoxyethylene hardened castor oil, polyoxyethylene higher alcohol ethers, polyoxy ethylene polyoxy propylene copolymers, polyoxy ethylene Nonionic surfactants such as polypropylene fatty acid esters; N-alkyl di aminoethylglycines, such as N-lauryl di aminoethylglycine, N-myristyl di aminoethylglycine, N-alkyl-N-carboxy methyl ammonium betaine, 2-alkyl-1-hydroxy ethyl imida One or more zwitterionic surfactants, such as chlorine betaine sodium, are mixed and used as a blowing agent. The amount used is in an amount of 0.01 to 5% by weight, preferably in an amount of 0.05 to 3% by weight.

Hereinafter, the present invention will be described in detail by the following Examples and Experimental Examples. However, the following Examples and Experimental Examples are merely illustrative of the present invention, and the content of the present invention is not limited by the following Examples and Experimental Examples.

Example  One. Lava sea salt  Produce

Example  1-1. Lava sea salt  Manufacture (1)

A 150m underground was excavated at Handong-ri, Gujwa-eup, Bukjeju-gun, Jeju-do, and 1kg of lava seawater taken from 44.35m underground (average sea level) was filtered using a sterile filter. Concentrated in vacuo to give a high concentration of lava salt water, and then dried in a hot air dryer to obtain 32 g of lava salt (yield 3.2%).

Example  1-2. Lava sea salt  Manufacture (2)

Excavated 150m underground in Handong-ri, Gujwa-eup, Bukjeju-gun, Jeju-do, Korea, and filtered 1 kg of lava saltwater taken from the underground (average sea level) 86.35 m using a sterile filter to reduce the deconcentrated lava saltwater to 100 g. Concentrated in vacuo to give a high concentration of lava saltwater, and dried in a hot air dryer to obtain 35 g (3.5% yield) of lava salt.

Example  1-3. Lava sea salt  Manufacture (3)

A 150m underground was excavated at Handong-ri, Gujwa-eup, Bukjeju-gun, Jeju-do, and 1kg of lava seawater taken from 126.35m underground (based on average sea level) was filtered using a sterile filter. Concentrated in vacuo to give a high concentration of lava saltwater, and dried in a hot air dryer to obtain 36 g (yield 3.6%) of lava salt.

Example  2. Functionality with Green Tea Extract Lava sea salt  Preparation of the composition

1 kg of dry green tea was immersed in 10 kg of 70% ethanol aqueous solution, refluxed for 3 hours, and extracted firstly, and the resultant was filtered to obtain a solid component and a liquid component, respectively. Then, the solids were re-extracted under the same conditions with 5 kg of the same solvent to obtain a liquid component, then mixed with the previously obtained liquid component, and concentrated to about 1 kg in a vacuum concentrator. Purified water was added to the obtained concentrate, diluted three times, and the precipitate formed after standing at room temperature for 1 hour was filtered off. The resulting green tea extract was dissolved in 500 g of lava salt salt obtained in Example 1, and the resulting solution was concentrated to give a high concentration of salt water. After the preparation, it was dried in a hot air dryer to obtain about 610 g of functional lava sea salt containing the green tea extract to be obtained in the present invention.

Example  3. Functionality Containing Black Tea Extract Lava sea salt  Preparation of the composition

1 kg of dried black tea was extracted in the same manner as in Example 2 to obtain about 650 g of functional lava sea salt containing the black tea extract to be obtained in the present invention.

Example  4. Functionality Containing Aloe Extract Lava sea salt  Preparation of the composition

1 kg of aloe was extracted in the same manner as in Example 2 to obtain about 610 g of functional lava sea salt containing the aloe extract to be obtained in the present invention.

Example  5. Functionality containing grape extract Lava sea salt  Preparation of the composition

1 kg of grapes were extracted in the same manner as in Example 2 to obtain about 580 g of functional lava sea salt containing the grape extract to be obtained in the present invention.

Example  6. Functionality with Banana Extract Lava sea salt  Preparation of the composition

1 kg of the banana powder was extracted in the same manner as in Example 2 to obtain about 1,000 g of functional lava sea salt containing the banana extract to be obtained in the present invention.

