KR100375905B1 - 디니트로톨루엔의제조방법 - Google Patents
디니트로톨루엔의제조방법 Download PDFInfo
- Publication number
- KR100375905B1 KR100375905B1 KR1019950024653A KR19950024653A KR100375905B1 KR 100375905 B1 KR100375905 B1 KR 100375905B1 KR 1019950024653 A KR1019950024653 A KR 1019950024653A KR 19950024653 A KR19950024653 A KR 19950024653A KR 100375905 B1 KR100375905 B1 KR 100375905B1
- Authority
- KR
- South Korea
- Prior art keywords
- acid
- weight
- nitric acid
- phase
- weight percent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4428462A DE4428462A1 (de) | 1994-08-11 | 1994-08-11 | Verfahren zur Herstellung von Dinitrotoluol |
| DEP4428462.4 | 1994-08-11 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR960007531A KR960007531A (ko) | 1996-03-22 |
| KR100375905B1 true KR100375905B1 (ko) | 2003-04-21 |
Family
ID=6525455
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019950024653A Expired - Fee Related KR100375905B1 (ko) | 1994-08-11 | 1995-08-10 | 디니트로톨루엔의제조방법 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5689018A (cg-RX-API-DMAC7.html) |
| EP (1) | EP0696571B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP3631814B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR100375905B1 (cg-RX-API-DMAC7.html) |
| CN (1) | CN1075054C (cg-RX-API-DMAC7.html) |
| BR (1) | BR9503612A (cg-RX-API-DMAC7.html) |
| CA (1) | CA2155562C (cg-RX-API-DMAC7.html) |
| DE (2) | DE4428462A1 (cg-RX-API-DMAC7.html) |
| ES (1) | ES2144074T3 (cg-RX-API-DMAC7.html) |
| TW (1) | TW314508B (cg-RX-API-DMAC7.html) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19521614A1 (de) * | 1995-06-14 | 1996-12-19 | Bayer Ag | Verfahren zur Herstellung von Dinitrotoluol |
| DE10055359C1 (de) * | 2000-11-08 | 2002-03-28 | Bayer Ag | Kontinuierliches isothermes Verfahren zur Herstellung von Mononitrotoluolen |
| DE10345601A1 (de) * | 2003-09-29 | 2005-05-12 | Basf Ag | Verfahren zur Entfernung von Nitrokresolen aus Abwasser der Mononitrotoluolherstellung und zur weiteren Verwendung des Extraktes |
| DE102004005913A1 (de) | 2004-02-05 | 2005-08-25 | Basf Ag | Verfahren zur Herstellung von Dinitrotoluol |
| US7041858B1 (en) * | 2005-02-09 | 2006-05-09 | Bayer Materialscience Llc | Process for the production of dinitrotoluene |
| CN100369885C (zh) * | 2006-01-17 | 2008-02-20 | 甘肃银光化学工业集团有限公司 | 连续制备二硝基甲苯的方法及其装置 |
| DE102006033722A1 (de) * | 2006-07-21 | 2008-01-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von Dinitrotoluol |
| CN101544567B (zh) * | 2008-03-28 | 2012-07-25 | 中国科学院大连化学物理研究所 | 一步法合成二硝基甲苯的硝化方法 |
| DE102018217955B4 (de) * | 2018-10-19 | 2020-06-04 | Plinke Gmbh | Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1333444A (fr) * | 1962-09-11 | 1963-07-26 | Ici Ltd | Dinitration du toluène |
| US3928475A (en) * | 1974-08-09 | 1975-12-23 | Du Pont | Azeotropic nitration of benzene |
| US4021498A (en) * | 1975-12-09 | 1977-05-03 | American Cyanamid Company | Adiabatic process for nitration of nitratable aromatic compounds |
| US4091042A (en) * | 1977-08-19 | 1978-05-23 | American Cyanamid Company | Continuous adiabatic process for the mononitration of benzene |
| US4367347A (en) * | 1981-06-01 | 1983-01-04 | Air Products And Chemicals, Inc. | High purity 2,4-dinitrotoluene from toluene nitration process |
| US4453027A (en) * | 1982-12-10 | 1984-06-05 | Monsanto Company | Adiabatic process for the nitration of halobenzenes |
| DE3409719A1 (de) * | 1984-03-16 | 1985-09-19 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von dinitrotoluol |
| ES2087139T3 (es) * | 1990-01-04 | 1996-07-16 | Nrm Int Tech | Procedimiento de nitracion. |
| US5057632A (en) * | 1990-10-22 | 1991-10-15 | Olin Corporation | Process for preparing dinitrotoluene |
| DE4309140C2 (de) * | 1993-03-22 | 2001-09-20 | Bayer Ag | Verfahren zur Herstellung von Dinitrotoluol |
| TW236610B (en) * | 1992-11-13 | 1994-12-21 | Bayer Ag | Preparation of dinitrotoluene |
-
1994
- 1994-08-11 DE DE4428462A patent/DE4428462A1/de not_active Withdrawn
-
1995
- 1995-07-31 EP EP95111996A patent/EP0696571B1/de not_active Expired - Lifetime
- 1995-07-31 ES ES95111996T patent/ES2144074T3/es not_active Expired - Lifetime
- 1995-07-31 DE DE59507681T patent/DE59507681D1/de not_active Expired - Fee Related
- 1995-08-03 US US08/510,803 patent/US5689018A/en not_active Expired - Fee Related
- 1995-08-07 CA CA002155562A patent/CA2155562C/en not_active Expired - Fee Related
- 1995-08-09 JP JP22279395A patent/JP3631814B2/ja not_active Expired - Fee Related
- 1995-08-10 BR BR9503612A patent/BR9503612A/pt not_active IP Right Cessation
- 1995-08-10 KR KR1019950024653A patent/KR100375905B1/ko not_active Expired - Fee Related
