CA1098170A - Sensor for generating nuclear magnetic resonance signals - Google Patents
Sensor for generating nuclear magnetic resonance signalsInfo
- Publication number
- CA1098170A CA1098170A CA297,905A CA297905A CA1098170A CA 1098170 A CA1098170 A CA 1098170A CA 297905 A CA297905 A CA 297905A CA 1098170 A CA1098170 A CA 1098170A
- Authority
- CA
- Canada
- Prior art keywords
- sensor
- rotor
- frame
- gas
- gap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000005481 NMR spectroscopy Methods 0.000 title claims abstract description 37
- 238000012360 testing method Methods 0.000 claims abstract description 21
- 239000000523 sample Substances 0.000 claims description 26
- 238000004804 winding Methods 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 8
- 230000006698 induction Effects 0.000 claims description 6
- 230000035945 sensitivity Effects 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 239000011521 glass Substances 0.000 claims description 4
- 239000000919 ceramic Substances 0.000 claims description 3
- 239000010453 quartz Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 230000005284 excitation Effects 0.000 claims description 2
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 238000013022 venting Methods 0.000 claims 1
- 239000007789 gas Substances 0.000 description 29
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 6
- 238000007373 indentation Methods 0.000 description 4
- 238000011835 investigation Methods 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229940102098 revolution Drugs 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 1
- 229920004943 Delrin® Polymers 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 238000001460 carbon-13 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- -1 for example Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000000696 magnetic material Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
- G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
- G01R33/307—Sample handling arrangements, e.g. sample cells, spinning mechanisms specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
- G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
- G01R33/31—Temperature control thereof
Landscapes
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU2491999 | 1977-06-03 | ||
| SU772491999A SU765724A1 (ru) | 1977-06-03 | 1977-06-03 | Датчик сигналов дерного магнитного резонанса |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1098170A true CA1098170A (en) | 1981-03-24 |
Family
ID=20711508
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA297,905A Expired CA1098170A (en) | 1977-06-03 | 1978-02-28 | Sensor for generating nuclear magnetic resonance signals |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4254373A (https=) |
| JP (1) | JPS5417796A (https=) |
| CA (1) | CA1098170A (https=) |
| CH (1) | CH628143A5 (https=) |
| DD (1) | DD136769A1 (https=) |
| DE (1) | DE2809237C2 (https=) |
| FR (1) | FR2393304A1 (https=) |
| GB (1) | GB1594042A (https=) |
| IT (1) | IT1093167B (https=) |
| SU (1) | SU765724A1 (https=) |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4201941A (en) * | 1978-08-04 | 1980-05-06 | International Business Machines Corporation | Spinning apparatus for NMR spectrometers |
| US4275350A (en) * | 1979-05-29 | 1981-06-23 | Varian Associates, Inc. | Sample spinning mechanism for NMR probes |
| JPS6051056B2 (ja) | 1980-06-13 | 1985-11-12 | 株式会社東芝 | 核磁気共鳴装置 |
| US4306878A (en) * | 1980-08-29 | 1981-12-22 | Brown Charles E | Method of selecting flame retardants for polymers |