Example  7. Functionality containing apple extract Lava sea salt  Preparation of the composition

Using 1 kg of apple powder was extracted in the same manner as in Example 2 to obtain about 1,100 g of functional lava sea salt containing the apple extract to be obtained in the present invention.

Example  8. Functionality with Green Tea and Black Tea Extract Lava sea salt  Preparation of the composition

1 kg of green tea and 1 kg of black tea were extracted in the same manner as in Example 2 to obtain about 1190 g of functional lava sea salt containing the green tea and black tea extract to be obtained in the present invention.

Example  9. Functional Containing Aloe and Grape Extracts Lava sea salt  Preparation of the composition

1 kg of aloe and 1 kg of grapes were extracted in the same manner as in Example 2 to obtain 1100 g of functional lava sea salt containing the aloe and grape extract to be obtained in the present invention.

Example  10. Functionality containing banana and apple extracts Lava sea salt  Preparation of the composition

1 kg of bananas and 1 kg of apples were used to extract 2050 g of functional lava sea salt containing the banana and apple extract to be obtained in the same manner as in Example 2.

Example  11.Functionality containing green tea, aloe and apple extract Lava sea salt  Preparation of the composition

1 kg of green tea, 1 kg of aloe and 1 kg of apple were extracted in the same manner as in Example 2 to obtain 2100 g of functional lava sea salt containing green tea, aloe and apple extract to be obtained in the present invention.

Example  12. Functionality Containing Black Tea, Grape and Banana Extracts Lava sea salt  Preparation of the composition

1 g of black tea, 1 kg of grapes and 1 kg of bananas were extracted in the same manner as in Example 2 to obtain 2010 g of functional lava sea salt containing black tea, grape and banana extract to be obtained in the present invention.

Experimental Example  One. Moisturizing  Measure

The moisturizing effect on the composition of the present invention was measured as follows by using a coneneometer CM 825 (Corneometer CM 825, Courate, Khazaka), distilled water was used as a control.

Five women in their twenties were divided into 8 x 2 cm 2 upper arms and 8 compartments, and washed several times with water to remove water without irritation. After 15 minutes, samples were evenly applied by dropping 10 μl into each compartment. After 2 hours, 5 measurements were taken per compartment using a coneometer. Room temperature was carried out in a constant temperature and humidity room of 21 ± 2 ℃, relative humidity 50 ± 5%. The measured value was used by averaging the value obtained by measuring 5 times, and the result is shown in Table 1 using following formula (1).

Moisturizing Power (Corneometer Value) = S-△ S

  S: Cone meter before sample application

△ S: Cone meter after sample application for 2 hours

As a result of the experiment, as shown in Table 1, it was confirmed that the composition obtained in Examples 1 to 12 was superior in moisturizing power than distilled water used as a control.

Experimental Example   2. Cytotoxicity Experiment

MTT assay [3- (4,5-dimethylthylthiazol-2-yl) -2,5- by culturing fibroblasts (Human Skin fibroblast, ATCC, CRL-2310) to examine the cytotoxicity of the composition of the present invention diphenyltetrazolium bromide reduction test] was performed using the method described in the literature (T. Mosmann, J. Immunol. Methods , 65 , p55, 1983).

2-1. Cell culture

Human fibroblasts were seeded in 24-well culture plates at a concentration of 5 × 10 4 cells / ml. Medium was used DMEM (Dubelcco'S Modified Eagle Medium; BRL, USA) containing 10% bovine serum.

24 hours after inoculation, it was replaced with DMEM containing 2% of bovine serum, and the compositions obtained in Examples 1 to 7 were added at concentrations of 50, 100 and 200 ug / ml, followed by 37 ° C., 5% CO for 3 days. Incubated in ₂ incubators. Control was purified water.

2-2. Cell viability measurement

The supernatant of the cultured cells of Experimental Example 2-1 was removed and again washed by adding 200 ul of 5% PBS (phosphate buffered saline).

After MTT (Sigma, USA) solution was added 1.0 ml per well, MTT was removed after 4 hours, DMSO was added 1.0 ml per well, and then incubated at 37 ° C. for 12 hours, and the absorbance was measured at 570 nm. Survival rate of the cells was calculated using the following equation (2).

