JPS5931439A - 螢光ｘ線分析用ガラスビード標準試料の作成方法 - Google Patents
螢光ｘ線分析用ガラスビード標準試料の作成方法Info
- Publication number
- JPS5931439A JPS5931439A JP57141861A JP14186182A JPS5931439A JP S5931439 A JPS5931439 A JP S5931439A JP 57141861 A JP57141861 A JP 57141861A JP 14186182 A JP14186182 A JP 14186182A JP S5931439 A JPS5931439 A JP S5931439A
- Authority
- JP
- Japan
- Prior art keywords
- sample
- flux
- standard sample
- reagent
- prepared
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011521 glass Substances 0.000 title claims abstract description 13
- 239000011324 bead Substances 0.000 title claims abstract description 11
- 238000002441 X-ray diffraction Methods 0.000 title claims description 5
- 238000002360 preparation method Methods 0.000 title claims description 3
- 230000003287 optical effect Effects 0.000 title description 2
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 26
- 238000002844 melting Methods 0.000 claims abstract description 26
- 230000008018 melting Effects 0.000 claims abstract description 26
- 238000000034 method Methods 0.000 claims abstract description 16
- 238000001816 cooling Methods 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 21
- 229910052751 metal Inorganic materials 0.000 claims description 5
- 239000002184 metal Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 3
- 230000004907 flux Effects 0.000 abstract description 6
- 238000002156 mixing Methods 0.000 abstract description 5
- 238000005303 weighing Methods 0.000 abstract description 4
- 238000005259 measurement Methods 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- 238000010298 pulverizing process Methods 0.000 abstract description 2
- 229910011131 Li2B4O7 Inorganic materials 0.000 abstract 1
- 229910004835 Na2B4O7 Inorganic materials 0.000 abstract 1
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 abstract 1
- 238000004458 analytical method Methods 0.000 description 14
- 238000011088 calibration curve Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 238000005464 sample preparation method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000951471 Citrus junos Species 0.000 description 1
- UNPLRYRWJLTVAE-UHFFFAOYSA-N Cloperastine hydrochloride Chemical compound Cl.C1=CC(Cl)=CC=C1C(C=1C=CC=CC=1)OCCN1CCCCC1 UNPLRYRWJLTVAE-UHFFFAOYSA-N 0.000 description 1
- 241000254158 Lampyridae Species 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 241001474791 Proboscis Species 0.000 description 1
- 241000750631 Takifugu chinensis Species 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000002224 dissection Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000007496 glass forming Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000013076 target substance Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2202—Preparing specimens therefor
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Sampling And Sample Adjustment (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57141861A JPS5931439A (ja) | 1982-08-16 | 1982-08-16 | 螢光ｘ線分析用ガラスビード標準試料の作成方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57141861A JPS5931439A (ja) | 1982-08-16 | 1982-08-16 | 螢光ｘ線分析用ガラスビード標準試料の作成方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5931439A true JPS5931439A (ja) | 1984-02-20 |
| JPS6362695B2 JPS6362695B2 (enExample) | 1988-12-05 |
Family
ID=15301866
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57141861A Granted JPS5931439A (ja) | 1982-08-16 | 1982-08-16 | 螢光ｘ線分析用ガラスビード標準試料の作成方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5931439A (enExample) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6459033A (en) * | 1987-08-31 | 1989-03-06 | Ngk Insulators Ltd | Sample transporting device for analysis |
| JPH02218947A (ja) * | 1989-02-20 | 1990-08-31 | Ngk Insulators Ltd | 碍子汚損量測定方法及びその装置 |
| WO2010140496A1 (ja) * | 2009-06-03 | 2010-12-09 | 住友電気工業株式会社 | 樹脂中の赤リン定量用標準試料の製造方法 |
| CN103439167A (zh) * | 2013-09-11 | 2013-12-11 | 淄博出入境检验检疫局综合技术服务中心 | 一种含铅陶瓷釉标准样品的制备方法 |
