JPS6352339B2 - - Google Patents
Info
- Publication number
- JPS6352339B2 JPS6352339B2 JP53039639A JP3963978A JPS6352339B2 JP S6352339 B2 JPS6352339 B2 JP S6352339B2 JP 53039639 A JP53039639 A JP 53039639A JP 3963978 A JP3963978 A JP 3963978A JP S6352339 B2 JPS6352339 B2 JP S6352339B2
- Authority
- JP
- Japan
- Prior art keywords
- rotor
- sensor
- stile
- winding
- magnetic resonance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000005481 NMR spectroscopy Methods 0.000 claims description 56
- 238000004804 winding Methods 0.000 claims description 27
- 239000007789 gas Substances 0.000 description 37
- 239000000523 sample Substances 0.000 description 27
- 230000035945 sensitivity Effects 0.000 description 7
- 239000000126 substance Substances 0.000 description 5
- 239000011521 glass Substances 0.000 description 4
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000007373 indentation Methods 0.000 description 2
- 230000006698 induction Effects 0.000 description 2
- 239000000696 magnetic material Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229920004943 Delrin® Polymers 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 229920006324 polyoxymethylene Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
- G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
- G01R33/307—Sample handling arrangements, e.g. sample cells, spinning mechanisms specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
- G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
- G01R33/31—Temperature control thereof
Landscapes
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU772491999A SU765724A1 (ru) | 1977-06-03 | 1977-06-03 | Датчик сигналов дерного магнитного резонанса |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5417796A JPS5417796A (en) | 1979-02-09 |
| JPS6352339B2 true JPS6352339B2 (https=) | 1988-10-18 |
Family
ID=20711508
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP3963978A Granted JPS5417796A (en) | 1977-06-03 | 1978-04-04 | Sensor for generating nuclear magnetic resonance |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4254373A (https=) |
| JP (1) | JPS5417796A (https=) |
| CA (1) | CA1098170A (https=) |
| CH (1) | CH628143A5 (https=) |
| DD (1) | DD136769A1 (https=) |
| DE (1) | DE2809237C2 (https=) |
| FR (1) | FR2393304A1 (https=) |
| GB (1) | GB1594042A (https=) |
| IT (1) | IT1093167B (https=) |
| SU (1) | SU765724A1 (https=) |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4201941A (en) * | 1978-08-04 | 1980-05-06 | International Business Machines Corporation | Spinning apparatus for NMR spectrometers |
| US4275350A (en) * | 1979-05-29 | 1981-06-23 | Varian Associates, Inc. | Sample spinning mechanism for NMR probes |
| JPS6051056B2 (ja) | 1980-06-13 | 1985-11-12 | 株式会社東芝 | 核磁気共鳴装置 |
| US4306878A (en) * | 1980-08-29 | 1981-12-22 | Brown Charles E | Method of selecting flame retardants for polymers |
| US4352066A (en) * | 1980-10-31 | 1982-09-28 | International Business Machines Corporation | Method for adjusting the magic angle in NMR experiments |
| US4446430A (en) * | 1981-08-31 | 1984-05-01 | Monsanto Company | Sample spinner for nuclear magnetic resonance spectrometer |
| US4456882A (en) * | 1982-01-04 | 1984-06-26 | University Of South Carolina | High speed cylindrical nuclear magnetic resonance (NMR) sample spinner |