Cell viability = Cell OD570nm value / control OD570nm value X 100

As a result of the experiment, it was found that the composition obtained in Examples 1 to 7 was not toxic to fibroblasts at a concentration range of 200 ug / ml (see FIG. 1).

Thereafter, the experiment was conducted with the highest concentration of 200 ug / ml in the cell experiment.

Experimental Example  3. iNOS Activity inhibition experiment

Activity of Inducible Nitric Oxide Synthase (iNOS) for the Inhibitory Effect of Inflammation Induced Using Raw264.7 Cells (TIB-71, ATCC, USA) Was measured using the method described in the literature (Green L. et al., Anal. Biochem., 126 , pp131-138, 1982).

Suspend 8 x 105 cells in 10% FBS-DMEM (Fetal Bovine Serum, Fetal Bovine Serum, Dulbecco's Modified Eagle Medium, Gibcosa) medium containing no phenol-red and inoculate them in 24-well culture plates. Attached. After one day, the sample was incubated for 18 hours by treatment at a concentration of 200 ug / ml, followed by incubation for 24 hours by treatment with 1 ug / ml lipopolysaccharide (LPS, lipopolysaccharide, Sigma). Thereafter, the supernatant was collected, 100 ul each was added to a 96-well plate, and the same amount of Gries' reagent (Griess reagent, Sigma Co., Ltd.) was added thereto, and the mixture was gently shaken at room temperature for 10 minutes to measure absorbance at 570 nm. A calibration curve was prepared using sodium nitrite as a standard, and the amount of nitric oxide produced in each culture was determined. The yield of each sample was determined using the amount of nitric oxide produced in the lipopolysaccharide-treated group as 100%, and the control was used only as a medium without LPS treatment.

As a result of the experiment, as shown in Table 2, it was confirmed that the compositions obtained in Examples 1 to 7 significantly inhibit the activity of iNOS.

Experimental Example  4. PGE ₂ , IL-6 and IL-8 Production Inhibitory Effects

Production of PGE ₂ (Prostaglandin E ₂ ), IL-6 (Interleukin-6), and IL-8 (Interleukin-8) to investigate the inhibitory effect of inflammation using fibroblasts (Human Skin fibroblast, ATCC, CRL-2310) Was measured as follows.

Human fibroblasts were seeded in 6-well culture plates at a density of 1 × 10 5 cells and incubated in a 37 ° C., 5% CO ₂ incubator for 24 hours. After treatment with 500 μM of H ₂ O ₂ in a well for 24 hours stimulation, the samples were treated by concentration, reacted for 48 hours, the cultures were collected, and ELISA analysis was performed. Savorol (α-bisaborol) was used as a control. PGE ₂ was used assay kit from Asay Design, IL-6 and IL-8 was used as Endogen kit, and was tested according to the method specified in each company's manual. As a control group, alpha bisabolol (α-bisabolol), which is a material frequently used as an anti-inflammatory and stimulant, was used. The inhibitory effect was expressed by the following Equation 3.

Inhibitory effect = 1- (sample-control) / (H ₂ O ₂ -control) X100

As a result of the experiment, as shown in Table 3, it was confirmed that the composition obtained in Examples 1 to 12 inhibited the production of PGE ₂ , IL-6 and IL-8.

Experimental Example  5. Antimicrobial effect against causative agent

5-1. Cultivation of Strains

Streptococcus mutans were inoculated in BHI (brain heart infusion) broth, and then recovered three times in a 37 ° C shaking incubator to recover the activity, and the recovered strains were divided into agar plate medium at 37 ° C. Incubated for 24 hours in anaerobic conditions.

5-2. Antibacterial Experiment

After diluting the cavities precultured in Experimental Example 5-1 to 106 CFU / ml, each 0.1 ml each put into a test tube and 2.5 ml of top agar maintained at 45 ℃ was mixed well, BHI Pour over agar. When the surface was hardened, a paper disk (diameter 8 mm) was placed to absorb the composition obtained in Examples 1 to 10 and 50 ul of salts in which the salt of natural salt was dissolved at a concentration of 1 mg / ml as a control and incubated for 24 hours in an incubator at 37 ° C. After that, the diameter of the clear zone was measured and compared.

