JPWO2020180397A5 - - Google Patents
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- Publication number
- JPWO2020180397A5 JPWO2020180397A5 JP2021552751A JP2021552751A JPWO2020180397A5 JP WO2020180397 A5 JPWO2020180397 A5 JP WO2020180397A5 JP 2021552751 A JP2021552751 A JP 2021552751A JP 2021552751 A JP2021552751 A JP 2021552751A JP WO2020180397 A5 JPWO2020180397 A5 JP WO2020180397A5
- Authority
- JP
- Japan
- Prior art keywords
- resin
- vessel
- eductor
- solution
- regenerant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011347 resin Substances 0.000 claims description 105
- 229920005989 resin Polymers 0.000 claims description 105
- 239000000126 substance Substances 0.000 claims description 29
- 239000012492 regenerant Substances 0.000 claims description 26
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 17
- 238000012544 monitoring process Methods 0.000 claims description 17
- 238000004140 cleaning Methods 0.000 claims description 15
- 125000000129 anionic group Chemical group 0.000 claims description 11
- 125000002091 cationic group Chemical group 0.000 claims description 10
- 239000002699 waste material Substances 0.000 claims description 10
- 238000000746 purification Methods 0.000 claims description 6
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 230000008929 regeneration Effects 0.000 claims description 4
- 238000011069 regeneration method Methods 0.000 claims description 4
- 238000005342 ion exchange Methods 0.000 claims description 3
- 235000013980 iron oxide Nutrition 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 238000009792 diffusion process Methods 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims 5
- 238000006722 reduction reaction Methods 0.000 claims 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 3
- 238000004891 communication Methods 0.000 claims 3
- 229910044991 metal oxide Inorganic materials 0.000 claims 3
- 150000004706 metal oxides Chemical class 0.000 claims 3
- 239000012530 fluid Substances 0.000 claims 2
- 230000003134 recirculating effect Effects 0.000 claims 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims 1
- 239000003456 ion exchange resin Substances 0.000 claims 1
- 229920003303 ion-exchange polymer Polymers 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims 1
- 230000000007 visual effect Effects 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 2
- 230000001172 regenerating effect Effects 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
Applications Claiming Priority (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201862724587P | 2018-08-29 | 2018-08-29 | |
| US16/292,131 US10532351B1 (en) | 2018-08-29 | 2019-03-04 | Method for restoring kinetic properties of resin |
| US16/292,131 | 2019-03-04 | ||
| US16/676,128 US10737260B2 (en) | 2018-08-29 | 2019-11-06 | System and method for restoring kinetic properties of resin |
| US16/676,128 | 2019-11-06 | ||
| PCT/US2020/013382 WO2020180397A1 (en) | 2018-08-29 | 2020-01-13 | System and method for regenerating and restoring kinetic properties of resin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2022523820A JP2022523820A (ja) | 2022-04-26 |
| JPWO2020180397A5 true JPWO2020180397A5 (enExample) | 2023-01-26 |
Family
ID=69141194
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2021552751A Pending JP2022523820A (ja) | 2018-08-29 | 2020-01-13 | 樹脂の反応速度特性を再生及び回復するためのシステム並びに方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (5) | US10532351B1 (enExample) |
| EP (1) | EP3934806A4 (enExample) |
| JP (1) | JP2022523820A (enExample) |
| KR (1) | KR102917719B1 (enExample) |
| CN (1) | CN113543881A (enExample) |
