JPWO2019229660A5 - - Google Patents
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- JPWO2019229660A5 JPWO2019229660A5 JP2020566209A JP2020566209A JPWO2019229660A5 JP WO2019229660 A5 JPWO2019229660 A5 JP WO2019229660A5 JP 2020566209 A JP2020566209 A JP 2020566209A JP 2020566209 A JP2020566209 A JP 2020566209A JP WO2019229660 A5 JPWO2019229660 A5 JP WO2019229660A5
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- JP
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- 238000001228 spectrum Methods 0.000 description 2
- CZDYPVPMEAXLPK-UHFFFAOYSA-N tetramethylsilane Chemical compound C[Si](C)(C)C CZDYPVPMEAXLPK-UHFFFAOYSA-N 0.000 description 2
- 238000001644 13C nuclear magnetic resonance spectroscopy Methods 0.000 description 1
- 238000013480 data collection Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
Description
取得パラメーター：
取得温度：７９．８５～９９．８５℃；
取得ポイント数（ＴＤ）：６４；
サイズ：３２；
ラインブロードニング（ＬＢ）：１．２Ｈｚ；
スペクトルウィンドウ（ＳＷ）：１８０００Ｈｚ（２４０．０～０．０ｐｐｍ）；
ＰＵＬＰＲＯＧ＊：「ｚｇｉｇ＿ｂｉｌｅｖ」；INVGATEベースのプログラム；
ＣＰＤＰＲＧ２＊：「ｗａｌｔｚ１６＿ｂｉｌｅｖ」；デカップリングプログラム；
緩和時間（Ｄ１）：１０秒；
パルス角：９０°；
スキャン数：６６００（ｓ／ｎ＝＞７５０）；
ｓ／ｎ比の計算：２００～１０ｐｐｍのスペクトル振幅、６０～５０ｐｐｍの自動ノイズ計算、２７．９～２７．３ｐｐｍの基準ピーク＊＊からの信号の計算；
データ収集／処理プログラム：ＴＯＰＳＰＩＮ。
（＊）ＮＯＥ（核オーバーハウザー増強）効果を排除するためのデカップリングを備えた取得プログラム。
（＊＊）１３Ｃ－ＮＭＲスペクトルにおけるピーク割り当ては、ＴＭＳ（テトラメチルシラン）に基づく。
取得温度：７９．８５～９９．８５℃；
取得ポイント数（ＴＤ）：６４；
サイズ：３２；
ラインブロードニング（ＬＢ）：１．２Ｈｚ；
スペクトルウィンドウ（ＳＷ）：１８０００Ｈｚ（２４０．０～０．０ｐｐｍ）；
ＰＵＬＰＲＯＧ＊：「ｚｇｉｇ＿ｂｉｌｅｖ」；INVGATEベースのプログラム；
ＣＰＤＰＲＧ２＊：「ｗａｌｔｚ１６＿ｂｉｌｅｖ」；デカップリングプログラム；
緩和時間（Ｄ１）：１０秒；
パルス角：９０°；
スキャン数：６６００（ｓ／ｎ＝＞７５０）；
ｓ／ｎ比の計算：２００～１０ｐｐｍのスペクトル振幅、６０～５０ｐｐｍの自動ノイズ計算、２７．９～２７．３ｐｐｍの基準ピーク＊＊からの信号の計算；
データ収集／処理プログラム：ＴＯＰＳＰＩＮ。
（＊）ＮＯＥ（核オーバーハウザー増強）効果を排除するためのデカップリングを備えた取得プログラム。
（＊＊）１３Ｃ－ＮＭＲスペクトルにおけるピーク割り当ては、ＴＭＳ（テトラメチルシラン）に基づく。
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT102018000005841 | 2018-05-30 | ||
| IT102018000005841A IT201800005841A1 (it) | 2018-05-30 | 2018-05-30 | Procedimento per la preparazione di copolimeri random butadiene-isoprene ad elevato contenuto di unita’ 1,4-cis |
| PCT/IB2019/054427 WO2019229660A1 (en) | 2018-05-30 | 2019-05-29 | Process for preparing random butadiene-isoprene copolymers having a high content of cis-1,4 units |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2021525813A JP2021525813A (ja) | 2021-09-27 |
| JPWO2019229660A5 true JPWO2019229660A5 (ja) | 2022-06-03 |
| JP7374929B2 JP7374929B2 (ja) | 2023-11-07 |
Family
ID=63312326
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020566209A Active JP7374929B2 (ja) | 2018-05-30 | 2019-05-29 | 高含有量のシス－１，４ユニットを有するランダムブタジエン－イソプレンコポリマーを作製する方法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US20210198404A1 (ja) |
| EP (1) | EP3802646A1 (ja) |
| JP (1) | JP7374929B2 (ja) |
| KR (1) | KR20210016583A (ja) |
| CN (1) | CN112424244A (ja) |
| BR (1) | BR112020024506B1 (ja) |
| CA (1) | CA3101559A1 (ja) |
| IT (1) | IT201800005841A1 (ja) |
| MX (1) | MX2020012892A (ja) |
| SG (1) | SG11202011603PA (ja) |
| WO (1) | WO2019229660A1 (ja) |
| ZA (1) | ZA202007549B (ja) |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5405815A (en) * | 1993-06-17 | 1995-04-11 | The Goodyear Tire & Rubber Company | Process for preparing a catalyst system useful in the synthesis of isoprene-butadiene rubber |
