JPS6411056B2 - - Google Patents

Info

Publication number

JPS6411056B2

JPS6411056B2 JP8712881A JP8712881A JPS6411056B2 JP S6411056 B2 JPS6411056 B2 JP S6411056B2 JP 8712881 A JP8712881 A JP 8712881A JP 8712881 A JP8712881 A JP 8712881A JP S6411056 B2 JPS6411056 B2 JP S6411056B2

Authority

JP

Japan

Prior art keywords

parts

spherical

aging agent

molten

added

Prior art date

1981-06-05

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Links

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• DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 26
• 239000003795 chemical substances by application Substances 0.000 claims description 25
• 230000003712 anti-aging effect Effects 0.000 claims description 24
• 239000007864 aqueous solution Substances 0.000 claims description 13
• 239000003945 anionic surfactant Substances 0.000 claims description 8
• 238000003756 stirring Methods 0.000 claims description 8
• 238000004519 manufacturing process Methods 0.000 claims description 6
• 239000002002 slurry Substances 0.000 claims description 5
• 150000001412 amines Chemical class 0.000 claims description 4
• 239000002245 particle Substances 0.000 description 13
• 238000000034 method Methods 0.000 description 11
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
• 239000000243 solution Substances 0.000 description 9
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
• -1 alkyl sulfate salt Chemical class 0.000 description 7
• 238000002844 melting Methods 0.000 description 7
• 230000008018 melting Effects 0.000 description 7
• 239000011734 sodium Substances 0.000 description 7
• 229910052708 sodium Inorganic materials 0.000 description 7
• 229910052783 alkali metal Inorganic materials 0.000 description 6
• 150000001340 alkali metals Chemical class 0.000 description 6
• 125000000217 alkyl group Chemical group 0.000 description 6
• 150000001875 compounds Chemical class 0.000 description 5
• 238000001035 drying Methods 0.000 description 5
• 238000001914 filtration Methods 0.000 description 5
• 239000000843 powder Substances 0.000 description 5
• 238000005406 washing Methods 0.000 description 5
• CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 4
• FKHKSWSHWLYDOI-UHFFFAOYSA-N 2-phenylbenzene-1,4-diamine Chemical compound NC1=CC=C(N)C(C=2C=CC=CC=2)=C1 FKHKSWSHWLYDOI-UHFFFAOYSA-N 0.000 description 4
• 238000001816 cooling Methods 0.000 description 4
• 229920001477 hydrophilic polymer Polymers 0.000 description 4
• 239000012798 spherical particle Substances 0.000 description 4
• ZZMVLMVFYMGSMY-UHFFFAOYSA-N 4-n-(4-methylpentan-2-yl)-1-n-phenylbenzene-1,4-diamine Chemical compound C1=CC(NC(C)CC(C)C)=CC=C1NC1=CC=CC=C1 ZZMVLMVFYMGSMY-UHFFFAOYSA-N 0.000 description 3
• 238000013329 compounding Methods 0.000 description 3
• 239000007787 solid Substances 0.000 description 3
• IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
• OUBMGJOQLXMSNT-UHFFFAOYSA-N N-isopropyl-N'-phenyl-p-phenylenediamine Chemical compound C1=CC(NC(C)C)=CC=C1NC1=CC=CC=C1 OUBMGJOQLXMSNT-UHFFFAOYSA-N 0.000 description 2
• BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 description 2
• 229940063953 ammonium lauryl sulfate Drugs 0.000 description 2
• 125000003118 aryl group Chemical group 0.000 description 2
• 230000007423 decrease Effects 0.000 description 2
• 235000019329 dioctyl sodium sulphosuccinate Nutrition 0.000 description 2
• YHAIUSTWZPMYGG-UHFFFAOYSA-L disodium;2,2-dioctyl-3-sulfobutanedioate Chemical compound [Na+].[Na+].CCCCCCCCC(C([O-])=O)(C(C([O-])=O)S(O)(=O)=O)CCCCCCCC YHAIUSTWZPMYGG-UHFFFAOYSA-L 0.000 description 2
• GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 description 2
• QGVQVNIIRBPOAM-UHFFFAOYSA-N dodecyl naphthalene-1-sulfonate;sodium Chemical compound [Na].C1=CC=C2C(S(=O)(=O)OCCCCCCCCCCCC)=CC=CC2=C1 QGVQVNIIRBPOAM-UHFFFAOYSA-N 0.000 description 2
• 239000000428 dust Substances 0.000 description 2
• 230000000694 effects Effects 0.000 description 2
• 238000002156 mixing Methods 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical compound C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 description 2
• 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 2
• 238000007711 solidification Methods 0.000 description 2
• 230000008023 solidification Effects 0.000 description 2
• NBDYSLCMCUDINP-UHFFFAOYSA-N 3-[dodecanoyl(methyl)amino]propanoic acid;sodium Chemical compound [Na].CCCCCCCCCCCC(=O)N(C)CCC(O)=O NBDYSLCMCUDINP-UHFFFAOYSA-N 0.000 description 1
• 125000006539 C12 alkyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
• QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 description 1
• 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
• ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 1
• 238000005054 agglomeration Methods 0.000 description 1
• 230000002776 aggregation Effects 0.000 description 1
• 235000004279 alanine Nutrition 0.000 description 1
• 150000008055 alkyl aryl sulfonates Chemical class 0.000 description 1
• 239000002280 amphoteric surfactant Substances 0.000 description 1
• 239000002518 antifoaming agent Substances 0.000 description 1
• 229910052799 carbon Inorganic materials 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 239000006185 dispersion Substances 0.000 description 1
• 230000008014 freezing Effects 0.000 description 1
• 238000007710 freezing Methods 0.000 description 1
• 239000000463 material Substances 0.000 description 1
• 125000001624 naphthyl group Chemical group 0.000 description 1
• 239000002736 nonionic surfactant Substances 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 238000005453 pelletization Methods 0.000 description 1
• 238000007873 sieving Methods 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1