- 1995-08-11 TW TW084108355A patent/TW314508B/zh active
- 1995-08-11 CN CN95109295A patent/CN1075054C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR960007531A (ko) | 1996-03-22 |
| ES2144074T3 (es) | 2000-06-01 |
| BR9503612A (pt) | 1996-04-30 |
| CN1075054C (zh) | 2001-11-21 |
| CA2155562A1 (en) | 1996-02-12 |
| EP0696571A3 (de) | 1998-06-10 |
| DE4428462A1 (de) | 1996-02-15 |
| EP0696571A2 (de) | 1996-02-14 |
| CA2155562C (en) | 2006-11-14 |
| EP0696571B1 (de) | 2000-01-26 |
| DE59507681D1 (de) | 2000-03-02 |
| TW314508B (cg-RX-API-DMAC7.html) | 1997-09-01 |
| CN1121507A (zh) | 1996-05-01 |
| JPH0859565A (ja) | 1996-03-05 |
| US5689018A (en) | 1997-11-18 |
| JP3631814B2 (ja) | 2005-03-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR100357406B1 (ko) | 디니트로톨루엔의제조방법 | |
| CA2155562C (en) | Process for the production of dinitrotoluene | |
| KR100358318B1 (ko) | 디니트로톨루엔의제조방법 | |
| US5099078A (en) | Process for preparing dinitrotoluene | |
| US6583327B2 (en) | Continuous isothermal process for preparing mononitrotoluenes | |
| US5663462A (en) | Process for the production of dinitrotoluene and isomeric mixtures of dinitrotoluene | |
| RS14904A (sr) | Dvostepeni postupak za pripremanje dinitrotoluola | |
| US5006325A (en) | Process for the recovery of nitric acid | |
| US3799993A (en) | Process for the manufacture of trinitrotoluene | |
| US6528690B2 (en) | Adiabatic process for producing dinitrotoluene | |
| US5354924A (en) | Process for the production of dinitrotoluene | |
| KR100869014B1 (ko) | 인산의 존재하에 모노니트로톨루엔의 연속 등온 제조 방법 | |
| CA1340073C (en) | Process for the production of dinitrotoleune or mononitrobenzene | |
| KR970010465B1 (ko) | 디니트로톨루엔 또는 모노니트로벤젠의 제조방법 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
St.27 status event code: A-0-1-A10-A12-nap-PA0109 |
|
| R17-X000 | Change to representative recorded |
St.27 status event code: A-3-3-R10-R17-oth-X000 |
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| PG1501 | Laying open of application |
St.27 status event code: A-1-1-Q10-Q12-nap-PG1501 |
|
| R17-X000 | Change to representative recorded |
St.27 status event code: A-3-3-R10-R17-oth-X000 |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-3-3-R10-R18-oth-X000 |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-3-3-R10-R18-oth-X000 |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-3-3-R10-R18-oth-X000 |
|
| PN2301 | Change of applicant |
St.27 status event code: A-3-3-R10-R13-asn-PN2301 St.27 status event code: A-3-3-R10-R11-asn-PN2301 |
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| A201 | Request for examination | ||
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
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| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
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| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-3-3-R10-R18-oth-X000 |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-3-3-R10-R18-oth-X000 |
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| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
St.27 status event code: A-1-2-D10-D21-exm-PE0902 |
|
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
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| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
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| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
St.27 status event code: A-1-2-D10-D22-exm-PE0701 |
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| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
St.27 status event code: A-2-4-F10-F11-exm-PR0701 |
|
| PR1002 | Payment of registration fee |
St.27 status event code: A-2-2-U10-U11-oth-PR1002 Fee payment year number: 1 |
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| PG1601 | Publication of registration |
St.27 status event code: A-4-4-Q10-Q13-nap-PG1601 |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |
|
| LAPS | Lapse due to unpaid annual fee | ||
| PC1903 | Unpaid annual fee |
St.27 status event code: A-4-4-U10-U13-oth-PC1903 Not in force date: 20060301 Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE |
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| PC1903 | Unpaid annual fee |
St.27 status event code: N-4-6-H10-H13-oth-PC1903 Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE Not in force date: 20060301 |
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| R18-X000 | Changes to party contact information recorded |
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| R18-X000 | Changes to party contact information recorded |
St.27 status event code: A-5-5-R10-R18-oth-X000 |