| WO2015000571A1 (de) * | 2013-07-03 | 2015-01-08 | Thyssenkrupp Industrial Solutions Ag | Verfahren sowie eine vorrichtung zur herstellung einer tablette |
| CN107543748A (zh) * | 2017-08-22 | 2018-01-05 | 抚顺新钢铁有限责任公司 | 氧化铁矿x射线荧光分析中熔片复合式脱模方法 |
| CN109444198A (zh) * | 2018-12-13 | 2019-03-08 | 柳州钢铁股份有限公司 | 适用于膨润土、粘土化学成分的快速测定方法 |
-
1982
- 1982-08-16 JP JP57141861A patent/JPS5931439A/ja active Granted
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6459033A (en) * | 1987-08-31 | 1989-03-06 | Ngk Insulators Ltd | Sample transporting device for analysis |
| JPH02218947A (ja) * | 1989-02-20 | 1990-08-31 | Ngk Insulators Ltd | 碍子汚損量測定方法及びその装置 |
| WO2010140496A1 (ja) * | 2009-06-03 | 2010-12-09 | 住友電気工業株式会社 | 樹脂中の赤リン定量用標準試料の製造方法 |
| JP2010281632A (ja) * | 2009-06-03 | 2010-12-16 | Sumitomo Electric Ind Ltd | 樹脂中の赤リン定量用標準試料の製造方法 |
| CN102119327A (zh) * | 2009-06-03 | 2011-07-06 | 住友电气工业株式会社 | 制备用于定量确定树脂中红磷的标准试样的方法 |
| US8012757B2 (en) | 2009-06-03 | 2011-09-06 | Sumitomo Electric Industries, Ltd. | Method for producing standard sample for use in quantitative determination of red phosphorus in resin |
| RU2663769C2 (ru) * | 2013-07-03 | 2018-08-09 | Тиссенкрупп Индастриал Солюшнз Аг | Способ и устройства для изготовления таблетки |
| WO2015000571A1 (de) * | 2013-07-03 | 2015-01-08 | Thyssenkrupp Industrial Solutions Ag | Verfahren sowie eine vorrichtung zur herstellung einer tablette |
| US10067039B2 (en) | 2013-07-03 | 2018-09-04 | Thyssenkrupp Industrial Solutions Ag | Method and apparatus for producing a pellet |
| CN103439167A (zh) * | 2013-09-11 | 2013-12-11 | 淄博出入境检验检疫局综合技术服务中心 | 一种含铅陶瓷釉标准样品的制备方法 |
| CN103439167B (zh) * | 2013-09-11 | 2015-09-16 | 淄博出入境检验检疫局综合技术服务中心 | 一种含铅陶瓷釉标准样品的制备方法 |
| CN107543748A (zh) * | 2017-08-22 | 2018-01-05 | 抚顺新钢铁有限责任公司 | 氧化铁矿x射线荧光分析中熔片复合式脱模方法 |
| CN109444198A (zh) * | 2018-12-13 | 2019-03-08 | 柳州钢铁股份有限公司 | 适用于膨润土、粘土化学成分的快速测定方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6362695B2 (enExample) | 1988-12-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Murao et al. | Thermodynamic modeling of the SFCA phase Ca2 (Fe, Ca) 6 (Fe, Al, Si) 6O20 | |
| CN109358082A (zh) | 一种熔融制样-x射线荧光测定钛铁中合金元素的方法 | |
| CN105806865A (zh) | X射线荧光光谱法用铜精矿熔融制片方法 | |
| Lezzerini et al. | Reproducibility, precision and trueness of X-ray fluorescence data for mineralogical and/or petrographic purposes | |
| JPS5931439A (ja) | 螢光ｘ線分析用ガラスビード標準試料の作成方法 | |
| CA2513566C (en) | X-ray fluorescence flux composition | |
| CN108508050A (zh) | X射线荧光光谱法测定钢渣中镧、铈和钡含量的方法 | |
| CN109975384A (zh) | 一种检测岩石中金属分布率的方法 | |
| CA2625318C (en) | Nickel flux composition | |
| Gebhardt | Rapid methods for chemical analysis of hydraulic cement | |
| Asif et al. | Study of the digestion of chromite during nickel sulphide fire assay for the platinum group elements and gold | |
| CN106338534A (zh) | 采用x射线荧光光谱仪快速测定萤石中氟化钙含量的方法 | |
| CN113820341A (zh) | Xrf分析用含钴熔剂、其制备方法与xrf分析用样品的制备方法 | |
| Hunt et al. | Major, minor and trace element mass fractions determined using ED-XRF, WD-XRF and INAA for five certified clay reference materials: NCS DC 60102–60105; NCS DC 61101 (GBW 03101A, 03102A, 03103, and 03115) | |
| Dhara et al. | Universal EDXRF method for multi-elemental determinations using fused bead specimens | |
| CN109444198A (zh) | 适用于膨润土、粘土化学成分的快速测定方法 | |
| JPH06249768A (ja) | 蛍光ｘ線分析用試料調製方法 | |
| AU2007202706B2 (en) | X-ray flux composition mixture | |
| Vuchkova et al. | Fusion method for preparation of refractory nickel based alloy powders for X-ray fluorescence spectrometry | |
| Feret | Routine analysis of iron ores by X-ray spectrometry | |
| AU2007216909A1 (en) | Copper X-ray flux composition | |
| CN116380958A (zh) | 一种矿石中TiO2含量的荧光检测方法 | |
| AU2007202703A1 (en) | X-ray flux composition | |
| Chirnside et al. | The determination of small amounts of iron and chromium in sapphire and ruby for maser applications | |
| McCarthy | Aspects of the chemistry of some stony meteorites |