| JPS58167947A (ja) * | 1982-03-29 | 1983-10-04 | Hitachi Ltd | 核磁気共鳴装置のスピンナ |
| US4511841A (en) * | 1982-06-17 | 1985-04-16 | Chemagnetics, Inc. | Method and apparatus for high speed magic angle spinning |
| US4510450A (en) * | 1982-09-28 | 1985-04-09 | The Medical College Of Wisconsin, Inc. | Apparatus and assay method for the quantitative determination of mineral content in bone |
| US4517516A (en) * | 1983-04-08 | 1985-05-14 | Varian Associates, Inc. | NMR Probe coil form structure |
| US4587492A (en) * | 1984-03-02 | 1986-05-06 | Varian Associates, Inc. | Thermal barrier for variable temperature NMR |
| US4739270A (en) * | 1986-06-03 | 1988-04-19 | Varian Associates, Inc. | High speed spinner for NMR spectrometer |
| US4940942A (en) * | 1989-04-14 | 1990-07-10 | Bartuska Victor J | Method and apparatus for conducting variable-temperature solid state magnetic resonance spectroscopy |
| US5416414A (en) * | 1990-04-27 | 1995-05-16 | British Technology Group Limited | Sample mount for NMR microscopy |
| US5202633A (en) * | 1990-11-01 | 1993-04-13 | Doty Scientific, Inc. | High temperature nmr sample spinner |
| JP3749550B2 (ja) * | 1991-12-19 | 2006-03-01 | バリアン・インコーポレイテッド | Ｎｍｒサンプルシェーパー |
| US5325059A (en) * | 1992-03-26 | 1994-06-28 | Doty Scientific Inc. | DOR NMR sample spinner |
| US5289130A (en) * | 1992-07-31 | 1994-02-22 | Doty Scientific Inc. | NMR sample rotor cooling technique |
| US5408181A (en) * | 1993-08-30 | 1995-04-18 | Auburn International, Inc. | NMR system for measuring polymer properties |
| DE4440241C1 (de) * | 1994-10-25 | 1996-03-21 | Rainer Schmieg | Turbine |
| US6054857A (en) * | 1997-03-18 | 2000-04-25 | Doty Scientific, Inc. | NMR MAS sealing sample cells and methods |
| EE00330U1 (et) | 2002-05-30 | 2002-10-15 | Keemilise ja Bioloogilise F��sika Instituut | Tuuma magnetresonants-spektromeetri mõõtepea |
| EE00582U1 (et) * | 2004-04-20 | 2006-01-16 | Keemilise ja Bioloogilise Füüsika Instituut | Kõrge lahutusega madaltemperatuurne tahke keha tuumamagnetresonantsi mõõtepea |
| US7170292B2 (en) * | 2004-10-20 | 2007-01-30 | Doty Scientific, Inc. | NMR MAS inflow bernoulli bearing |
| DE202006002074U1 (de) * | 2006-02-08 | 2006-07-13 | AixNMR Zentrum für Magnetische Resonanz e.V. | Unilateraler NMR Sensor mit mikroskopischer Tiefenauflösung |
| JP2007315886A (ja) * | 2006-05-25 | 2007-12-06 | Hitachi Ltd | 核磁気共鳴装置用気体軸受および核磁気共鳴装置 |
| DE102006048955B4 (de) * | 2006-10-17 | 2010-12-16 | Bruker Biospin Gmbh | Vollautomatische MAS-NMR-Apparatur |
| US7541807B2 (en) * | 2007-07-19 | 2009-06-02 | Varian, Inc. | Rotor drive apparatus and methods utilizing center-fed radial-outflow gas |
| WO2009130002A1 (de) * | 2008-04-23 | 2009-10-29 | Gsi Helmholtzzentrum Für Schwerionenforschung Gmbh | Magnetfelderzeugungsvorrichtung |
| JP5445754B2 (ja) * | 2009-10-01 | 2014-03-19 | 株式会社 Ｊｅｏｌ Ｒｅｓｏｎａｎｃｅ | Ｎｍｒにおけるマジック角精密調整方法及び装置 |
| EP2498098B1 (en) * | 2011-03-09 | 2013-05-22 | Bruker BioSpin AG | Method for NMR spectroscopy on solid samples |
| RU2472139C1 (ru) * | 2011-08-15 | 2013-01-10 | Общество с ограниченной ответственностью "УНИСИТ" (ООО "УНИСИТ") | Ячейка для осуществления спектральных измерений методом спектроскопии ядерного магнитного резонанса при вращении образца вещества под магическим углом |
| US9063060B2 (en) * | 2011-10-10 | 2015-06-23 | Jeol Resonance Inc. | Solid-state NMR spectrometer, sample holder therefor, and method of solid-state NMR spectroscopy |
| FR2986609B1 (fr) * | 2012-02-07 | 2017-06-02 | Commissariat Energie Atomique | Dispositif d'isolation thermique et procede de fonctionnement d'un tel dispositif |
| JP5953633B2 (ja) * | 2012-10-09 | 2016-07-20 | 日本電子株式会社 | Ｎｍｒ測定用スピナ |
| KR101458978B1 (ko) * | 2013-10-17 | 2014-11-07 | 한국기초과학지원연구원 | 폐순환 가스루프를 이용한 핵자기 공명장치용 극저온 프로브 |
| DE102016218772A1 (de) * | 2016-09-28 | 2018-03-29 | Bruker Biospin Gmbh | Verbesserte Temperierung eines NMR-MAS-Rotors |
| CN108590629B (zh) | 2018-03-23 | 2020-09-18 | 中国石油大学(北京) | 井下三维扫描核磁共振成像测井仪探头、天线、及仪器 |
| JP6823304B2 (ja) * | 2018-08-31 | 2021-02-03 | 国立大学法人大阪大学 | Ｎｍｒプローブシステム及びｎｍｒプローブシステム使用方法 |
| DE102019202001B3 (de) * | 2019-02-14 | 2020-06-25 | Bruker Biospin Gmbh | MAS-Probenkopf mit thermisch isolierter Probenkammer |
| RU201791U1 (ru) * | 2020-07-28 | 2021-01-13 | Федеральное государственное бюджетное учреждение науки институт химии растворов им. Г.А. Крестова Российской академии наук | Ячейка высокого давления для регистрации спектров ядерного магнитного резонанса при сверхкритических параметрах состояния |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2960649A (en) * | 1954-06-18 | 1960-11-15 | Bloch Felix | Line narrowing gyromagnetic apparatus |
| NL239213A (https=) * | 1958-06-05 | |||
| US3462677A (en) * | 1967-06-12 | 1969-08-19 | Varian Associates | Gyromagnetic resonance spectrometer having means for measuring the rate of sample rotation |
| US3512078A (en) * | 1967-06-12 | 1970-05-12 | Varian Associates | Gyromagnetic resonance spectrometer employing air pressure for ejecting samples from the magnet |
| US3588677A (en) * | 1968-05-15 | 1971-06-28 | Jury Lvovich Kleiman | Device for rotation of a thermostatted sample |
| US3681683A (en) * | 1970-09-14 | 1972-08-01 | Varian Associates | Gyromagnetic resonance spectrometer utilizing an improved sample spinning and ejecting structure |
| GB1480478A (en) * | 1973-05-21 | 1977-07-20 | Perkin Elmer Ltd | Spinning in a magnetic field |
| US4088944A (en) * | 1976-10-04 | 1978-05-09 | Varian Associates, Inc. | NMR Spectrometer employing self centering turbine |
-
1977
- 1977-06-03 SU SU772491999A patent/SU765724A1/ru active
-
1978
- 1978-02-27 DD DD78203867A patent/DD136769A1/xx not_active IP Right Cessation
- 1978-02-28 CA CA297,905A patent/CA1098170A/en not_active Expired
- 1978-03-01 GB GB8106/78A patent/GB1594042A/en not_active Expired
- 1978-03-02 CH CH228878A patent/CH628143A5/de not_active IP Right Cessation
- 1978-03-03 DE DE2809237A patent/DE2809237C2/de not_active Expired
- 1978-03-03 IT IT20875/78A patent/IT1093167B/it active
- 1978-03-06 FR FR7806330A patent/FR2393304A1/fr active Granted
- 1978-03-27 US US05/890,252 patent/US4254373A/en not_active Expired - Lifetime
- 1978-04-04 JP JP3963978A patent/JPS5417796A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| IT7820875A0 (it) | 1978-03-03 |
| IT1093167B (it) | 1985-07-19 |
| DE2809237A1 (de) | 1979-01-11 |
| FR2393304A1 (fr) | 1978-12-29 |
| JPS5417796A (en) | 1979-02-09 |
| FR2393304B1 (https=) | 1979-09-07 |
| DD136769A1 (de) | 1979-07-25 |
| CH628143A5 (de) | 1982-02-15 |
| CA1098170A (en) | 1981-03-24 |
| SU765724A1 (ru) | 1980-09-23 |
| US4254373A (en) | 1981-03-03 |
| DE2809237C2 (de) | 1984-04-26 |
| GB1594042A (en) | 1981-07-30 |
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