| DE10032876A1 (de) * | 2000-03-24 | 2001-09-27 | Bayer Ag | Verfahren zur Polymerisation von konjugierten Diolefinen (Dienen) mit Katalysatoren der Seltenen Erden in Gegenwart vinylaromatischer Lösungsmittel |
| CN1249109C (zh) * | 2001-02-28 | 2006-04-05 | 株式会社普利司通 | 用于生产具有窄分子量分布的共轭二烯聚合物的连续方法和由其制成的产品 |
| ITMI20011901A1 (it) * | 2001-09-12 | 2003-03-12 | Enichem Spa | Copolimeri random butadiene-isoprene struttura trans-1,4 |
| WO2003048221A1 (fr) * | 2001-12-07 | 2003-06-12 | Societe De Technologie Michelin | Procede de preparation de copolymeres butadiene/isoprene et ces copolymeres |
| ZA200210309B (en) * | 2001-12-31 | 2003-07-03 | Goodyear Tire & Rubber | Group III-B metal catalyst system. |
| US7022783B2 (en) * | 2001-12-31 | 2006-04-04 | The Goodyear Tire & Rubber Company | Group III-B metal catalyst system |
| US6780948B2 (en) * | 2002-03-28 | 2004-08-24 | The Goodyear Tire & Rubber Company | Synthesis of polyisoprene with neodymium catalyst |
| US7091150B2 (en) * | 2003-12-19 | 2006-08-15 | The Goodyear Tire & Rubber Company | Synthetic polyisoprene rubber |
| US7885821B2 (en) * | 2006-04-03 | 2011-02-08 | Michael Tait | Package pickup indicator system |
| US8314189B2 (en) * | 2007-10-12 | 2012-11-20 | Bridgestone Corporation | Polymers functionalized with heterocyclic nitrile compounds |
| ITMI20080570A1 (it) * | 2008-04-02 | 2009-10-03 | Polimeri Europa Spa | Procedimento per la preparazione di polibutadiene ramificato ad alto contenuto in unita' 1,4-cis |
| US20120264897A1 (en) * | 2009-12-02 | 2012-10-18 | Ruehmer Thomas D | Catalyst systems for rubber polymerizations |
| US8445580B2 (en) * | 2011-05-31 | 2013-05-21 | The Goodyear Tire & Rubber Company | Tire with tread of polybutadiene rubber |
| ITMI20120808A1 (it) * | 2012-05-11 | 2013-11-12 | Versalis Spa | "procedimento per la preparazione di polibutadiene ramificato ad alto contenuto in unita' 1,4-cis" |
| CN104130350B (zh) * | 2013-05-02 | 2017-08-22 | 中国石油化工股份有限公司 | 一种丁二烯‑异戊二烯共聚物橡胶及其制备方法 |
| RU2658913C1 (ru) * | 2014-08-20 | 2018-06-26 | Бриджстоун Корпорейшн | Способ изготовления полимера сопряженного диена, полимер сопряженного диена, резиновая смесь и шина |
-
2018
- 2018-05-30 IT IT102018000005841A patent/IT201800005841A1/it unknown
-
2019
- 2019-05-29 BR BR112020024506-2A patent/BR112020024506B1/pt active IP Right Grant
- 2019-05-29 CA CA3101559A patent/CA3101559A1/en active Pending
- 2019-05-29 MX MX2020012892A patent/MX2020012892A/es unknown
- 2019-05-29 KR KR1020207037984A patent/KR20210016583A/ko not_active Application Discontinuation
- 2019-05-29 WO PCT/IB2019/054427 patent/WO2019229660A1/en active Application Filing
- 2019-05-29 CN CN201980036449.4A patent/CN112424244A/zh active Pending
- 2019-05-29 SG SG11202011603PA patent/SG11202011603PA/en unknown
- 2019-05-29 US US17/058,413 patent/US20210198404A1/en active Pending
- 2019-05-29 JP JP2020566209A patent/JP7374929B2/ja active Active
- 2019-05-29 EP EP19732475.9A patent/EP3802646A1/en active Pending
-
2020
- 2020-12-03 ZA ZA2020/07549A patent/ZA202007549B/en unknown
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