As a result of the experiment, as shown in Table 4, it was confirmed that the composition obtained in Examples 1 to 7 shows a good anti-caries activity compared to the control.

Experimental Example  6. Sensory analysis through clinical

For women aged 25 to 45 years, the sensory analysis of saline dissolved in the composition of the present invention proceeded as follows.

The subjects were 20 females up to 45 years of age, and the experiment was performed after one hour in a constant temperature and humidity room with an internal temperature of 21 ± 2 ° C. and a relative humidity of 50 ± 5% without makeup. Saline dissolved in purified water at a concentration of 10 mg / ml of the composition obtained in Examples 1 to 10 was used, and purified water was used as a control. The subject was not provided with information about the sample, and was randomly sprayed into the cheeks by 20 ml. After spraying the brine, the degree of feeling of refreshment, softness and suppleness felt after 5 minutes was surveyed. Skin sensation was determined by the inspection criteria of Table 5 below, and the skin sensation of saline for the compositions obtained in Examples 1 to 7 is shown in Table 6 below.

Formulation examples of cosmetics, soaps and oral compositions comprising lava sea salt and lava sea salt containing one or more selected from green tea, black tea, aloe, grapes, bananas and apple extracts of the present invention, but the present invention is limited thereto. It is not intended to be, but to explain in detail.

Formulation example  1. Flexible Lotion

number Raw material Content (% by weight) One Lava sea salt 0.5 2 Butylene Glycol 4.0 3 glycerin 8.0 4 Carboxy Vinyl Polymer 0.06 5 Disodium ethylenediamineteracetic acid 0.01 6 ethanol 7.0 7 Triethanolamine 0.2 8 Sorbitan monostearate 0.8 9 Hydrogenated  Caster oil 0.4 10 Phenyltrimethicone 3.5 11 Paraoxybenzoic acid propyl 0.2 12 Methyl paraoxybenzoate 0.2 13 Purified water Remaining amount system 100.0

Formulation example  2. Nutritional Cosmetics

number Raw material Content (% by weight) One Lava salt containing green tea extract 0.5 2 Stearic acid 1.0 3 Cetyl alcohol 1.0 4 Glyceryl Monostearate 1.0 5 Polyoxyethylene sorbitan monostearate 1.0 6 Sorbitan sesquioleate 1.0 7 Liquid paraffin 4.0 8 Carlylic Of Capric triglyceride 4.0 9 Squalane 3.0 10 Carboxy Vinyl Polymer 0.1 11 Butylene glycol 5.0 12 Triethanolamine 0.2 13 Paraoxybenzoic acid propyl 0.2 14 Methyl paraoxybenzoate 0.2 15 Purified water Remaining amount system 100.0

Formulation example  3. Nutrition Cream

number Raw material Content (% by weight) One   Lava salt containing banana extract 0.5 2 Stearic acid 2.0 3 Cetyl alcohol 2.0 4 Glyceryl Monostearate 2.0 5 Polyoxyethylene sorbitan monostearate 0.5 6 Sorbitan sesquioleate 0.5 7 Glyceryl Monostearate / Glyceryl Stearate / Polyoxyethylene Stearate 1.0 8 Wax 1.0 9 Liquid paraffin 4.0 10 Carlylic Of Capric triglyceride 4.0 11 Squalane 4.0 12 Carboxy Vinyl Polymer 0.3 13 Butylene glycol 5.0 14 glycerin 3.0 15 Triethanolamine 0.5 16 Paraoxybenzoic acid propyl 0.2 17 Methyl paraoxybenzoate 0.2 18 Purified water Remaining amount system 100.0

Formulation example  4. Essence

number Raw material Content (% by weight) One Lava salt containing aloe extract 0.5 2 Cytostolol 1.70 3 Polyglyceryl 2-oleate 1.50 4 Ceramide 0.7 5 Ceteares-4 1.2 6 cholesterol 1.5 7 Dicetylphosphate 0.4 8 Concentrated glycerin 5.0 9 Sunflower oil 15.0 10 Carboxy Vinyl Polymer 0.2 11 Xanthan Gum 0.2 12 antiseptic a very small amount 13 Spices a very small amount 14 Purified water Remaining amount system 100.0