| US4352066A (en) * | 1980-10-31 | 1982-09-28 | International Business Machines Corporation | Method for adjusting the magic angle in NMR experiments |
| US4446430A (en) * | 1981-08-31 | 1984-05-01 | Monsanto Company | Sample spinner for nuclear magnetic resonance spectrometer |
| US4456882A (en) * | 1982-01-04 | 1984-06-26 | University Of South Carolina | High speed cylindrical nuclear magnetic resonance (NMR) sample spinner |
| JPS58167947A (ja) * | 1982-03-29 | 1983-10-04 | Hitachi Ltd | 核磁気共鳴装置のスピンナ |
| US4511841A (en) * | 1982-06-17 | 1985-04-16 | Chemagnetics, Inc. | Method and apparatus for high speed magic angle spinning |
| US4510450A (en) * | 1982-09-28 | 1985-04-09 | The Medical College Of Wisconsin, Inc. | Apparatus and assay method for the quantitative determination of mineral content in bone |
| US4517516A (en) * | 1983-04-08 | 1985-05-14 | Varian Associates, Inc. | NMR Probe coil form structure |
| US4587492A (en) * | 1984-03-02 | 1986-05-06 | Varian Associates, Inc. | Thermal barrier for variable temperature NMR |
| US4739270A (en) * | 1986-06-03 | 1988-04-19 | Varian Associates, Inc. | High speed spinner for NMR spectrometer |
| US4940942A (en) * | 1989-04-14 | 1990-07-10 | Bartuska Victor J | Method and apparatus for conducting variable-temperature solid state magnetic resonance spectroscopy |
| US5416414A (en) * | 1990-04-27 | 1995-05-16 | British Technology Group Limited | Sample mount for NMR microscopy |
| US5202633A (en) * | 1990-11-01 | 1993-04-13 | Doty Scientific, Inc. | High temperature nmr sample spinner |
| JP3749550B2 (ja) * | 1991-12-19 | 2006-03-01 | バリアン・インコーポレイテッド | Nmrサンプルシェーパー |
| US5325059A (en) * | 1992-03-26 | 1994-06-28 | Doty Scientific Inc. | DOR NMR sample spinner |
| US5289130A (en) * | 1992-07-31 | 1994-02-22 | Doty Scientific Inc. | NMR sample rotor cooling technique |
| US5408181A (en) * | 1993-08-30 | 1995-04-18 | Auburn International, Inc. | NMR system for measuring polymer properties |
| DE4440241C1 (de) * | 1994-10-25 | 1996-03-21 | Rainer Schmieg | Turbine |
| US6054857A (en) * | 1997-03-18 | 2000-04-25 | Doty Scientific, Inc. | NMR MAS sealing sample cells and methods |
| EE00330U1 (et) | 2002-05-30 | 2002-10-15 | Keemilise ja Bioloogilise F��sika Instituut | Tuuma magnetresonants-spektromeetri mõõtepea |
| EE00582U1 (et) * | 2004-04-20 | 2006-01-16 | Keemilise ja Bioloogilise Füüsika Instituut | Kõrge lahutusega madaltemperatuurne tahke keha tuumamagnetresonantsi mõõtepea |
| US7170292B2 (en) * | 2004-10-20 | 2007-01-30 | Doty Scientific, Inc. | NMR MAS inflow bernoulli bearing |
| DE202006002074U1 (de) * | 2006-02-08 | 2006-07-13 | AixNMR Zentrum für Magnetische Resonanz e.V. | Unilateraler NMR Sensor mit mikroskopischer Tiefenauflösung |
| JP2007315886A (ja) * | 2006-05-25 | 2007-12-06 | Hitachi Ltd | 核磁気共鳴装置用気体軸受および核磁気共鳴装置 |
| DE102006048955B4 (de) * | 2006-10-17 | 2010-12-16 | Bruker Biospin Gmbh | Vollautomatische MAS-NMR-Apparatur |
| US7541807B2 (en) * | 2007-07-19 | 2009-06-02 | Varian, Inc. | Rotor drive apparatus and methods utilizing center-fed radial-outflow gas |
| WO2009130002A1 (de) * | 2008-04-23 | 2009-10-29 | Gsi Helmholtzzentrum Für Schwerionenforschung Gmbh | Magnetfelderzeugungsvorrichtung |
| JP5445754B2 (ja) * | 2009-10-01 | 2014-03-19 | 株式会社 Jeol Resonance | Nmrにおけるマジック角精密調整方法及び装置 |
| EP2498098B1 (en) * | 2011-03-09 | 2013-05-22 | Bruker BioSpin AG | Method for NMR spectroscopy on solid samples |
| RU2472139C1 (ru) * | 2011-08-15 | 2013-01-10 | Общество с ограниченной ответственностью "УНИСИТ" (ООО "УНИСИТ") | Ячейка для осуществления спектральных измерений методом спектроскопии ядерного магнитного резонанса при вращении образца вещества под магическим углом |