| AU (1) | AU2020233564A1 (enExample) |
| CA (1) | CA3132151A1 (enExample) |
| IL (1) | IL285777A (enExample) |
| WO (1) | WO2020180397A1 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10532351B1 (en) * | 2018-08-29 | 2020-01-14 | Thomas O. Miller | Method for restoring kinetic properties of resin |
| US12311349B2 (en) * | 2019-03-04 | 2025-05-27 | lonx Solutions, LLC | System and method for regenerating and restoring kinetic properties of resin |
| WO2022155160A1 (en) * | 2021-01-12 | 2022-07-21 | Ionx Solutions, Llc | System and method for regenerating and restoring kinetic properties of resin |
| WO2022212419A1 (en) * | 2021-03-29 | 2022-10-06 | Ionx Solutions, Llc | System and method for on-site cleaning and restoration of kinetic properties of ion exchange resin |
| CN115101229B (zh) * | 2022-06-14 | 2025-01-24 | 华能海南昌江核电有限公司 | 一种放射性废树脂再生式去污处理方法 |
| TW202432511A (zh) | 2022-12-23 | 2024-08-16 | 日商住友化學股份有限公司 | 化合物、包含源自該化合物的結構單元的樹脂、抗蝕劑組成物以及抗蝕劑圖案的製造方法 |
Family Cites Families (44)
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|---|---|---|---|---|
| US3139401A (en) | 1962-01-05 | 1964-06-30 | Hach Chemical Co | Method for removing rust from water softeners |
| GB1054578A (en) | 1964-11-12 | 1967-01-11 | United Kingdom Atomic Energy Authority | Improvements in or relating to Ion Exchange Methods and Apparatus |
| US3749249A (en) * | 1971-03-05 | 1973-07-31 | Ecodyne Corp | Method and apparatus |
| JPS4937888A (enExample) * | 1972-08-11 | 1974-04-08 | ||
| US4220531A (en) * | 1978-04-14 | 1980-09-02 | Gordon B. Nute | Apparatus for deionizing liquids with ion exchange resins |
| US4151079A (en) * | 1978-06-05 | 1979-04-24 | Nalco Chemical Company | Regeneration of ion exchange resins |
| JPS5524570A (en) * | 1978-08-11 | 1980-02-21 | Ebara Infilco Co Ltd | Removing method for phosphates in solution |
| JPS5926143A (ja) * | 1982-08-05 | 1984-02-10 | Ebara Infilco Co Ltd | イオン交換樹脂の除鉄回生方法 |
| US4500430A (en) | 1982-09-22 | 1985-02-19 | Dasgupta Purnendu K | Continuously rejuvenated ion exchanger |
| JPS59139944A (ja) * | 1983-01-31 | 1984-08-11 | Hitachi Ltd | 懸濁固形物付着イオン交換樹脂の洗浄方法 |
| US4511675A (en) | 1983-04-19 | 1985-04-16 | Auerswald David C | Method for regenerating water polishers using ammonium sulphate |
| US4880513A (en) * | 1986-06-20 | 1989-11-14 | The Graver Company | Method and apparatus for generating acid and base regenerants and the use thereof to regenerate ion-exchange resins |
| US4913803A (en) * | 1988-04-07 | 1990-04-03 | Radiological & Chemical Technology, Inc. | Particle separation system |
| US5082567A (en) * | 1990-11-08 | 1992-01-21 | Occidental Chemical Corporation | Regeneration of cationic exchange resins |
| JP3348109B2 (ja) * | 1992-01-02 | 2002-11-20 | コノコ・インコーポレーテッド | 水酸化ナトリウムで陽イオン交換樹脂からアルカノールアミンを選択的に再生するためのモニターおよび制御システム |
| JPH06134322A (ja) * | 1992-10-23 | 1994-05-17 | I C I Japan Kk | イオン交換樹脂 |
| US5858119A (en) * | 1995-05-17 | 1999-01-12 | Mayne; Michael D. | Ion exchange resin cleaning method |
| JP2002159867A (ja) | 2000-11-27 | 2002-06-04 | Kurita Water Ind Ltd | アニオン交換樹脂の再生方法 |
| JP2002361244A (ja) * | 2001-06-08 | 2002-12-17 | Hitachi Electric Systems Ltd | 水道水軟水化装置 |
| AU2003228540A1 (en) | 2002-04-12 | 2003-10-27 | Ionics, Incorporated | Ion exchange regeneration and upw treatment system |
| US7482387B2 (en) * | 2004-02-17 | 2009-01-27 | Institute Of Nuclear Energy | Method for processing spent ion-exchange resins |
| JP2006184045A (ja) * | 2004-12-27 | 2006-07-13 | Ebara Kogyo Senjo Kk | 化学除染用イオン交換樹脂塔 |
| US8585906B2 (en) * | 2006-07-14 | 2013-11-19 | Rayne Dealership Corporation | Regeneration of ion exchange resin and recovery of regenerant solution |
| JP5298639B2 (ja) * | 2008-05-26 | 2013-09-25 | 栗田工業株式会社 | 水溶性樹脂成分含有アルカリ廃液の処理方法および処理装置 |
| US8063112B2 (en) * | 2008-12-08 | 2011-11-22 | Cansolv Technologies Inc. | Process for the regeneration of an ion exchange resin using sulfurous acid |
| US8870445B2 (en) | 2008-12-12 | 2014-10-28 | II Gordon C. Burns | Liquid accelerator and chemical mixing apparatus and method |
| ES2566536T3 (es) * | 2010-07-01 | 2016-04-13 | Emd Millipore Corporation | Dispositivo y procedimiento de electrodesionización que comprende el control de la corriente eléctrica mediante la medición de la expansión del material de intercambio iónico |
| EP2625694A4 (en) * | 2010-10-06 | 2014-04-23 | Electric Power Res Inst | ION EXCHANGE REGENERATION AND NUCLEAR SPECIFIC SELECTION PROCEDURES |
| CN102219285B (zh) * | 2011-05-17 | 2013-01-02 | 南京大学 | 一种连续流内循环拟流化床树脂离子交换与吸附反应器 |
| US20120312750A1 (en) | 2011-06-08 | 2012-12-13 | Chandler Systems, Inc. | Water Softener System and Method |
| US9005448B2 (en) | 2011-08-12 | 2015-04-14 | General Electric Company | Mobile water treatment and resin transfer hub |
| JP2013139028A (ja) * | 2011-12-09 | 2013-07-18 | Shinryo Corp | アニオン交換樹脂の再生方法及び再生アニオン交換樹脂 |
| US9597679B2 (en) * | 2011-12-13 | 2017-03-21 | Ecolab Usa Inc. | Integrated acid regeneration of ion exchange resins for industrial applications |
| WO2014089614A1 (en) * | 2012-12-11 | 2014-06-19 | Clean Teq Pty Ltd | A process, method and plant for recovering scandium |
| US9896352B2 (en) * | 2013-03-15 | 2018-02-20 | Avantech, Inc. | Apparatus for removal of radionuclides in liquids |
| WO2015029057A2 (en) * | 2013-09-02 | 2015-03-05 | Reliance Industries Limited | A method for regeneration of spent ion exchange resins |
| WO2015143538A1 (en) | 2014-03-24 | 2015-10-01 | Production Plus Energy Services Inc. | Systems and methods for producing formation fluids |
| JP6015737B2 (ja) * | 2014-11-13 | 2016-10-26 | 栗田工業株式会社 | 再生型イオン交換装置の運転方法 |
| CA2967681A1 (en) * | 2014-11-14 | 2016-05-19 | Filterboxx Water And Environmental Corp. | Ion-exchange purification method and apparatus |
| EP3244990A1 (en) | 2014-12-19 | 2017-11-22 | The Procter and Gamble Company | A spatially controllable eductor for managing solid additives and processes using same |
| JP6315611B2 (ja) * | 2015-11-30 | 2018-04-25 | 壽化工機株式会社 | 混床式樹脂充填塔の混合樹脂の分離方法、混床式樹脂充填塔、及び水処理装置 |
| CN207271271U (zh) * | 2017-09-28 | 2018-04-27 | 荣成市固废综合处理与应用产业园有限公司 | 一种阳离子树脂铁中毒在线复苏装置 |
| CN107442185A (zh) * | 2017-09-28 | 2017-12-08 | 荣成市固废综合处理与应用产业园有限公司 | 一种阳离子树脂铁中毒在线复苏装置及复苏方法 |
| US10532351B1 (en) * | 2018-08-29 | 2020-01-14 | Thomas O. Miller | Method for restoring kinetic properties of resin |
-
2019
- 2019-03-04 US US16/292,131 patent/US10532351B1/en active Active
- 2019-11-06 US US16/676,128 patent/US10737260B2/en active Active
-
2020
- 2020-01-13 WO PCT/US2020/013382 patent/WO2020180397A1/en not_active Ceased
- 2020-01-13 CA CA3132151A patent/CA3132151A1/en active Pending
- 2020-01-13 JP JP2021552751A patent/JP2022523820A/ja active Pending
- 2020-01-13 CN CN202080018776.XA patent/CN113543881A/zh active Pending
- 2020-01-13 AU AU2020233564A patent/AU2020233564A1/en not_active Abandoned
- 2020-01-13 KR KR1020217031721A patent/KR102917719B1/ko active Active
- 2020-01-13 EP EP20767286.6A patent/EP3934806A4/en active Pending
- 2020-08-05 US US16/986,229 patent/US11433387B2/en active Active
-
2021
- 2021-08-22 IL IL285777A patent/IL285777A/en unknown
-
2022
- 2022-09-02 US US17/902,796 patent/US11911755B2/en active Active
-
2024
- 2024-01-17 US US18/415,481 patent/US12239971B2/en active Active
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