Formulation example  5. Toothpaste

number Raw material Content (% by weight) One Lava salt containing grape extract 1.00 2 glycerin 20.40 3 Garlic Gum 0.80 4 Ion exchange water 10.37 5 Methylparaben 0.10 6 Propylparaben 0.02 7 Sodium saccharin 0.20 8 Sorbitol (70%) 13.00 9 Dicalcium Phosphate Dihydrate 34.00 10 Dicalcium Phosphate Anhydride 14.00 11 Calcium carbonate 5.00 12 Sodium Lauryl Sulfate 1.20 system 100.0

Formulation example  6. Mouthwash

number Raw material Content (% by weight) One Lava sea salt 1.6 2 Sodium Lauryl Sulfate 0.6 3 Sodium Lauroyl Acid 1.5 4 Sorbitol solution 30.0 5 Polyethylene glycol 10.0 6 Sodium monofluorophosphate 0.76 7 Ethyl alcohol 15.0 8 Distilled water Remaining amount system 100.0

Formulation example  7. Soap

number Raw material Content (% by weight) One Lava salt containing black tea extract 1.5 2 Butylated hydroxy toluene 0.05 3 Ethylenediaminetetraacetic acid 0.05 4 Spices 1.49 5 dyes 0.01 6 Titanium oxide 0.2 7 Vitamin E Acetate 2.0 8 Polyethylene glycol 6.0 9 Toilet soap (moisture 13 parts) Remaining amount system 100

As described above, the lava sea salt of the present invention and lava sea salt containing one or more selected from green tea, black tea, aloe, grape, banana and apple extracts exhibits skin moisturizing, skin elasticity and anti-inflammatory effects. It can be used as a composition for the oral cavity having a protective and improving cosmetic, bath, soap composition and caries prevention effect.

Claims (20)

Excavated 100 to 200 m underground in Handong-ri, Gujwa-eup, Bukjeju-gun, Jeju Island, and sterilized the lava seawater taken from 30 to 150 m underground (based on average sea level) using a sterile filter. Or a lava sea salt obtained by a method such as gout drying and a lava sea salt containing at least one selected from green tea, black tea, aloe, grape, banana, and apple extract as an active ingredient. The cosmetic composition according to claim 1, which contains lava sea salt. The cosmetic composition according to claim 1, which contains lava sea salt and green tea extract. The cosmetic composition according to claim 1, which contains lava sea salt and black tea extract. The cosmetic composition according to claim 1, which contains lava sea salt and aloe extract. The cosmetic composition according to claim 1, which contains lava sea salt and grape extract. The cosmetic composition according to claim 1, which contains lava sea salt and a banana extract. The cosmetic composition according to claim 1, which contains lava sea salt and an apple extract. The cosmetic composition according to claim 1, which contains lava sea salt, green tea and black tea extract. The cosmetic composition according to claim 1, which contains lava sea salt, aloe and grape extract. The cosmetic composition according to claim 1, which contains lava sea salt, banana and apple extract. The cosmetic composition according to claim 1, which contains lava sea salt, green tea, aloe and apple extract. The cosmetic composition according to claim 1, which contains lava sea salt, black tea, grape and banana extract. delete The skin lotion, skin softener, skin toner, astringent, lotion, wheat lotion, moisturizing lotion, nutrition lotion, massage cream, nutrition cream, moisturizing cream, hand cream, foundation, essence, nutrition essence, pack, Cosmetic composition, wherein the cosmetic composition is at least one formulation selected from the group consisting of soap, cleansing foam, cleansing lotion, cleansing cream, body lotion and body cleanser. delete The bath composition according to claim 1, comprising lava sea salt and lava sea salt containing at least one selected from green tea, black tea, aloe, grapes, bananas and apple extracts. The soap composition according to claim 1, comprising lava sea salt and lava sea salt containing one or more selected from green tea, black tea, aloe, grape, banana, and apple extract as active ingredients. The composition for oral cavity according to claim 1, which contains lava sea salt and lava sea salt containing at least one selected from green tea, black tea, aloe, grape, banana, and apple extract as active ingredients. 20. The oral composition according to claim 19, which is at least one formulation selected from the group consisting of a toothpaste, a mouthwash and a mouthwash.

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