JPS6362695B2 - - Google Patents
Info
- Publication number
- JPS6362695B2 JPS6362695B2 JP57141861A JP14186182A JPS6362695B2 JP S6362695 B2 JPS6362695 B2 JP S6362695B2 JP 57141861 A JP57141861 A JP 57141861A JP 14186182 A JP14186182 A JP 14186182A JP S6362695 B2 JPS6362695 B2 JP S6362695B2
- Authority
- JP
- Japan
- Prior art keywords
- sample
- melting agent
- standard
- reagent
- measured
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000002844 melting Methods 0.000 claims description 42
- 230000008018 melting Effects 0.000 claims description 42
- 239000011521 glass Substances 0.000 claims description 21
- 239000011324 bead Substances 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 15
- 238000002441 X-ray diffraction Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 239000000523 sample Substances 0.000 description 55
- 239000003153 chemical reaction reagent Substances 0.000 description 39
- 239000003795 chemical substances by application Substances 0.000 description 28
- 238000004458 analytical method Methods 0.000 description 10
- 238000011088 calibration curve Methods 0.000 description 8
- 238000005259 measurement Methods 0.000 description 8
- 238000005303 weighing Methods 0.000 description 8
- 230000008859 change Effects 0.000 description 5
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- 238000005204 segregation Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000004907 flux Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000002893 slag Substances 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 238000005464 sample preparation method Methods 0.000 description 2
- 230000003595 spectral effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000002194 synthesizing effect Effects 0.000 description 2
- 230000009466 transformation Effects 0.000 description 2
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- 239000004484 Briquette Substances 0.000 description 1
- SYTIQXASYKJXRY-UHFFFAOYSA-N [Au].[Rh].[Pt] Chemical compound [Au].[Rh].[Pt] SYTIQXASYKJXRY-UHFFFAOYSA-N 0.000 description 1
- 239000000538 analytical sample Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000002529 flux (metallurgy) Substances 0.000 description 1
- 238000007496 glass forming Methods 0.000 description 1
- JUWSSMXCCAMYGX-UHFFFAOYSA-N gold platinum Chemical compound [Pt].[Au] JUWSSMXCCAMYGX-UHFFFAOYSA-N 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- -1 ores Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2202—Preparing specimens therefor
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Sampling And Sample Adjustment (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57141861A JPS5931439A (ja) | 1982-08-16 | 1982-08-16 | 螢光x線分析用ガラスビード標準試料の作成方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57141861A JPS5931439A (ja) | 1982-08-16 | 1982-08-16 | 螢光x線分析用ガラスビード標準試料の作成方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5931439A JPS5931439A (ja) | 1984-02-20 |
| JPS6362695B2 true JPS6362695B2 (enExample) | 1988-12-05 |
Family
ID=15301866
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57141861A Granted JPS5931439A (ja) | 1982-08-16 | 1982-08-16 | 螢光x線分析用ガラスビード標準試料の作成方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5931439A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105358955A (zh) * | 2013-07-03 | 2016-02-24 | 蒂森克虏伯工业解决方案股份公司 | 用于制备压片的方法和装置 |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6459033A (en) * | 1987-08-31 | 1989-03-06 | Ngk Insulators Ltd | Sample transporting device for analysis |
| JP2507580B2 (ja) * | 1989-02-20 | 1996-06-12 | 日本碍子株式会社 | 碍子汚損量測定方法及びその装置 |
| JP4770968B2 (ja) | 2009-06-03 | 2011-09-14 | 住友電気工業株式会社 | 樹脂中の赤リン定量用標準試料の製造方法 |
| CN103439167B (zh) * | 2013-09-11 | 2015-09-16 | 淄博出入境检验检疫局综合技术服务中心 | 一种含铅陶瓷釉标准样品的制备方法 |
| CN107543748A (zh) * | 2017-08-22 | 2018-01-05 | 抚顺新钢铁有限责任公司 | 氧化铁矿x射线荧光分析中熔片复合式脱模方法 |
| CN109444198A (zh) * | 2018-12-13 | 2019-03-08 | 柳州钢铁股份有限公司 | 适用于膨润土、粘土化学成分的快速测定方法 |
-
1982
- 1982-08-16 JP JP57141861A patent/JPS5931439A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105358955A (zh) * | 2013-07-03 | 2016-02-24 | 蒂森克虏伯工业解决方案股份公司 | 用于制备压片的方法和装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5931439A (ja) | 1984-02-20 |
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