| US9063060B2 (en) * | 2011-10-10 | 2015-06-23 | Jeol Resonance Inc. | Solid-state NMR spectrometer, sample holder therefor, and method of solid-state NMR spectroscopy |
| FR2986609B1 (fr) * | 2012-02-07 | 2017-06-02 | Commissariat Energie Atomique | Dispositif d'isolation thermique et procede de fonctionnement d'un tel dispositif |
| JP5953633B2 (ja) * | 2012-10-09 | 2016-07-20 | 日本電子株式会社 | Nmr測定用スピナ |
| KR101458978B1 (ko) * | 2013-10-17 | 2014-11-07 | 한국기초과학지원연구원 | 폐순환 가스루프를 이용한 핵자기 공명장치용 극저온 프로브 |
| DE102016218772A1 (de) * | 2016-09-28 | 2018-03-29 | Bruker Biospin Gmbh | Verbesserte Temperierung eines NMR-MAS-Rotors |
| CN108590629B (zh) | 2018-03-23 | 2020-09-18 | 中国石油大学(北京) | 井下三维扫描核磁共振成像测井仪探头、天线、及仪器 |
| JP6823304B2 (ja) * | 2018-08-31 | 2021-02-03 | 国立大学法人大阪大学 | Nmrプローブシステム及びnmrプローブシステム使用方法 |
| DE102019202001B3 (de) * | 2019-02-14 | 2020-06-25 | Bruker Biospin Gmbh | MAS-Probenkopf mit thermisch isolierter Probenkammer |
| RU201791U1 (ru) * | 2020-07-28 | 2021-01-13 | Федеральное государственное бюджетное учреждение науки институт химии растворов им. Г.А. Крестова Российской академии наук | Ячейка высокого давления для регистрации спектров ядерного магнитного резонанса при сверхкритических параметрах состояния |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2960649A (en) * | 1954-06-18 | 1960-11-15 | Bloch Felix | Line narrowing gyromagnetic apparatus |
| NL239213A (https=) * | 1958-06-05 | |||
| US3462677A (en) * | 1967-06-12 | 1969-08-19 | Varian Associates | Gyromagnetic resonance spectrometer having means for measuring the rate of sample rotation |
| US3512078A (en) * | 1967-06-12 | 1970-05-12 | Varian Associates | Gyromagnetic resonance spectrometer employing air pressure for ejecting samples from the magnet |
| US3588677A (en) * | 1968-05-15 | 1971-06-28 | Jury Lvovich Kleiman | Device for rotation of a thermostatted sample |
| US3681683A (en) * | 1970-09-14 | 1972-08-01 | Varian Associates | Gyromagnetic resonance spectrometer utilizing an improved sample spinning and ejecting structure |
| GB1480478A (en) * | 1973-05-21 | 1977-07-20 | Perkin Elmer Ltd | Spinning in a magnetic field |
| US4088944A (en) * | 1976-10-04 | 1978-05-09 | Varian Associates, Inc. | NMR Spectrometer employing self centering turbine |
-
1977
- 1977-06-03 SU SU772491999A patent/SU765724A1/ru active
-
1978
- 1978-02-27 DD DD78203867A patent/DD136769A1/xx not_active IP Right Cessation
- 1978-02-28 CA CA297,905A patent/CA1098170A/en not_active Expired
- 1978-03-01 GB GB8106/78A patent/GB1594042A/en not_active Expired
- 1978-03-02 CH CH228878A patent/CH628143A5/de not_active IP Right Cessation
- 1978-03-03 DE DE2809237A patent/DE2809237C2/de not_active Expired
- 1978-03-03 IT IT20875/78A patent/IT1093167B/it active
- 1978-03-06 FR FR7806330A patent/FR2393304A1/fr active Granted
- 1978-03-27 US US05/890,252 patent/US4254373A/en not_active Expired - Lifetime
- 1978-04-04 JP JP3963978A patent/JPS5417796A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| IT7820875A0 (it) | 1978-03-03 |
| IT1093167B (it) | 1985-07-19 |
| DE2809237A1 (de) | 1979-01-11 |
| FR2393304A1 (fr) | 1978-12-29 |
| JPS5417796A (en) | 1979-02-09 |
| JPS6352339B2 (https=) | 1988-10-18 |
| FR2393304B1 (https=) | 1979-09-07 |
| DD136769A1 (de) | 1979-07-25 |
| CH628143A5 (de) | 1982-02-15 |
| SU765724A1 (ru) | 1980-09-23 |
| US4254373A (en) | 1981-03-03 |
| DE2809237C2 (de) | 1984-04-26 |
| GB1594042A (en) | 1981-07-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |